An Efficient Synthesis of 1,8-Dioxo-Octahydroxanthenes Derivatives Using Heterogeneous Ce-ZSM-11 Zeolite Catalyst

The Ce-ZSM-11 zeolite has been used as an efficient catalyst for the one pot synthesis of 1,8-dioxo-octahydroxanthene derivatives from aromatic aldehyde and 5,5-dimethyl-cyclohexane-1,3-dione under reflux condition. The catalyst was characterized by Powder X-ray diffraction (XRD), Scanning Electron...

Full description

Bibliographic Details
Main Authors: Rameshwar R. Magar, Ganesh T. Pawar, Sachin P. Gadekar, Machhindra Karbhari Lande
Format: Article
Language:English
Published: Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS) 2018-12-01
Series:Bulletin of Chemical Reaction Engineering & Catalysis
Subjects:
Online Access:https://journal.bcrec.id/index.php/bcrec/article/view/2062
_version_ 1811153887247204352
author Rameshwar R. Magar
Ganesh T. Pawar
Sachin P. Gadekar
Machhindra Karbhari Lande
author_facet Rameshwar R. Magar
Ganesh T. Pawar
Sachin P. Gadekar
Machhindra Karbhari Lande
author_sort Rameshwar R. Magar
collection DOAJ
description The Ce-ZSM-11 zeolite has been used as an efficient catalyst for the one pot synthesis of 1,8-dioxo-octahydroxanthene derivatives from aromatic aldehyde and 5,5-dimethyl-cyclohexane-1,3-dione under reflux condition. The catalyst was characterized by Powder X-ray diffraction (XRD), Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDS), Fourier Transform Infrared Spectroscopy (FTIR), Brunauer-Emmer-Teller (BET) surface area analysis, and Temperature Programmed Desorption (TPD) techniques. This method provides several advantageous such as use of inexpensive catalyst, simple work-up procedure, high yield of desired product and reusability of catalyst.
first_indexed 2024-03-11T22:50:23Z
format Article
id doaj.art-144d91ab9ad641c4a356259084a4dc9c
institution Directory Open Access Journal
issn 1978-2993
language English
last_indexed 2024-03-11T22:50:23Z
publishDate 2018-12-01
publisher Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)
record_format Article
series Bulletin of Chemical Reaction Engineering & Catalysis
spelling doaj.art-144d91ab9ad641c4a356259084a4dc9c2023-09-22T03:45:31ZengMasyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)Bulletin of Chemical Reaction Engineering & Catalysis1978-29932018-12-0113343644610.9767/bcrec.13.3.2062.436-4461440An Efficient Synthesis of 1,8-Dioxo-Octahydroxanthenes Derivatives Using Heterogeneous Ce-ZSM-11 Zeolite CatalystRameshwar R. Magar0Ganesh T. Pawar1Sachin P. Gadekar2Machhindra Karbhari Lande3Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad (M.S.), 431004, IndiaDepartment of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad (M.S.), 431004, IndiaDepartment of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad (M.S.), 431004, IndiaDepartment of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad (M.S.), 431004, IndiaThe Ce-ZSM-11 zeolite has been used as an efficient catalyst for the one pot synthesis of 1,8-dioxo-octahydroxanthene derivatives from aromatic aldehyde and 5,5-dimethyl-cyclohexane-1,3-dione under reflux condition. The catalyst was characterized by Powder X-ray diffraction (XRD), Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDS), Fourier Transform Infrared Spectroscopy (FTIR), Brunauer-Emmer-Teller (BET) surface area analysis, and Temperature Programmed Desorption (TPD) techniques. This method provides several advantageous such as use of inexpensive catalyst, simple work-up procedure, high yield of desired product and reusability of catalyst.https://journal.bcrec.id/index.php/bcrec/article/view/2062ce-zsm-11 zeolite1,8-dioxo-octahydroxanthenearomatic aldehyde5,5-dimethyl-cyclohexane-1,3-dione
spellingShingle Rameshwar R. Magar
Ganesh T. Pawar
Sachin P. Gadekar
Machhindra Karbhari Lande
An Efficient Synthesis of 1,8-Dioxo-Octahydroxanthenes Derivatives Using Heterogeneous Ce-ZSM-11 Zeolite Catalyst
Bulletin of Chemical Reaction Engineering & Catalysis
ce-zsm-11 zeolite
1,8-dioxo-octahydroxanthene
aromatic aldehyde
5,5-dimethyl-cyclohexane-1,3-dione
title An Efficient Synthesis of 1,8-Dioxo-Octahydroxanthenes Derivatives Using Heterogeneous Ce-ZSM-11 Zeolite Catalyst
title_full An Efficient Synthesis of 1,8-Dioxo-Octahydroxanthenes Derivatives Using Heterogeneous Ce-ZSM-11 Zeolite Catalyst
title_fullStr An Efficient Synthesis of 1,8-Dioxo-Octahydroxanthenes Derivatives Using Heterogeneous Ce-ZSM-11 Zeolite Catalyst
title_full_unstemmed An Efficient Synthesis of 1,8-Dioxo-Octahydroxanthenes Derivatives Using Heterogeneous Ce-ZSM-11 Zeolite Catalyst
title_short An Efficient Synthesis of 1,8-Dioxo-Octahydroxanthenes Derivatives Using Heterogeneous Ce-ZSM-11 Zeolite Catalyst
title_sort efficient synthesis of 1 8 dioxo octahydroxanthenes derivatives using heterogeneous ce zsm 11 zeolite catalyst
topic ce-zsm-11 zeolite
1,8-dioxo-octahydroxanthene
aromatic aldehyde
5,5-dimethyl-cyclohexane-1,3-dione
url https://journal.bcrec.id/index.php/bcrec/article/view/2062
work_keys_str_mv AT rameshwarrmagar anefficientsynthesisof18dioxooctahydroxanthenesderivativesusingheterogeneouscezsm11zeolitecatalyst
AT ganeshtpawar anefficientsynthesisof18dioxooctahydroxanthenesderivativesusingheterogeneouscezsm11zeolitecatalyst
AT sachinpgadekar anefficientsynthesisof18dioxooctahydroxanthenesderivativesusingheterogeneouscezsm11zeolitecatalyst
AT machhindrakarbharilande anefficientsynthesisof18dioxooctahydroxanthenesderivativesusingheterogeneouscezsm11zeolitecatalyst
AT rameshwarrmagar efficientsynthesisof18dioxooctahydroxanthenesderivativesusingheterogeneouscezsm11zeolitecatalyst
AT ganeshtpawar efficientsynthesisof18dioxooctahydroxanthenesderivativesusingheterogeneouscezsm11zeolitecatalyst
AT sachinpgadekar efficientsynthesisof18dioxooctahydroxanthenesderivativesusingheterogeneouscezsm11zeolitecatalyst
AT machhindrakarbharilande efficientsynthesisof18dioxooctahydroxanthenesderivativesusingheterogeneouscezsm11zeolitecatalyst