Microwave-assisted synthesis of biologically active amide derivatives of naphthenic acids under neat conditions
Within the field of green chemistry, a noticeable results were obtained in the solvent-free synthesis of amide derivatives of naphthenic acids under microwave irradiation. Naphthenic acid amides, anilides, and morpholides were synthesized directly from free carboxylic acids and amines in the absence...
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| Format: | Article |
| Language: | English |
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Society of Chemists and Technologists of Macedonia
2018-06-01
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| Series: | Macedonian Journal of Chemistry and Chemical Engineering |
| Subjects: | |
| Online Access: | https://mjcce.org.mk/index.php/MJCCE/article/view/1371 |
| _version_ | 1818616463085273088 |
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| author | Ljubica Grbović Bojana Radovan Vasiljević Ksenija Pavlović Timea Hajnal-Jafari Simonida Đurić Mirjana Popsavin Slavko Kevrešan |
| author_facet | Ljubica Grbović Bojana Radovan Vasiljević Ksenija Pavlović Timea Hajnal-Jafari Simonida Đurić Mirjana Popsavin Slavko Kevrešan |
| author_sort | Ljubica Grbović |
| collection | DOAJ |
| description | Within the field of green chemistry, a noticeable results were obtained in the solvent-free synthesis of amide derivatives of naphthenic acids under microwave irradiation. Naphthenic acid amides, anilides, and morpholides were synthesized directly from free carboxylic acids and amines in the absence of solvent and catalyst under high-temperature heating in a closed-vessel system of microwave reactor. With this new and efficient method, different primary, secondary, and tertiary amide derivatives of naphthenic acids were obtained in good to excellent yields. Synthesized derivatives were assayed as plant rooting agents for their stimulative effects on the formation of adventitious roots in sunflower cuttings and susceptibility for growth stimulation of Pseudomonas sp. strains. |
| first_indexed | 2024-12-16T16:50:12Z |
| format | Article |
| id | doaj.art-0dbcf19cd0294398abfbf27d269fb44e |
| institution | Directory Open Access Journal |
| issn | 1857-5552 1857-5625 |
| language | English |
| last_indexed | 2024-12-16T16:50:12Z |
| publishDate | 2018-06-01 |
| publisher | Society of Chemists and Technologists of Macedonia |
| record_format | Article |
| series | Macedonian Journal of Chemistry and Chemical Engineering |
| spelling | doaj.art-0dbcf19cd0294398abfbf27d269fb44e2022-12-21T22:24:03ZengSociety of Chemists and Technologists of MacedoniaMacedonian Journal of Chemistry and Chemical Engineering1857-55521857-56252018-06-01371132010.20450/mjcce.2018.1371355Microwave-assisted synthesis of biologically active amide derivatives of naphthenic acids under neat conditionsLjubica Grbović0Bojana Radovan Vasiljević1Ksenija Pavlović2Timea Hajnal-Jafari3Simonida Đurić4Mirjana Popsavin5Slavko Kevrešan6Department of Chemistry, Biochemistry and Environmental Protection, Faculty of Sciences, University of Novi Sad, Trg Dositeja Obradovića 3, 21 000 Novi SadDepartment of Chemistry, Biochemistry and Environmental Protection, Faculty of Sciences, University of Novi Sad, Trg Dositeja Obradovića 3, 21 000 Novi SadDepartment of Chemistry, Biochemistry and Environmental Protection, Faculty of Sciences, University of Novi Sad, Trg Dositeja Obradovića 3, 21 000 Novi SadDepartment of Field and Vegetable Crops, Faculty of Agriculture, University of Novi Sad, Trg Dositeja Obradovića 8, 21 000 Novi SadDepartment of Field and Vegetable Crops, Faculty of Agriculture, University of Novi Sad, Trg Dositeja Obradovića 8, 21 000 Novi SadDepartment of Chemistry, Biochemistry and Environmental Protection, Faculty of Sciences, University of Novi Sad, Trg Dositeja Obradovića 3, 21 000 Novi SadDepartment of Field and Vegetable Crops, Faculty of Agriculture, University of Novi Sad, Trg Dositeja Obradovića 8, 21 000 Novi SadWithin the field of green chemistry, a noticeable results were obtained in the solvent-free synthesis of amide derivatives of naphthenic acids under microwave irradiation. Naphthenic acid amides, anilides, and morpholides were synthesized directly from free carboxylic acids and amines in the absence of solvent and catalyst under high-temperature heating in a closed-vessel system of microwave reactor. With this new and efficient method, different primary, secondary, and tertiary amide derivatives of naphthenic acids were obtained in good to excellent yields. Synthesized derivatives were assayed as plant rooting agents for their stimulative effects on the formation of adventitious roots in sunflower cuttings and susceptibility for growth stimulation of Pseudomonas sp. strains.https://mjcce.org.mk/index.php/MJCCE/article/view/1371green chemistry, naphthenic acid amidessolvent-free synthesisplant rooting agents, bacterial proliferation |
| spellingShingle | Ljubica Grbović Bojana Radovan Vasiljević Ksenija Pavlović Timea Hajnal-Jafari Simonida Đurić Mirjana Popsavin Slavko Kevrešan Microwave-assisted synthesis of biologically active amide derivatives of naphthenic acids under neat conditions Macedonian Journal of Chemistry and Chemical Engineering green chemistry, naphthenic acid amides solvent-free synthesis plant rooting agents, bacterial proliferation |
| title | Microwave-assisted synthesis of biologically active amide derivatives of naphthenic acids under neat conditions |
| title_full | Microwave-assisted synthesis of biologically active amide derivatives of naphthenic acids under neat conditions |
| title_fullStr | Microwave-assisted synthesis of biologically active amide derivatives of naphthenic acids under neat conditions |
| title_full_unstemmed | Microwave-assisted synthesis of biologically active amide derivatives of naphthenic acids under neat conditions |
| title_short | Microwave-assisted synthesis of biologically active amide derivatives of naphthenic acids under neat conditions |
| title_sort | microwave assisted synthesis of biologically active amide derivatives of naphthenic acids under neat conditions |
| topic | green chemistry, naphthenic acid amides solvent-free synthesis plant rooting agents, bacterial proliferation |
| url | https://mjcce.org.mk/index.php/MJCCE/article/view/1371 |
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