Coupling Ultrafiltration-Based Processes to Concentrate Phenolic Compounds from Aqueous Goji Berry Extracts

In this work, a membrane-based process for the purification and concentration of antioxidant compounds from aqueous Goji (<i>Lycium barbarum</i> L.) berry extracts was investigated. The aqueous extract was previously clarified with hollow fiber ultrafiltration (UF) membranes in order to...

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Main Authors: Carmela Conidi, Enrico Drioli, Alfredo Cassano
Format: Article
Language:English
Published: MDPI AG 2020-08-01
Series:Molecules
Subjects:
Online Access:https://www.mdpi.com/1420-3049/25/16/3761
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author Carmela Conidi
Enrico Drioli
Alfredo Cassano
author_facet Carmela Conidi
Enrico Drioli
Alfredo Cassano
author_sort Carmela Conidi
collection DOAJ
description In this work, a membrane-based process for the purification and concentration of antioxidant compounds from aqueous Goji (<i>Lycium barbarum</i> L.) berry extracts was investigated. The aqueous extract was previously clarified with hollow fiber ultrafiltration (UF) membranes in order to remove suspended solids and β-carotene and to produce a clarified extract enriched in phenolic compounds. Then, three UF flat sheet polyamide membranes with a molecular weight cut-off (MWCO) in the range 1000–3500 Da were tested to purify and concentrate phenolic compounds from the clarified extract. The effect of MWCO and transmembrane pressure (TMP) on the performance of selected membranes in terms of productivity and selectivity towards total dissolved solids (TDS), total phenolic compounds (TPC), total carbohydrates (TC) and total antioxidant activity (TAA) was evaluated. Experimental results indicated that the 2500 Da membrane exhibited a lower fouling index, higher cleaning efficiency, lower rejection towards carbohydrates (lower than 30%) and higher rejection towards phenolic compounds (higher than 50%) in comparison to the other investigated membranes. The inclusion of a diafiltration process in the treatment of the clarified extract with this membrane in a spiral-wound configuration improved the concentration of sugar compounds in the permeate stream and increased the purification of phenolic compounds in the retentate fraction.
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spelling doaj.art-15b29a054733445bac30418938b42b6a2023-11-20T10:30:20ZengMDPI AGMolecules1420-30492020-08-012516376110.3390/molecules25163761Coupling Ultrafiltration-Based Processes to Concentrate Phenolic Compounds from Aqueous Goji Berry ExtractsCarmela Conidi0Enrico Drioli1Alfredo Cassano2Institute on Membrane Technology, ITM-CNR, Via P. Bucci 17/C, 87036 CS Rende, ItalyInstitute on Membrane Technology, ITM-CNR, Via P. Bucci 17/C, 87036 CS Rende, ItalyDepartment of Engineering and of the Environment, University of Calabria, Via P. Bucci 45/A, 87036 CS Rende, ItalyIn this work, a membrane-based process for the purification and concentration of antioxidant compounds from aqueous Goji (<i>Lycium barbarum</i> L.) berry extracts was investigated. The aqueous extract was previously clarified with hollow fiber ultrafiltration (UF) membranes in order to remove suspended solids and β-carotene and to produce a clarified extract enriched in phenolic compounds. Then, three UF flat sheet polyamide membranes with a molecular weight cut-off (MWCO) in the range 1000–3500 Da were tested to purify and concentrate phenolic compounds from the clarified extract. The effect of MWCO and transmembrane pressure (TMP) on the performance of selected membranes in terms of productivity and selectivity towards total dissolved solids (TDS), total phenolic compounds (TPC), total carbohydrates (TC) and total antioxidant activity (TAA) was evaluated. Experimental results indicated that the 2500 Da membrane exhibited a lower fouling index, higher cleaning efficiency, lower rejection towards carbohydrates (lower than 30%) and higher rejection towards phenolic compounds (higher than 50%) in comparison to the other investigated membranes. The inclusion of a diafiltration process in the treatment of the clarified extract with this membrane in a spiral-wound configuration improved the concentration of sugar compounds in the permeate stream and increased the purification of phenolic compounds in the retentate fraction.https://www.mdpi.com/1420-3049/25/16/3761<i>Lycium barbarum</i> L.Goji berriesultrafiltrationantioxidantsphenolic compoundsmembrane processes
spellingShingle Carmela Conidi
Enrico Drioli
Alfredo Cassano
Coupling Ultrafiltration-Based Processes to Concentrate Phenolic Compounds from Aqueous Goji Berry Extracts
Molecules
<i>Lycium barbarum</i> L.
Goji berries
ultrafiltration
antioxidants
phenolic compounds
membrane processes
title Coupling Ultrafiltration-Based Processes to Concentrate Phenolic Compounds from Aqueous Goji Berry Extracts
title_full Coupling Ultrafiltration-Based Processes to Concentrate Phenolic Compounds from Aqueous Goji Berry Extracts
title_fullStr Coupling Ultrafiltration-Based Processes to Concentrate Phenolic Compounds from Aqueous Goji Berry Extracts
title_full_unstemmed Coupling Ultrafiltration-Based Processes to Concentrate Phenolic Compounds from Aqueous Goji Berry Extracts
title_short Coupling Ultrafiltration-Based Processes to Concentrate Phenolic Compounds from Aqueous Goji Berry Extracts
title_sort coupling ultrafiltration based processes to concentrate phenolic compounds from aqueous goji berry extracts
topic <i>Lycium barbarum</i> L.
Goji berries
ultrafiltration
antioxidants
phenolic compounds
membrane processes
url https://www.mdpi.com/1420-3049/25/16/3761
work_keys_str_mv AT carmelaconidi couplingultrafiltrationbasedprocessestoconcentratephenoliccompoundsfromaqueousgojiberryextracts
AT enricodrioli couplingultrafiltrationbasedprocessestoconcentratephenoliccompoundsfromaqueousgojiberryextracts
AT alfredocassano couplingultrafiltrationbasedprocessestoconcentratephenoliccompoundsfromaqueousgojiberryextracts