Diethyl [(2,5-diiodo-4-methylphenyl)methyl]phosphonate
The title compound, C12H17I2O3P, was prepared in three steps from p-xylene. Heterodimers between nearly identical molecules are connected via three hydrogen bonds from benzylic and ester methylene groups to phosphonate. The dimers form chains along the a-axis direction, stabilized by C—H...O bridges...
| Main Authors: | , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2021-06-01
|
| Series: | IUCrData |
| Subjects: | |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S2414314621006544 |
| _version_ | 1818669266010898432 |
|---|---|
| author | Dieter Schollmeyer Oleg Sadovski Heiner Detert |
| author_facet | Dieter Schollmeyer Oleg Sadovski Heiner Detert |
| author_sort | Dieter Schollmeyer |
| collection | DOAJ |
| description | The title compound, C12H17I2O3P, was prepared in three steps from p-xylene. Heterodimers between nearly identical molecules are connected via three hydrogen bonds from benzylic and ester methylene groups to phosphonate. The dimers form chains along the a-axis direction, stabilized by C—H...O bridges. |
| first_indexed | 2024-12-17T06:49:29Z |
| format | Article |
| id | doaj.art-1607a611e0bb49b8b0f210d97f31cbc1 |
| institution | Directory Open Access Journal |
| issn | 2414-3146 |
| language | English |
| last_indexed | 2024-12-17T06:49:29Z |
| publishDate | 2021-06-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | IUCrData |
| spelling | doaj.art-1607a611e0bb49b8b0f210d97f31cbc12022-12-21T21:59:38ZengInternational Union of CrystallographyIUCrData2414-31462021-06-0166x21065410.1107/S2414314621006544bt4116Diethyl [(2,5-diiodo-4-methylphenyl)methyl]phosphonateDieter Schollmeyer0Oleg Sadovski1Heiner Detert2University of Mainz, Institut for Organic Chemistry, Duesbergweg 10-14, 55099 Mainz, GermanyUniversity of Mainz, Institut for Organic Chemistry, Duesbergweg 10-14, 55099 Mainz, GermanyUniversity of Mainz, Institut for Organic Chemistry, Duesbergweg 10-14, 55099 Mainz, GermanyThe title compound, C12H17I2O3P, was prepared in three steps from p-xylene. Heterodimers between nearly identical molecules are connected via three hydrogen bonds from benzylic and ester methylene groups to phosphonate. The dimers form chains along the a-axis direction, stabilized by C—H...O bridges.http://scripts.iucr.org/cgi-bin/paper?S2414314621006544crystal structureiodinephosphonatetwo-component twin |
| spellingShingle | Dieter Schollmeyer Oleg Sadovski Heiner Detert Diethyl [(2,5-diiodo-4-methylphenyl)methyl]phosphonate IUCrData crystal structure iodine phosphonate two-component twin |
| title | Diethyl [(2,5-diiodo-4-methylphenyl)methyl]phosphonate |
| title_full | Diethyl [(2,5-diiodo-4-methylphenyl)methyl]phosphonate |
| title_fullStr | Diethyl [(2,5-diiodo-4-methylphenyl)methyl]phosphonate |
| title_full_unstemmed | Diethyl [(2,5-diiodo-4-methylphenyl)methyl]phosphonate |
| title_short | Diethyl [(2,5-diiodo-4-methylphenyl)methyl]phosphonate |
| title_sort | diethyl 2 5 diiodo 4 methylphenyl methyl phosphonate |
| topic | crystal structure iodine phosphonate two-component twin |
| url | http://scripts.iucr.org/cgi-bin/paper?S2414314621006544 |
| work_keys_str_mv | AT dieterschollmeyer diethyl25diiodo4methylphenylmethylphosphonate AT olegsadovski diethyl25diiodo4methylphenylmethylphosphonate AT heinerdetert diethyl25diiodo4methylphenylmethylphosphonate |