Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental Design

Mn-Al alloys are important alloys due to their magnetic properties and have been identified as permanent magnets. This alloy possesses magnetic properties and can be manufactured at a relatively low cost. Mn-Al alloys could be an alternative to rare earth magnets and hard ferrites and have a promisi...

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Main Authors: Can Burak Danisman, Gultekin Goller
Format: Article
Language:English
Published: Polish Academy of Sciences 2023-12-01
Series:Archives of Metallurgy and Materials
Subjects:
Online Access:https://journals.pan.pl/Content/129640/PDF/AMM-2023-4-16-Goller.pdf
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author Can Burak Danisman
Gultekin Goller
author_facet Can Burak Danisman
Gultekin Goller
author_sort Can Burak Danisman
collection DOAJ
description Mn-Al alloys are important alloys due to their magnetic properties and have been identified as permanent magnets. This alloy possesses magnetic properties and can be manufactured at a relatively low cost. Mn-Al alloys could be an alternative to rare earth magnets and hard ferrites and have a promising future. In this study, the effects of sintering temperature, holding time and pressure on densification, average grain size and magnetic properties of the SPS-ed Mn-Al alloys were observed. However, with the different sintering parameters, the magnetic phase τ phase could be achieved. To obtain the τ phase, different annealing methods were tried, yet samples heated to 650°C and air cooled exhibited magnetic properties. This sample was selected from various sintering parameters due to its high density of 99% N6 (800°C – 300 sec – 60 MPa) and has an average grain size of 137±18.1 µm. The uniqueness of this work is that statistical approaches such as Taguchi design of experiment (DOE) and regression were used for optimization of the manufacturing process.
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spelling doaj.art-13f9a878a21542f2ae0be5c8c0acc3a12023-12-22T14:27:45ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092023-12-01vol. 68No 413571367https://doi.org/10.24425/amm.2023.146201Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental DesignCan Burak Danisman0https://orcid.org/0009-0008-6692-2928Gultekin Goller1https://orcid.org/0000-0003-4680-3936Istanbul Technical University, Department of Metallurgical and Materials Engineering, Istanbul, 34469, TurkeyIstanbul Technical University, Department of Metallurgical and Materials Engineering, Istanbul, 34469, TurkeyMn-Al alloys are important alloys due to their magnetic properties and have been identified as permanent magnets. This alloy possesses magnetic properties and can be manufactured at a relatively low cost. Mn-Al alloys could be an alternative to rare earth magnets and hard ferrites and have a promising future. In this study, the effects of sintering temperature, holding time and pressure on densification, average grain size and magnetic properties of the SPS-ed Mn-Al alloys were observed. However, with the different sintering parameters, the magnetic phase τ phase could be achieved. To obtain the τ phase, different annealing methods were tried, yet samples heated to 650°C and air cooled exhibited magnetic properties. This sample was selected from various sintering parameters due to its high density of 99% N6 (800°C – 300 sec – 60 MPa) and has an average grain size of 137±18.1 µm. The uniqueness of this work is that statistical approaches such as Taguchi design of experiment (DOE) and regression were used for optimization of the manufacturing process.https://journals.pan.pl/Content/129640/PDF/AMM-2023-4-16-Goller.pdfmn-al magnetsspsτ phasedoe
spellingShingle Can Burak Danisman
Gultekin Goller
Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental Design
Archives of Metallurgy and Materials
mn-al magnets
sps
τ phase
doe
title Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental Design
title_full Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental Design
title_fullStr Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental Design
title_full_unstemmed Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental Design
title_short Spark Plasma Sintered Mn-Al (Magnets) Production and Characterization with Experimental Design
title_sort spark plasma sintered mn al magnets production and characterization with experimental design
topic mn-al magnets
sps
τ phase
doe
url https://journals.pan.pl/Content/129640/PDF/AMM-2023-4-16-Goller.pdf
work_keys_str_mv AT canburakdanisman sparkplasmasinteredmnalmagnetsproductionandcharacterizationwithexperimentaldesign
AT gultekingoller sparkplasmasinteredmnalmagnetsproductionandcharacterizationwithexperimentaldesign