Assessment of Cementitious Ceramic Tile Adhesives in the Light of Repeatability and Reproducibility of the Tensile Adhesion Strength Measurements

The paper presents the results of tensile adhesion strength measurements of ceramic tile adhesive (CTA) stored in various conditions performed by ten operators in one laboratory using the same equipment and auxiliary materials. The obtained results allowed the authors to estimate the repeatability a...

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Main Authors: Jacek Michalak, Radosław Ziomek
Format: Article
Language:English
Published: MDPI AG 2023-06-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/16/12/4245
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author Jacek Michalak
Radosław Ziomek
author_facet Jacek Michalak
Radosław Ziomek
author_sort Jacek Michalak
collection DOAJ
description The paper presents the results of tensile adhesion strength measurements of ceramic tile adhesive (CTA) stored in various conditions performed by ten operators in one laboratory using the same equipment and auxiliary materials. The obtained results allowed the authors to estimate the repeatability and reproducibility of the tensile adhesion strength measurement method using the methodology following ISO 5725-2:1994+AC1:2002. Standard deviations of repeatability ranging from 0.09 to 0.15 for the general means value in the range of 0.89–1.76 MPa and standard deviations of reproducibility ranging from 0.14 to 0.21 for the same general means content indicate that the accuracy of tensile adhesion strength measurement method is not high enough. From the group of ten operators, five perform tensile adhesion strength measurements daily, the remaining five perform other measures, and the results obtained by professionals and non-professionals showed no significant differences. In light of the obtained results, compliance assessment with this method with the criteria set out in the harmonized standard EN 12004:2007+A1:2012 carried out by different operators may be divergent, and there is a significant risk of incorrect assessments. This risk is additionally increasing in the case of the evaluation conducted by market surveillance authorities, which use the simple acceptance rule that does not consider measurement variability.
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spelling doaj.art-12605b6b673c433283ae925bbd046e112023-11-18T11:23:33ZengMDPI AGMaterials1996-19442023-06-011612424510.3390/ma16124245Assessment of Cementitious Ceramic Tile Adhesives in the Light of Repeatability and Reproducibility of the Tensile Adhesion Strength MeasurementsJacek Michalak0Radosław Ziomek1Research and Development Center, Atlas sp. z o.o., 2 Kilińskiego St., 91-421 Lodz, PolandResearch and Development Center, Atlas sp. z o.o., 2 Kilińskiego St., 91-421 Lodz, PolandThe paper presents the results of tensile adhesion strength measurements of ceramic tile adhesive (CTA) stored in various conditions performed by ten operators in one laboratory using the same equipment and auxiliary materials. The obtained results allowed the authors to estimate the repeatability and reproducibility of the tensile adhesion strength measurement method using the methodology following ISO 5725-2:1994+AC1:2002. Standard deviations of repeatability ranging from 0.09 to 0.15 for the general means value in the range of 0.89–1.76 MPa and standard deviations of reproducibility ranging from 0.14 to 0.21 for the same general means content indicate that the accuracy of tensile adhesion strength measurement method is not high enough. From the group of ten operators, five perform tensile adhesion strength measurements daily, the remaining five perform other measures, and the results obtained by professionals and non-professionals showed no significant differences. In light of the obtained results, compliance assessment with this method with the criteria set out in the harmonized standard EN 12004:2007+A1:2012 carried out by different operators may be divergent, and there is a significant risk of incorrect assessments. This risk is additionally increasing in the case of the evaluation conducted by market surveillance authorities, which use the simple acceptance rule that does not consider measurement variability.https://www.mdpi.com/1996-1944/16/12/4245tensile adhesion strengthceramic tile adhesive (CTA)assessment and verification of constancy of performance (AVCP)construction productsrepeatabilityreproducibility
spellingShingle Jacek Michalak
Radosław Ziomek
Assessment of Cementitious Ceramic Tile Adhesives in the Light of Repeatability and Reproducibility of the Tensile Adhesion Strength Measurements
Materials
tensile adhesion strength
ceramic tile adhesive (CTA)
assessment and verification of constancy of performance (AVCP)
construction products
repeatability
reproducibility
title Assessment of Cementitious Ceramic Tile Adhesives in the Light of Repeatability and Reproducibility of the Tensile Adhesion Strength Measurements
title_full Assessment of Cementitious Ceramic Tile Adhesives in the Light of Repeatability and Reproducibility of the Tensile Adhesion Strength Measurements
title_fullStr Assessment of Cementitious Ceramic Tile Adhesives in the Light of Repeatability and Reproducibility of the Tensile Adhesion Strength Measurements
title_full_unstemmed Assessment of Cementitious Ceramic Tile Adhesives in the Light of Repeatability and Reproducibility of the Tensile Adhesion Strength Measurements
title_short Assessment of Cementitious Ceramic Tile Adhesives in the Light of Repeatability and Reproducibility of the Tensile Adhesion Strength Measurements
title_sort assessment of cementitious ceramic tile adhesives in the light of repeatability and reproducibility of the tensile adhesion strength measurements
topic tensile adhesion strength
ceramic tile adhesive (CTA)
assessment and verification of constancy of performance (AVCP)
construction products
repeatability
reproducibility
url https://www.mdpi.com/1996-1944/16/12/4245
work_keys_str_mv AT jacekmichalak assessmentofcementitiousceramictileadhesivesinthelightofrepeatabilityandreproducibilityofthetensileadhesionstrengthmeasurements
AT radosławziomek assessmentofcementitiousceramictileadhesivesinthelightofrepeatabilityandreproducibilityofthetensileadhesionstrengthmeasurements