4-Chloro-N′-(2-hydroxy-4-methoxybenzylidene)benzohydrazide methanol monosolvate
The title compound, C15H13ClN2O3·CH3OH, was synthesized by the condensation reaction of 2-hydroxy-4-methoxybenzaldehyde with 4-chlorobenzohydrazide in methanol. The Schiff base molecule displays a trans configuration with respect to the C=N and C—N bonds. The dihedral angl...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2011-11-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536811039778 |
| _version_ | 1818958769419190272 |
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| author | Feng Zhi Rong Wang Yi Zhang Qiang Wang Yi-Lin Yang |
| author_facet | Feng Zhi Rong Wang Yi Zhang Qiang Wang Yi-Lin Yang |
| author_sort | Feng Zhi |
| collection | DOAJ |
| description | The title compound, C15H13ClN2O3·CH3OH, was synthesized by the condensation reaction of 2-hydroxy-4-methoxybenzaldehyde with 4-chlorobenzohydrazide in methanol. The Schiff base molecule displays a trans configuration with respect to the C=N and C—N bonds. The dihedral angle between the two benzene rings is 5.3 (2)°. In the crystal, molecules are linked by N—H...O and O—H...O hydrogen-bond interactions into chains running parallel to the a axis. An intramolecular O—H...N hydrogen bond is observed. |
| first_indexed | 2024-12-20T11:31:00Z |
| format | Article |
| id | doaj.art-0ffdd7e275274c51a268889ca3008d41 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-20T11:31:00Z |
| publishDate | 2011-11-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-0ffdd7e275274c51a268889ca3008d412022-12-21T19:42:15ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682011-11-016711o2825o282510.1107/S16005368110397784-Chloro-N′-(2-hydroxy-4-methoxybenzylidene)benzohydrazide methanol monosolvateFeng ZhiRong WangYi ZhangQiang WangYi-Lin YangThe title compound, C15H13ClN2O3·CH3OH, was synthesized by the condensation reaction of 2-hydroxy-4-methoxybenzaldehyde with 4-chlorobenzohydrazide in methanol. The Schiff base molecule displays a trans configuration with respect to the C=N and C—N bonds. The dihedral angle between the two benzene rings is 5.3 (2)°. In the crystal, molecules are linked by N—H...O and O—H...O hydrogen-bond interactions into chains running parallel to the a axis. An intramolecular O—H...N hydrogen bond is observed.http://scripts.iucr.org/cgi-bin/paper?S1600536811039778 |
| spellingShingle | Feng Zhi Rong Wang Yi Zhang Qiang Wang Yi-Lin Yang 4-Chloro-N′-(2-hydroxy-4-methoxybenzylidene)benzohydrazide methanol monosolvate Acta Crystallographica Section E |
| title | 4-Chloro-N′-(2-hydroxy-4-methoxybenzylidene)benzohydrazide methanol monosolvate |
| title_full | 4-Chloro-N′-(2-hydroxy-4-methoxybenzylidene)benzohydrazide methanol monosolvate |
| title_fullStr | 4-Chloro-N′-(2-hydroxy-4-methoxybenzylidene)benzohydrazide methanol monosolvate |
| title_full_unstemmed | 4-Chloro-N′-(2-hydroxy-4-methoxybenzylidene)benzohydrazide methanol monosolvate |
| title_short | 4-Chloro-N′-(2-hydroxy-4-methoxybenzylidene)benzohydrazide methanol monosolvate |
| title_sort | 4 chloro n amp 8242 2 hydroxy 4 methoxybenzylidene benzohydrazide methanol monosolvate |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536811039778 |
| work_keys_str_mv | AT fengzhi 4chloronamp82422hydroxy4methoxybenzylidenebenzohydrazidemethanolmonosolvate AT rongwang 4chloronamp82422hydroxy4methoxybenzylidenebenzohydrazidemethanolmonosolvate AT yizhang 4chloronamp82422hydroxy4methoxybenzylidenebenzohydrazidemethanolmonosolvate AT qiangwang 4chloronamp82422hydroxy4methoxybenzylidenebenzohydrazidemethanolmonosolvate AT yilinyang 4chloronamp82422hydroxy4methoxybenzylidenebenzohydrazidemethanolmonosolvate |