Extraction of Tannic Acid from Kenaf Bast Fibre using Ultrasonic Assisted Extraction
Tannic acid or tannin, type of phenolic compound contains in kenaf bast fibre. Conventional extraction has certain limitations in terms of time, energy, and solvent consumption. Ultrasound assisted extraction (UAE) can extract bioactive components in shorter time, low temperature, with lesser energy...
| Main Authors: | , , , , , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
Polish Academy of Sciences
2022-08-01
|
| Series: | Archives of Metallurgy and Materials |
| Subjects: | |
| Online Access: | https://journals.pan.pl/Content/124059/PDF/AMM-2022-3-34-Mohamad.pdf |
| _version_ | 1818473154051309568 |
|---|---|
| author | M. Mohamad H.A. Ibrahim M.F.M. Nasir N.A. Mohidem N.F. Shoparwe P.T. Teo M.N. Masri A.R. Irfan |
| author_facet | M. Mohamad H.A. Ibrahim M.F.M. Nasir N.A. Mohidem N.F. Shoparwe P.T. Teo M.N. Masri A.R. Irfan |
| author_sort | M. Mohamad |
| collection | DOAJ |
| description | Tannic acid or tannin, type of phenolic compound contains in kenaf bast fibre. Conventional extraction has certain limitations in terms of time, energy, and solvent consumption. Ultrasound assisted extraction (UAE) can extract bioactive components in shorter time, low temperature, with lesser energy and solvent requirement. UAE as alternative extraction technique is better equipped to retain the functionality of the bioactive compounds. In this study, the conditions for ultrasound assisted extraction (UAE) of tannic acid from kenaf bast fibre by assessing the effect of sonication time and different duty cycles were optimized. The use of ultrasound to extract tannic acid from kenaf bast fiber was evaluated. Ultrasound-assisted extraction (UAE) was carried out using ethanol as solvent to intensify the extraction efficacy. Phytochemical screening was conducted to identify the presence of tannic acid in extracts. The extracts then were analyzed using High-Performance Liquid Chromatography (HPLC) and Scanning Electron Microscopy (SEM). It was found that 0.2429 mg/mL of tannic acid was obtained under the extraction conditions of extraction temperature of 40℃, sonication time of 20 minutes and duty cycle of 50%. From SEM analysis, it was found that the raw sample demonstrated rough surface and no porous but kenaf bast fibre display smoother surface with less impurities and few pores appeared after the extraction process using UAE. These results indicate that ultrasound-assisted extraction is an efficient method for extracting tannic acid from kenaf bast fibre with the advantages of lower extraction time and higher extraction yield. |
| first_indexed | 2024-04-14T04:19:21Z |
| format | Article |
| id | doaj.art-11aa4499156a4c44a579f7f720ef8302 |
| institution | Directory Open Access Journal |
| issn | 2300-1909 |
| language | English |
| last_indexed | 2024-04-14T04:19:21Z |
| publishDate | 2022-08-01 |
| publisher | Polish Academy of Sciences |
| record_format | Article |
| series | Archives of Metallurgy and Materials |
| spelling | doaj.art-11aa4499156a4c44a579f7f720ef83022022-12-22T02:12:34ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092022-08-01vol. 67No 310611066https://doi.org/10.24425/amm.2022.139703Extraction of Tannic Acid from Kenaf Bast Fibre using Ultrasonic Assisted ExtractionM. Mohamad0https://orcid.org/0000-0003-1376-5232H.A. Ibrahim1M.F.M. Nasir2N.A. Mohidem3https://orcid.org/0000-0001-9892-4823N.F. Shoparwe4P.T. Teo5https://orcid.org/0000-0002-2012-5981M.N. Masri6https://orcid.org/0000-0003-2577-6756A.R. Irfan7https://orcid.org/0000-0002-6606-9874Universiti Malaysia Kelantan, Faculty of Bioengineering and Technology, Jeli Campus, Kelantan, MalaysiaUniversiti Malaysia Kelantan, Faculty of Bioengineering and Technology, Jeli Campus, Kelantan, MalaysiaNational Kenaf and Tobacco Board, Kubang Kerian, Kelantan, MalaysiaUniversiti Putra Malaysia, Faculty of Engineering Selangor, Department of Biological and Agricultural Engineering, MalaysiaUniversiti Malaysia Kelantan, Faculty