Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental Design
Mn-Al alloys are important alloys due to their magnetic properties and have been identified as permanent magnets. This alloy possesses magnetic properties and can be manufactured at a relatively low cost. Mn-Al alloys could be an alternative to rare earth magnets and hard ferrites and have a promisi...
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Format: | Article |
Language: | English |
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Polish Academy of Sciences
2023-12-01
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Series: | Archives of Metallurgy and Materials |
Subjects: | |
Online Access: | https://journals.pan.pl/Content/129640/PDF/AMM-2023-4-16-Goller.pdf |
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author | Can Burak Danisman Gultekin Goller |
author_facet | Can Burak Danisman Gultekin Goller |
author_sort | Can Burak Danisman |
collection | DOAJ |
description | Mn-Al alloys are important alloys due to their magnetic properties and have been identified as permanent magnets. This alloy possesses magnetic properties and can be manufactured at a relatively low cost. Mn-Al alloys could be an alternative to rare earth magnets and hard ferrites and have a promising future. In this study, the effects of sintering temperature, holding time and pressure on densification, average grain size and magnetic properties of the SPS-ed Mn-Al alloys were observed. However, with the different sintering parameters, the magnetic phase τ phase could be achieved. To obtain the τ phase, different annealing methods were tried, yet samples heated to 650°C and air cooled exhibited magnetic properties. This sample was selected from various sintering parameters due to its high density of 99% N6 (800°C – 300 sec – 60 MPa) and has an average grain size of 137±18.1 µm. The uniqueness of this work is that statistical approaches such as Taguchi design of experiment (DOE) and regression were used for optimization of the manufacturing process. |
first_indexed | 2024-03-08T20:29:37Z |
format | Article |
id | doaj.art-13f9a878a21542f2ae0be5c8c0acc3a1 |
institution | Directory Open Access Journal |
issn | 2300-1909 |
language | English |
last_indexed | 2024-03-08T20:29:37Z |
publishDate | 2023-12-01 |
publisher | Polish Academy of Sciences |
record_format | Article |
series | Archives of Metallurgy and Materials |
spelling | doaj.art-13f9a878a21542f2ae0be5c8c0acc3a12023-12-22T14:27:45ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092023-12-01vol. 68No 413571367https://doi.org/10.24425/amm.2023.146201Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental DesignCan Burak Danisman0https://orcid.org/0009-0008-6692-2928Gultekin Goller1https://orcid.org/0000-0003-4680-3936Istanbul Technical University, Department of Metallurgical and Materials Engineering, Istanbul, 34469, TurkeyIstanbul Technical University, Department of Metallurgical and Materials Engineering, Istanbul, 34469, TurkeyMn-Al alloys are important alloys due to their magnetic properties and have been identified as permanent magnets. This alloy possesses magnetic properties and can be manufactured at a relatively low cost. Mn-Al alloys could be an alternative to rare earth magnets and hard ferrites and have a promising future. In this study, the effects of sintering temperature, holding time and pressure on densification, average grain size and magnetic properties of the SPS-ed Mn-Al alloys were observed. However, with the different sintering parameters, the magnetic phase τ phase could be achieved. To obtain the τ phase, different annealing methods were tried, yet samples heated to 650°C and air cooled exhibited magnetic properties. This sample was selected from various sintering parameters due to its high density of 99% N6 (800°C – 300 sec – 60 MPa) and has an average grain size of 137±18.1 µm. The uniqueness of this work is that statistical approaches such as Taguchi design of experiment (DOE) and regression were used for optimization of the manufacturing process.https://journals.pan.pl/Content/129640/PDF/AMM-2023-4-16-Goller.pdfmn-al magnetsspsτ phasedoe |
spellingShingle | Can Burak Danisman Gultekin Goller Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental Design Archives of Metallurgy and Materials mn-al magnets sps τ phase doe |
title | Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental Design |
title_full | Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental Design |
title_fullStr | Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental Design |
title_full_unstemmed | Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental Design |
title_short | Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental Design |
title_sort | spark plasma sintered mn al magnets production and characterization with experimental design |
topic | mn-al magnets sps τ phase doe |
url | https://journals.pan.pl/Content/129640/PDF/AMM-2023-4-16-Goller.pdf |
work_keys_str_mv | AT canburakdanisman sparkplasmasinteredmnalmagnetsproductionandcharacterizationwithexperimentaldesign AT gultekingoller sparkplasmasinteredmnalmagnetsproductionandcharacterizationwithexperimentaldesign |