Synthesis of carbon nanostructures by the pyrolysis of wood sawdust in a tubular reactor

Carbon nanostructures were produced by wood sawdust pyrolysis. The results obtained revealed that the thermodynamic simulations (FactSage) were successful to predict the best reaction conditions for the synthesis of carbon, and potentially carbon fibers and nanotubes production. Graphite formation w...

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Bibliographic Details
Main Authors: Maria G. Sebag Bernd, Saulo R. Bragança, Nestor Heck, Luiz C.P. da Silva Filho
Format: Article
Language:English
Published: Elsevier 2017-04-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S223878541630093X
Description
Summary:Carbon nanostructures were produced by wood sawdust pyrolysis. The results obtained revealed that the thermodynamic simulations (FactSage) were successful to predict the best reaction conditions for the synthesis of carbon, and potentially carbon fibers and nanotubes production. Graphite formation was indicated by XRD study, and by thermal analysis which presented the carbon oxidation range. The morphology of the samples (SEM/TEM analysis) showed carbon nanotubes/nanofibers varying in size and thickness, with defects and flaws. The tubular reactor was considered to be an economic and environmental correct way to nanomaterials growing, with the simultaneous generation of hydrogen and lower pollutant gas emissions.
ISSN:2238-7854