of Bioengineering and Technology, Jeli Campus, Kelantan, MalaysiaUniversiti Malaysia Kelantan, Faculty of Bioengineering and Technology, Jeli Campus, Kelantan, MalaysiaUniversiti Malaysia Kelantan, Faculty of Bioengineering and Technology, Jeli Campus, Kelantan, MalaysiaUniversiti Malaysia Perlis, Faculty of Mechanical Engineering Technology, Perlis, MalaysiaTannic acid or tannin, type of phenolic compound contains in kenaf bast fibre. Conventional extraction has certain limitations in terms of time, energy, and solvent consumption. Ultrasound assisted extraction (UAE) can extract bioactive components in shorter time, low temperature, with lesser energy and solvent requirement. UAE as alternative extraction technique is better equipped to retain the functionality of the bioactive compounds. In this study, the conditions for ultrasound assisted extraction (UAE) of tannic acid from kenaf bast fibre by assessing the effect of sonication time and different duty cycles were optimized. The use of ultrasound to extract tannic acid from kenaf bast fiber was evaluated. Ultrasound-assisted extraction (UAE) was carried out using ethanol as solvent to intensify the extraction efficacy. Phytochemical screening was conducted to identify the presence of tannic acid in extracts. The extracts then were analyzed using High-Performance Liquid Chromatography (HPLC) and Scanning Electron Microscopy (SEM). It was found that 0.2429 mg/mL of tannic acid was obtained under the extraction conditions of extraction temperature of 40℃, sonication time of 20 minutes and duty cycle of 50%. From SEM analysis, it was found that the raw sample demonstrated rough surface and no porous but kenaf bast fibre display smoother surface with less impurities and few pores appeared after the extraction process using UAE. These results indicate that ultrasound-assisted extraction is an efficient method for extracting tannic acid from kenaf bast fibre with the advantages of lower extraction time and higher extraction yield.https://journals.pan.pl/Content/124059/PDF/AMM-2022-3-34-Mohamad.pdfultrasonic assisted extraction (uae)sonication timeduty cycleextraction processkenaf bast fibre |
| spellingShingle | M. Mohamad H.A. Ibrahim M.F.M. Nasir N.A. Mohidem N.F. Shoparwe P.T. Teo M.N. Masri A.R. Irfan Extraction of Tannic Acid from Kenaf Bast Fibre using Ultrasonic Assisted Extraction Archives of Metallurgy and Materials ultrasonic assisted extraction (uae) sonication time duty cycle extraction process kenaf bast fibre |
| title | Extraction of Tannic Acid from Kenaf Bast Fibre using Ultrasonic Assisted Extraction |
| title_full | Extraction of Tannic Acid from Kenaf Bast Fibre using Ultrasonic Assisted Extraction |
| title_fullStr | Extraction of Tannic Acid from Kenaf Bast Fibre using Ultrasonic Assisted Extraction |
| title_full_unstemmed | Extraction of Tannic Acid from Kenaf Bast Fibre using Ultrasonic Assisted Extraction |
| title_short | Extraction of Tannic Acid from Kenaf Bast Fibre using Ultrasonic Assisted Extraction |
| title_sort | extraction of tannic acid from kenaf bast fibre using ultrasonic assisted extraction |
| topic | ultrasonic assisted extraction (uae) sonication time duty cycle extraction process kenaf bast fibre |
| url | https://journals.pan.pl/Content/124059/PDF/AMM-2022-3-34-Mohamad.pdf |
| work_keys_str_mv | AT mmohamad extractionoftannicacidfromkenafbastfibreusingultrasonicassistedextraction AT haibrahim extractionoftannicacidfromkenafbastfibreusingultrasonicassistedextraction AT mfmnasir extractionoftannicacidfromkenafbastfibreusingultrasonicassistedextraction AT namohidem extractionoftannicacidfromkenafbastfibreusingultrasonicassistedextraction AT nfshoparwe extractionoftannicacidfromkenafbastfibreusingultrasonicassistedextraction AT ptteo extractionoftannicacidfromkenafbastfibreusingultrasonicassistedextraction AT mnmasri extractionoftannicacidfromkenafbastfibreusingultrasonicassistedextraction AT arirfan extractionoftannicacidfromkenafbastfibreusingultrasonicassistedextraction |