Magnetic and electrical properties of Cr substituted Ni nano ferrites

Nano-ferrites with composition NiCrxFe2-xO4 (where x = 0.1, 0.3, 0.5, 0.7, 0.9, 1.0) were synthesized through citrate-gel auto combustion technique at moderately low temperature. X-ray analysis shows cubic spinel structure single phase without any impurity peak and average crystallite size in the ra...

Full description

Bibliographic Details
Main Authors: Katrapally Vijaya Kumar, Rapolu Sridhar, Dachepalli Ravinder
Format: Article
Language:English
Published: University of Novi Sad 2018-03-01
Series:Processing and Application of Ceramics
Subjects:
Online Access:http://www.tf.uns.ac.rs/publikacije/PAC/pdf/PAC%2039%2001.pdf
_version_ 1818535103111888896
author Katrapally Vijaya Kumar
Rapolu Sridhar
Dachepalli Ravinder
author_facet Katrapally Vijaya Kumar
Rapolu Sridhar
Dachepalli Ravinder
author_sort Katrapally Vijaya Kumar
collection DOAJ
description Nano-ferrites with composition NiCrxFe2-xO4 (where x = 0.1, 0.3, 0.5, 0.7, 0.9, 1.0) were synthesized through citrate-gel auto combustion technique at moderately low temperature. X-ray analysis shows cubic spinel structure single phase without any impurity peak and average crystallite size in the range 8.5–10.5 nm. Magnetic properties were measured using a vibrating sample magnetometer at room temperature in the applied field of ±6 KOe. The obtained M-H loop area is very narrow, hence the synthesized nano ferrites are soft magnetic materials with small coercivity. Magnetic parameters such as saturation magnetization (Ms), coercivity (Hc), remanent magnetization (Mr) and residual magnetization were measured and discussed with regard to Cr3+ ion concentration. Electrical properties were measured using two probe method from room temperature to well beyond transition temperature. The DC resistivity variation with temperature shows the semiconductor nature. Resistivity, drift mobility and activation energy values are measured and discussed with regard to composition. The Curie temperature was determined using DC resistivity data and Loria-Sinha method. The observed results can be explained in detail on the basis of composition.
first_indexed 2024-12-11T18:20:22Z
format Article
id doaj.art-146be54baac74edbaaf7486525cbbe1b
institution Directory Open Access Journal
issn 1820-6131
2406-1034
language English
last_indexed 2024-12-11T18:20:22Z
publishDate 2018-03-01
publisher University of Novi Sad
record_format Article
series Processing and Application of Ceramics
spelling doaj.art-146be54baac74edbaaf7486525cbbe1b2022-12-22T00:55:16ZengUniversity of Novi SadProcessing and Application of Ceramics1820-61312406-10342018-03-011211710.2298/PAC1801001VMagnetic and electrical properties of Cr substituted Ni nano ferritesKatrapally Vijaya Kumar0Rapolu Sridhar1Dachepalli Ravinder2Department of Physics, JNTUH College of Engineering Sultanpur, Sultanpur (V), Pulkal (M), Sangareddy-Dist. 502293 Telangana State, IndiaDepartment of BS&H, Vignan Institute of Technology & Science, Yadadri-Bhuvanagiri-Dist.508284, Telangana State, IndiaDepartment of Physics, Osmania University, Hyderabad-500007, Telangana State, IndiaNano-ferrites with composition NiCrxFe2-xO4 (where x = 0.1, 0.3, 0.5, 0.7, 0.9, 1.0) were synthesized through citrate-gel auto combustion technique at moderately low temperature. X-ray analysis shows cubic spinel structure single phase without any impurity peak and average crystallite size in the range 8.5–10.5 nm. Magnetic properties were measured using a vibrating sample magnetometer at room temperature in the applied field of ±6 KOe. The obtained M-H loop area is very narrow, hence the synthesized nano ferrites are soft magnetic materials with small coercivity. Magnetic parameters such as saturation magnetization (Ms), coercivity (Hc), remanent magnetization (Mr) and residual magnetization were measured and discussed with regard to Cr3+ ion concentration. Electrical properties were measured using two probe method from room temperature to well beyond transition temperature. The DC resistivity variation with temperature shows the semiconductor nature. Resistivity, drift mobility and activation energy values are measured and discussed with regard to composition. The Curie temperature was determined using DC resistivity data and Loria-Sinha method. The observed results can be explained in detail on the basis of composition.http://www.tf.uns.ac.rs/publikacije/PAC/pdf/PAC%2039%2001.pdfNi-Cr ferritescitrate-gel methodXRDmagnetic propertieselectrical properties
spellingShingle Katrapally Vijaya Kumar
Rapolu Sridhar
Dachepalli Ravinder
Magnetic and electrical properties of Cr substituted Ni nano ferrites
Processing and Application of Ceramics
Ni-Cr ferrites
citrate-gel method
XRD
magnetic properties
electrical properties
title Magnetic and electrical properties of Cr substituted Ni nano ferrites
title_full Magnetic and electrical properties of Cr substituted Ni nano ferrites
title_fullStr Magnetic and electrical properties of Cr substituted Ni nano ferrites
title_full_unstemmed Magnetic and electrical properties of Cr substituted Ni nano ferrites
title_short Magnetic and electrical properties of Cr substituted Ni nano ferrites
title_sort magnetic and electrical properties of cr substituted ni nano ferrites
topic Ni-Cr ferrites
citrate-gel method
XRD
magnetic properties
electrical properties
url http://www.tf.uns.ac.rs/publikacije/PAC/pdf/PAC%2039%2001.pdf
work_keys_str_mv AT katrapallyvijayakumar magneticandelectricalpropertiesofcrsubstitutedninanoferrites
AT rapolusridhar magneticandelectricalpropertiesofcrsubstitutedninanoferrites
AT dachepalliravinder magneticandelectricalpropertiesofcrsubstitutedninanoferrites