Effects of Chemical Curing Temperature and Time on the Properties of Liquefied Wood based As-cured Precursors and Carbon Fibers

Liquefied wood based as-cured precursors and carbon fibers prepared by different chemical curing processes were carried out to investigate the effects of curing temperature and time on the thermostability and microstructure of liquefied wood based precursors, the tensile strength of carbon fibers as...

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Main Authors: Junbo Shang, Jian Lin, Guangjie Zhao, Jianhui Zhang, Zimu Su, Sicen Guo
Format: Article
Language:English
Published: North Carolina State University 2015-09-01
Series:BioResources
Subjects:
Online Access:http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_10_4_7477_Shang_Chemical_Curing_Temperature_Precursors
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author Junbo Shang
Jian Lin
Guangjie Zhao
Jianhui Zhang
Zimu Su
Sicen Guo
author_facet Junbo Shang
Jian Lin
Guangjie Zhao
Jianhui Zhang
Zimu Su
Sicen Guo
author_sort Junbo Shang
collection DOAJ
description Liquefied wood based as-cured precursors and carbon fibers prepared by different chemical curing processes were carried out to investigate the effects of curing temperature and time on the thermostability and microstructure of liquefied wood based precursors, the tensile strength of carbon fibers as well. The primary fibers can be converted into precursors with high performance by directly heating at target curing temperature. With the temperature and duration increasing, the numbers of methylene bonds in precursors increased, resulting in the enhancement of cross-linkages among molecular chains and then the improvement of thermostability of precursors. Carbon fibers prepared from as-cured precursors (curing temperature 95 oC, curing time 3h) had the minimum value of the average interlayer spacing (d002), it also showed the highest tensile strength, almost 800 MPa, which can be classified as fibers of general grade.
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spelling doaj.art-14ee6086b40d4df8962e2c73aace702c2022-12-21T23:55:11ZengNorth Carolina State UniversityBioResources1930-21261930-21262015-09-011047477748810.15376/biores.10.4.7477-7488Effects of Chemical Curing Temperature and Time on the Properties of Liquefied Wood based As-cured Precursors and Carbon FibersJunbo Shang0Jian LinGuangjie ZhaoJianhui ZhangZimu SuSicen GuoBeijing Forestry University; China Liquefied wood based as-cured precursors and carbon fibers prepared by different chemical curing processes were carried out to investigate the effects of curing temperature and time on the thermostability and microstructure of liquefied wood based precursors, the tensile strength of carbon fibers as well. The primary fibers can be converted into precursors with high performance by directly heating at target curing temperature. With the temperature and duration increasing, the numbers of methylene bonds in precursors increased, resulting in the enhancement of cross-linkages among molecular chains and then the improvement of thermostability of precursors. Carbon fibers prepared from as-cured precursors (curing temperature 95 oC, curing time 3h) had the minimum value of the average interlayer spacing (d002), it also showed the highest tensile strength, almost 800 MPa, which can be classified as fibers of general grade.http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_10_4_7477_Shang_Chemical_Curing_Temperature_PrecursorsChemical curingCarbon fibersTensile strengthAs-cured Precursor
spellingShingle Junbo Shang
Jian Lin
Guangjie Zhao
Jianhui Zhang
Zimu Su
Sicen Guo
Effects of Chemical Curing Temperature and Time on the Properties of Liquefied Wood based As-cured Precursors and Carbon Fibers
BioResources
Chemical curing
Carbon fibers
Tensile strength
As-cured Precursor
title Effects of Chemical Curing Temperature and Time on the Properties of Liquefied Wood based As-cured Precursors and Carbon Fibers
title_full Effects of Chemical Curing Temperature and Time on the Properties of Liquefied Wood based As-cured Precursors and Carbon Fibers
title_fullStr Effects of Chemical Curing Temperature and Time on the Properties of Liquefied Wood based As-cured Precursors and Carbon Fibers
title_full_unstemmed Effects of Chemical Curing Temperature and Time on the Properties of Liquefied Wood based As-cured Precursors and Carbon Fibers
title_short Effects of Chemical Curing Temperature and Time on the Properties of Liquefied Wood based As-cured Precursors and Carbon Fibers
title_sort effects of chemical curing temperature and time on the properties of liquefied wood based as cured precursors and carbon fibers
topic Chemical curing
Carbon fibers
Tensile strength
As-cured Precursor
url http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_10_4_7477_Shang_Chemical_Curing_Temperature_Precursors
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