Synthesis of cubic Y zeolite using a pulsed microwave heating system
Cubic Y zeolite were successfully synthesized using microwave heating for 18 - 25 min, whereas 10 - 50 h are required by hydrothermal heating technique depending upon the lattice Si/Al ratio. To this end, we used a commercial microwave oven modified in order to provide pulsed microwave pumping on th...
| Main Authors: | , , , , , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol)
1999-01-01
|
| Series: | Materials Research |
| Subjects: | |
| Online Access: | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14391999000200011 |
| _version_ | 1818526697265299456 |
|---|---|
| author | Araújo L.R.G. de Cavalcante Jr. C.L. Farias K.M. Guedes I. Sasaki J.M. Freire P.T.C. Melo F.E.A. Mendes-Filho J. |
| author_facet | Araújo L.R.G. de Cavalcante Jr. C.L. Farias K.M. Guedes I. Sasaki J.M. Freire P.T.C. Melo F.E.A. Mendes-Filho J. |
| author_sort | Araújo L.R.G. de |
| collection | DOAJ |
| description | Cubic Y zeolite were successfully synthesized using microwave heating for 18 - 25 min, whereas 10 - 50 h are required by hydrothermal heating technique depending upon the lattice Si/Al ratio. To this end, we used a commercial microwave oven modified in order to provide pulsed microwave pumping on the synthesis mixtures. The obtained samples were analyzed by X-ray diffraction, BET surface area and infrared spectroscopy measurements. As a result, we verify that Y zeolite samples obtained from hydrogels containing low aluminum contents, present a good degree of crystallinity and then can be suitable for using in adsorption and catalysis experiments. |
| first_indexed | 2024-12-11T06:26:27Z |
| format | Article |
| id | doaj.art-0eff223e522e44b69150711c3585b678 |
| institution | Directory Open Access Journal |
| issn | 1516-1439 |
| language | English |
| last_indexed | 2024-12-11T06:26:27Z |
| publishDate | 1999-01-01 |
| publisher | Associação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol) |
| record_format | Article |
| series | Materials Research |
| spelling | doaj.art-0eff223e522e44b69150711c3585b6782022-12-22T01:17:39ZengAssociação Brasileira de Metalurgia e Materiais (ABM); Associação Brasileira de Cerâmica (ABC); Associação Brasileira de Polímeros (ABPol)Materials Research1516-14391999-01-0122105109Synthesis of cubic Y zeolite using a pulsed microwave heating systemAraújo L.R.G. deCavalcante Jr. C.L.Farias K.M.Guedes I.Sasaki J.M.Freire P.T.C.Melo F.E.A.Mendes-Filho J.Cubic Y zeolite were successfully synthesized using microwave heating for 18 - 25 min, whereas 10 - 50 h are required by hydrothermal heating technique depending upon the lattice Si/Al ratio. To this end, we used a commercial microwave oven modified in order to provide pulsed microwave pumping on the synthesis mixtures. The obtained samples were analyzed by X-ray diffraction, BET surface area and infrared spectroscopy measurements. As a result, we verify that Y zeolite samples obtained from hydrogels containing low aluminum contents, present a good degree of crystallinity and then can be suitable for using in adsorption and catalysis experiments.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14391999000200011synthetic zeolitesmicrowave heatingX-ray and infrared spectroscopy |
| spellingShingle | Araújo L.R.G. de Cavalcante Jr. C.L. Farias K.M. Guedes I. Sasaki J.M. Freire P.T.C. Melo F.E.A. Mendes-Filho J. Synthesis of cubic Y zeolite using a pulsed microwave heating system Materials Research synthetic zeolites microwave heating X-ray and infrared spectroscopy |
| title | Synthesis of cubic Y zeolite using a pulsed microwave heating system |
| title_full | Synthesis of cubic Y zeolite using a pulsed microwave heating system |
| title_fullStr | Synthesis of cubic Y zeolite using a pulsed microwave heating system |
| title_full_unstemmed | Synthesis of cubic Y zeolite using a pulsed microwave heating system |
| title_short | Synthesis of cubic Y zeolite using a pulsed microwave heating system |
| title_sort | synthesis of cubic y zeolite using a pulsed microwave heating system |
| topic | synthetic zeolites microwave heating X-ray and infrared spectroscopy |
| url | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-14391999000200011 |
| work_keys_str_mv | AT araujolrgde synthesisofcubicyzeoliteusingapulsedmicrowaveheatingsystem AT cavalcantejrcl synthesisofcubicyzeoliteusingapulsedmicrowaveheatingsystem AT fariaskm synthesisofcubicyzeoliteusingapulsedmicrowaveheatingsystem AT guedesi synthesisofcubicyzeoliteusingapulsedmicrowaveheatingsystem AT sasakijm synthesisofcubicyzeoliteusingapulsedmicrowaveheatingsystem AT freireptc synthesisofcubicyzeoliteusingapulsedmicrowaveheatingsystem AT melofea synthesisofcubicyzeoliteusingapulsedmicrowaveheatingsystem AT mendesfilhoj synthesisofcubicyzeoliteusingapulsedmicrowaveheatingsystem |