Effect depositions parameters on the characteristics of Ni0.5Co0.5Fe2O4 nanocomposite films prepared by DC reactive magnetron Co-Sputtering technique
In this work, spinel ferrites (NiCoFe2O4) were prepared as thin films by dc reactive dual-magnetron co-sputtering technique. Effects of some operation parameters, such as inter-electrode distance, and preparation conditions such as mixing ratio of argon and oxygen in the gas mixture, on the structu...
Main Authors: | , |
---|---|
Format: | Article |
Language: | English |
Published: |
University of Baghdad
2020-06-01
|
Series: | Iraqi Journal of Physics |
Subjects: | |
Online Access: | https://ijp.uobaghdad.edu.iq/index.php/physics/article/view/546 |
_version_ | 1827993268057538560 |
---|---|
author | Tawfiq S. Mahdi Firas J. Kadhim |
author_facet | Tawfiq S. Mahdi Firas J. Kadhim |
author_sort | Tawfiq S. Mahdi |
collection | DOAJ |
description |
In this work, spinel ferrites (NiCoFe2O4) were prepared as thin films by dc reactive dual-magnetron co-sputtering technique. Effects of some operation parameters, such as inter-electrode distance, and preparation conditions such as mixing ratio of argon and oxygen in the gas mixture, on the structural and spectroscopic characteristics of the prepared samples were studied. For samples prepared at inter-electrode distance of 5 cm, only one functional group of OH- was observed in the FTIR spectra as all bands belonging to the metal-oxygen vibration were observed. Similarly, the XRD results showed that decreasing the pressure of oxygen in the gas mixture lead to grow more crystal planes in the samples prepared at inter-electrode distance of 5 cm. The energy band gap was determined for the sample prepared with mixing ratio of 65:35 and found to be 2.7, 2 and 3.35 eV for direct allowed, direct forbidden and indirect allowed transitions, respectively. The high structural purity was confirmed as no traces for any elements other than Co, Ni, Fe and O were found in the final samples.
|
first_indexed | 2024-04-10T04:22:27Z |
format | Article |
id | doaj.art-0f6751db362e453a88295b874c98d1bd |
institution | Directory Open Access Journal |
issn | 2070-4003 2664-5548 |
language | English |
last_indexed | 2024-04-10T04:22:27Z |
publishDate | 2020-06-01 |
publisher | University of Baghdad |
record_format | Article |
series | Iraqi Journal of Physics |
spelling | doaj.art-0f6751db362e453a88295b874c98d1bd2023-03-10T20:54:01ZengUniversity of BaghdadIraqi Journal of Physics2070-40032664-55482020-06-01184510.30723/ijp.v18i45.546Effect depositions parameters on the characteristics of Ni0.5Co0.5Fe2O4 nanocomposite films prepared by DC reactive magnetron Co-Sputtering techniqueTawfiq S. Mahdi0Firas J. Kadhim1Department of Physics, College of Science, University of BaghdadDepartment of Physics, College of Science, University of Baghdad In this work, spinel ferrites (NiCoFe2O4) were prepared as thin films by dc reactive dual-magnetron co-sputtering technique. Effects of some operation parameters, such as inter-electrode distance, and preparation conditions such as mixing ratio of argon and oxygen in the gas mixture, on the structural and spectroscopic characteristics of the prepared samples were studied. For samples prepared at inter-electrode distance of 5 cm, only one functional group of OH- was observed in the FTIR spectra as all bands belonging to the metal-oxygen vibration were observed. Similarly, the XRD results showed that decreasing the pressure of oxygen in the gas mixture lead to grow more crystal planes in the samples prepared at inter-electrode distance of 5 cm. The energy band gap was determined for the sample prepared with mixing ratio of 65:35 and found to be 2.7, 2 and 3.35 eV for direct allowed, direct forbidden and indirect allowed transitions, respectively. The high structural purity was confirmed as no traces for any elements other than Co, Ni, Fe and O were found in the final samples. https://ijp.uobaghdad.edu.iq/index.php/physics/article/view/546Magnetron sputteringReactive sputteringSpinel ferritesThin films |
spellingShingle | Tawfiq S. Mahdi Firas J. Kadhim Effect depositions parameters on the characteristics of Ni0.5Co0.5Fe2O4 nanocomposite films prepared by DC reactive magnetron Co-Sputtering technique Iraqi Journal of Physics Magnetron sputtering Reactive sputtering Spinel ferrites Thin films |
title | Effect depositions parameters on the characteristics of Ni0.5Co0.5Fe2O4 nanocomposite films prepared by DC reactive magnetron Co-Sputtering technique |
title_full | Effect depositions parameters on the characteristics of Ni0.5Co0.5Fe2O4 nanocomposite films prepared by DC reactive magnetron Co-Sputtering technique |
title_fullStr | Effect depositions parameters on the characteristics of Ni0.5Co0.5Fe2O4 nanocomposite films prepared by DC reactive magnetron Co-Sputtering technique |
title_full_unstemmed | Effect depositions parameters on the characteristics of Ni0.5Co0.5Fe2O4 nanocomposite films prepared by DC reactive magnetron Co-Sputtering technique |
title_short | Effect depositions parameters on the characteristics of Ni0.5Co0.5Fe2O4 nanocomposite films prepared by DC reactive magnetron Co-Sputtering technique |
title_sort | effect depositions parameters on the characteristics of ni0 5co0 5fe2o4 nanocomposite films prepared by dc reactive magnetron co sputtering technique |
topic | Magnetron sputtering Reactive sputtering Spinel ferrites Thin films |
url | https://ijp.uobaghdad.edu.iq/index.php/physics/article/view/546 |
work_keys_str_mv | AT tawfiqsmahdi effectdepositionsparametersonthecharacteristicsofni05co05fe2o4nanocompositefilmspreparedbydcreactivemagnetroncosputteringtechnique AT firasjkadhim effectdepositionsparametersonthecharacteristicsofni05co05fe2o4nanocompositefilmspreparedbydcreactivemagnetroncosputteringtechnique |