Effect of Plastic Deformation on the Structure and Mechanical Properties of the Zn-4Ag-1Cu Zinc Alloy

It is known that zinc biodegradable alloys are a promising material for producing biomedical implants for orthopedics and vascular stents. Among them, the Zn-Ag-Cu zinc alloy is of special interest due to the antibacterial and antimicrobial properties of Ag and Cu. To improve the mechanical properti...

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Main Authors: Elvira Khafizova, Elvira Fakhretdinova, Rinat Islamgaliev, Milena Polenok, Vil Sitdikov, Hakan Yilmazer
Format: Article
Language:English
Published: MDPI AG 2023-06-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/16/13/4646
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author Elvira Khafizova
Elvira Fakhretdinova
Rinat Islamgaliev
Milena Polenok
Vil Sitdikov
Hakan Yilmazer
author_facet Elvira Khafizova
Elvira Fakhretdinova
Rinat Islamgaliev
Milena Polenok
Vil Sitdikov
Hakan Yilmazer
author_sort Elvira Khafizova
collection DOAJ
description It is known that zinc biodegradable alloys are a promising material for producing biomedical implants for orthopedics and vascular stents. Among them, the Zn-Ag-Cu zinc alloy is of special interest due to the antibacterial and antimicrobial properties of Ag and Cu. To improve the mechanical properties of the Zn-4Ag-1Cu zinc alloy, the effect of equal-channel angular pressing (ECAP) on the microstructure and strength has been investigated. The ECAP conditions for the Zn-4Ag-1Cu alloy were chosen by modeling in the Deform 3 D program (temperature and strain rate). The microstructure was analyzed using transmission electron microscopy, scanning electron microscopy and X-ray diffraction analysis. The study of strength was carried out by measuring the microhardness and tensile tests of small samples with a gauge dimension of 0.8 × 1 × 4 mm<sup>3</sup>. The microstructure after ECAP was characterized by equiaxed grains ranging in a size from 1.5 µm to 4 µm with particles in a size from 200 nm to 1 µm uniformly distributed along the boundaries. The ECAP samples showed a high strength of 348 MPa and good ductility of up to 30%, demonstrating their great potential as promising materials for producing medical stents.
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spelling doaj.art-132c9fee27124e8f8bf73623f91b58e02023-11-18T16:57:48ZengMDPI AGMaterials1996-19442023-06-011613464610.3390/ma16134646Effect of Plastic Deformation on the Structure and Mechanical Properties of the Zn-4Ag-1Cu Zinc AlloyElvira Khafizova0Elvira Fakhretdinova1Rinat Islamgaliev2Milena Polenok3Vil Sitdikov4Hakan Yilmazer5Institute of Physics of Advanced Materials, Ufa University of Science and Technology, 450076 Ufa, RussiaInstitute of Molecules and Crystal Physics, Ufa Federal Research Center of the Russian Academy of Sciences, 450075 Ufa, RussiaInstitute of Physics of Advanced Materials, Ufa University of Science and Technology, 450076 Ufa, RussiaInstitute of Physics of Advanced Materials, Ufa University of Science and Technology, 450076 Ufa, RussiaLLC “RN-BashNIPIneft”, Lenina Street 86/1, 450076 Ufa, RussiaDepartment of Metallurgical and Materials Engineering, Yildiz Technical University, Esenler 34220, Istanbul, TurkeyIt is known that zinc biodegradable alloys are a promising material for producing biomedical implants for orthopedics and vascular stents. Among them, the Zn-Ag-Cu zinc alloy is of special interest due to the antibacterial and antimicrobial properties of Ag and Cu. To improve the mechanical properties of the Zn-4Ag-1Cu zinc alloy, the effect of equal-channel angular pressing (ECAP) on the microstructure and strength has been investigated. The ECAP conditions for the Zn-4Ag-1Cu alloy were chosen by modeling in the Deform 3 D program (temperature and strain rate). The microstructure was analyzed using transmission electron microscopy, scanning electron microscopy and X-ray diffraction analysis. The study of strength was carried out by measuring the microhardness and tensile tests of small samples with a gauge dimension of 0.8 × 1 × 4 mm<sup>3</sup>. The microstructure after ECAP was characterized by equiaxed grains ranging in a size from 1.5 µm to 4 µm with particles in a size from 200 nm to 1 µm uniformly distributed along the boundaries. The ECAP samples showed a high strength of 348 MPa and good ductility of up to 30%, demonstrating their great potential as promising materials for producing medical stents.https://www.mdpi.com/1996-1944/16/13/4646biodegradable metalsZn-based alloysmechanical propertiesmicrostructuresequal-channel angular pressingcomputer simulation
spellingShingle Elvira Khafizova
Elvira Fakhretdinova
Rinat Islamgaliev
Milena Polenok
Vil Sitdikov
Hakan Yilmazer
Effect of Plastic Deformation on the Structure and Mechanical Properties of the Zn-4Ag-1Cu Zinc Alloy
Materials
biodegradable metals
Zn-based alloys
mechanical properties
microstructures
equal-channel angular pressing
computer simulation
title Effect of Plastic Deformation on the Structure and Mechanical Properties of the Zn-4Ag-1Cu Zinc Alloy
title_full Effect of Plastic Deformation on the Structure and Mechanical Properties of the Zn-4Ag-1Cu Zinc Alloy
title_fullStr Effect of Plastic Deformation on the Structure and Mechanical Properties of the Zn-4Ag-1Cu Zinc Alloy
title_full_unstemmed Effect of Plastic Deformation on the Structure and Mechanical Properties of the Zn-4Ag-1Cu Zinc Alloy
title_short Effect of Plastic Deformation on the Structure and Mechanical Properties of the Zn-4Ag-1Cu Zinc Alloy
title_sort effect of plastic deformation on the structure and mechanical properties of the zn 4ag 1cu zinc alloy
topic biodegradable metals
Zn-based alloys
mechanical properties
microstructures
equal-channel angular pressing
computer simulation
url https://www.mdpi.com/1996-1944/16/13/4646
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