Dynamic recrystallization and precipitation in an Al–Mg–Sc alloy: effect of strain rate

Al–Mg–Sc alloy ingots were compressed 80% at different strain rates (1/s, 0.01/s and 0.0001/s) and different temperatures (300 °C and 450 °C). The microstructure was characterized by SEM, EBSD, XRD and TEM. The EBSD results show that the samples with a deformation rate of 0.01/s have the largest num...

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Main Authors: Jingyu Jiang, Feng Jiang, Menghan Zhang
Format: Article
Language:English
Published: Elsevier 2022-07-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2238785422007931
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author Jingyu Jiang
Feng Jiang
Menghan Zhang
author_facet Jingyu Jiang
Feng Jiang
Menghan Zhang
author_sort Jingyu Jiang
collection DOAJ
description Al–Mg–Sc alloy ingots were compressed 80% at different strain rates (1/s, 0.01/s and 0.0001/s) and different temperatures (300 °C and 450 °C). The microstructure was characterized by SEM, EBSD, XRD and TEM. The EBSD results show that the samples with a deformation rate of 0.01/s have the largest number of tiny equiaxed grains at the grain boundaries, but the equiaxed grains in the 0.0001/s sample are less and larger. This indicates that the number of new equiaxed grains does not always increase with decreasing strain rate. Furthermore, the TEM results confirmed that the recrystallization mechanism with a strain rate of 0.0001/s is similar to in situ recrystallization. The XRD results show that with the increase of temperature and the decrease of strain rate, there are fewer dislocations in the samples after thermal deformation. The particle stimulated recrystallization is also different in the 0.01/s sample and the 0.0001/s sample. Furthermore, at a strain rate of 0.0001/s, a large number of fine Al3(Sc,Zr) particles appear, which is due to the dynamic precipitation during slow thermal deformation.
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spelling doaj.art-14f73560de5c4ae48f5a29be59da56ef2022-12-22T04:18:51ZengElsevierJournal of Materials Research and Technology2238-78542022-07-011914441456Dynamic recrystallization and precipitation in an Al–Mg–Sc alloy: effect of strain rateJingyu Jiang0Feng Jiang1Menghan Zhang2School of Metallurgy and Environment, Central South University, Changsha 410083, ChinaSchool of Material Science and Engineering, Central South University, Changsha 410083, China; Light Alloy Research Institute, Central South University, Changsha 410083, China; The National Key Laboratory of Science and Technology on High-Strength Lightweight Structural Materials, Central South University, Changsha 410083, China; Corresponding author.School of Material Science and Engineering, Central South University, Changsha 410083, China; Corresponding author.Al–Mg–Sc alloy ingots were compressed 80% at different strain rates (1/s, 0.01/s and 0.0001/s) and different temperatures (300 °C and 450 °C). The microstructure was characterized by SEM, EBSD, XRD and TEM. The EBSD results show that the samples with a deformation rate of 0.01/s have the largest number of tiny equiaxed grains at the grain boundaries, but the equiaxed grains in the 0.0001/s sample are less and larger. This indicates that the number of new equiaxed grains does not always increase with decreasing strain rate. Furthermore, the TEM results confirmed that the recrystallization mechanism with a strain rate of 0.0001/s is similar to in situ recrystallization. The XRD results show that with the increase of temperature and the decrease of strain rate, there are fewer dislocations in the samples after thermal deformation. The particle stimulated recrystallization is also different in the 0.01/s sample and the 0.0001/s sample. Furthermore, at a strain rate of 0.0001/s, a large number of fine Al3(Sc,Zr) particles appear, which is due to the dynamic precipitation during slow thermal deformation.http://www.sciencedirect.com/science/article/pii/S2238785422007931Al–Mg–Sc alloySlow hot deformationRecrystallizationAl3(Sc, Zr) precipitation
spellingShingle Jingyu Jiang
Feng Jiang
Menghan Zhang
Dynamic recrystallization and precipitation in an Al–Mg–Sc alloy: effect of strain rate
Journal of Materials Research and Technology
Al–Mg–Sc alloy
Slow hot deformation
Recrystallization
Al3(Sc, Zr) precipitation
title Dynamic recrystallization and precipitation in an Al–Mg–Sc alloy: effect of strain rate
title_full Dynamic recrystallization and precipitation in an Al–Mg–Sc alloy: effect of strain rate
title_fullStr Dynamic recrystallization and precipitation in an Al–Mg–Sc alloy: effect of strain rate
title_full_unstemmed Dynamic recrystallization and precipitation in an Al–Mg–Sc alloy: effect of strain rate
title_short Dynamic recrystallization and precipitation in an Al–Mg–Sc alloy: effect of strain rate
title_sort dynamic recrystallization and precipitation in an al mg sc alloy effect of strain rate
topic Al–Mg–Sc alloy
Slow hot deformation
Recrystallization
Al3(Sc, Zr) precipitation
url http://www.sciencedirect.com/science/article/pii/S2238785422007931
work_keys_str_mv AT jingyujiang dynamicrecrystallizationandprecipitationinanalmgscalloyeffectofstrainrate
AT fengjiang dynamicrecrystallizationandprecipitationinanalmgscalloyeffectofstrainrate
AT menghanzhang dynamicrecrystallizationandprecipitationinanalmgscalloyeffectofstrainrate