Control of Nd-Fe-B Morphology as Function of the PVP Concentration Using Electrospinning Process

In this study, we demonstrate a facile and cost-effective way to synthesize Nd-Fe-B of various shapes such as powders, rods and fibers using electrospinning, heat-treatment and washing procedures. Initially Nd-Fe-B fibers were fabricated using electrospinning. The as-spun Nd-Fe-B fibers had diameter...

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Main Authors: Nu Si A Eom, Muhammad Aneeq Haq, Jimin Lee, Kyoung-Mook Lim, Taek Soo Kim, Yong-Ho Choa, Bum Sung Kim
Format: Article
Language:English
Published: Polish Academy of Sciences 2020-07-01
Series:Archives of Metallurgy and Materials
Subjects:
Online Access:https://journals.pan.pl/Content/116369/PDF/AMM-2020-3-02-Bum%20Sung%20Kim.pdf
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author Nu Si A Eom
Muhammad Aneeq Haq
Jimin Lee
Kyoung-Mook Lim
Taek Soo Kim
Yong-Ho Choa
Bum Sung Kim
author_facet Nu Si A Eom
Muhammad Aneeq Haq
Jimin Lee
Kyoung-Mook Lim
Taek Soo Kim
Yong-Ho Choa
Bum Sung Kim
author_sort Nu Si A Eom
collection DOAJ
description In this study, we demonstrate a facile and cost-effective way to synthesize Nd-Fe-B of various shapes such as powders, rods and fibers using electrospinning, heat-treatment and washing procedures. Initially Nd-Fe-B fibers were fabricated using electrospinning. The as-spun Nd-Fe-B fibers had diameters ranging 489 to 630 nm depending on the PVP concentration in reaction solutions. The different morphologies of the Nd2Fe14B magnetic materials were related to the difference in thickness of the as-spun fibers. The relationships between the as-spun fiber thickness, the final morphology, and magnetic properties were briefly elucidated. The intrinsic coercivity of Nd2Fe14B changed with the change in morphology from powder (3908 Oe) to fiber (4622 Oe). This work demonstrates the effect of the Nd-Fe-B magnetic properties with morphology and can be extended to the experimental design of other magnetic materials.
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spelling doaj.art-15c2c912d387485797fd2d7daae03d2b2022-12-22T04:00:27ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092020-07-01vol. 65No 3993996https://doi.org/10.24425/amm.2020.133204Control of Nd-Fe-B Morphology as Function of the PVP Concentration Using Electrospinning ProcessNu Si A EomMuhammad Aneeq HaqJimin LeeKyoung-Mook LimTaek Soo KimYong-Ho Choahttps://orcid.org/0000-0002-1254-3593Bum Sung KimIn this study, we demonstrate a facile and cost-effective way to synthesize Nd-Fe-B of various shapes such as powders, rods and fibers using electrospinning, heat-treatment and washing procedures. Initially Nd-Fe-B fibers were fabricated using electrospinning. The as-spun Nd-Fe-B fibers had diameters ranging 489 to 630 nm depending on the PVP concentration in reaction solutions. The different morphologies of the Nd2Fe14B magnetic materials were related to the difference in thickness of the as-spun fibers. The relationships between the as-spun fiber thickness, the final morphology, and magnetic properties were briefly elucidated. The intrinsic coercivity of Nd2Fe14B changed with the change in morphology from powder (3908 Oe) to fiber (4622 Oe). This work demonstrates the effect of the Nd-Fe-B magnetic properties with morphology and can be extended to the experimental design of other magnetic materials.https://journals.pan.pl/Content/116369/PDF/AMM-2020-3-02-Bum%20Sung%20Kim.pdfnd2fe14b1-d magnet fiberelectrospinningmagnet propertiesmorphology
spellingShingle Nu Si A Eom
Muhammad Aneeq Haq
Jimin Lee
Kyoung-Mook Lim
Taek Soo Kim
Yong-Ho Choa
Bum Sung Kim
Control of Nd-Fe-B Morphology as Function of the PVP Concentration Using Electrospinning Process
Archives of Metallurgy and Materials
nd2fe14b
1-d magnet fiber
electrospinning
magnet properties
morphology
title Control of Nd-Fe-B Morphology as Function of the PVP Concentration Using Electrospinning Process
title_full Control of Nd-Fe-B Morphology as Function of the PVP Concentration Using Electrospinning Process
title_fullStr Control of Nd-Fe-B Morphology as Function of the PVP Concentration Using Electrospinning Process
title_full_unstemmed Control of Nd-Fe-B Morphology as Function of the PVP Concentration Using Electrospinning Process
title_short Control of Nd-Fe-B Morphology as Function of the PVP Concentration Using Electrospinning Process
title_sort control of nd fe b morphology as function of the pvp concentration using electrospinning process
topic nd2fe14b
1-d magnet fiber
electrospinning
magnet properties
morphology
url https://journals.pan.pl/Content/116369/PDF/AMM-2020-3-02-Bum%20Sung%20Kim.pdf
work_keys_str_mv AT nusiaeom controlofndfebmorphologyasfunctionofthepvpconcentrationusingelectrospinningprocess
AT muhammadaneeqhaq controlofndfebmorphologyasfunctionofthepvpconcentrationusingelectrospinningprocess
AT jiminlee controlofndfebmorphologyasfunctionofthepvpconcentrationusingelectrospinningprocess
AT kyoungmooklim controlofndfebmorphologyasfunctionofthepvpconcentrationusingelectrospinningprocess
AT taeksookim controlofndfebmorphologyasfunctionofthepvpconcentrationusingelectrospinningprocess
AT yonghochoa controlofndfebmorphologyasfunctionofthepvpconcentrationusingelectrospinningprocess
AT bumsungkim controlofndfebmorphologyasfunctionofthepvpconcentrationusingelectrospinningprocess