Thermal and chemical structure of ethanol and 2-ethylhexanoic acid/ethanol SpraySyn flames

Flame spray pyrolysis is intensively developing as a promising method of nanoparticle synthesis. The experimentally measured chemical and thermal structure of the spray flame is critically needed as a validation target for simulations of the synthesis of nanoparticles in these spray flames. This pap...

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Main Authors: Munko Gonchikzhapov, Tina Kasper
Format: Article
Language:English
Published: Elsevier 2023-09-01
Series:Applications in Energy and Combustion Science
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2666352X23000638
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author Munko Gonchikzhapov
Tina Kasper
author_facet Munko Gonchikzhapov
Tina Kasper
author_sort Munko Gonchikzhapov
collection DOAJ
description Flame spray pyrolysis is intensively developing as a promising method of nanoparticle synthesis. The experimentally measured chemical and thermal structure of the spray flame is critically needed as a validation target for simulations of the synthesis of nanoparticles in these spray flames. This paper presents an experimental study of the chemical and thermal structure of the flame produced by the SpraySyn burner. The spatial distribution of the main species is obtained by microprobe sampling in combination with orthogonal time-of-flight mass spectrometry. The temperature distribution is obtained by a micro-thermocouple technique. The presented species and temperature data are discussed in the context of their experimental uncertainties and the plausibility of the flame structure.
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spelling doaj.art-16883d89e9914d449a041c3bd41202012023-09-11T04:17:36ZengElsevierApplications in Energy and Combustion Science2666-352X2023-09-0115100174Thermal and chemical structure of ethanol and 2-ethylhexanoic acid/ethanol SpraySyn flamesMunko Gonchikzhapov0Tina Kasper1Corresponding author.; Technical Thermodynamics, Paderborn University, Warburgerstr. 100, Paderborn 33098, GermanyTechnical Thermodynamics, Paderborn University, Warburgerstr. 100, Paderborn 33098, GermanyFlame spray pyrolysis is intensively developing as a promising method of nanoparticle synthesis. The experimentally measured chemical and thermal structure of the spray flame is critically needed as a validation target for simulations of the synthesis of nanoparticles in these spray flames. This paper presents an experimental study of the chemical and thermal structure of the flame produced by the SpraySyn burner. The spatial distribution of the main species is obtained by microprobe sampling in combination with orthogonal time-of-flight mass spectrometry. The temperature distribution is obtained by a micro-thermocouple technique. The presented species and temperature data are discussed in the context of their experimental uncertainties and the plausibility of the flame structure.http://www.sciencedirect.com/science/article/pii/S2666352X23000638Nanoparticle synthesisFlame spray pyrolysisSpraySyn burnerFlame structureSpecies distributionTemperature distribution
spellingShingle Munko Gonchikzhapov
Tina Kasper
Thermal and chemical structure of ethanol and 2-ethylhexanoic acid/ethanol SpraySyn flames
Applications in Energy and Combustion Science
Nanoparticle synthesis
Flame spray pyrolysis
SpraySyn burner
Flame structure
Species distribution
Temperature distribution
title Thermal and chemical structure of ethanol and 2-ethylhexanoic acid/ethanol SpraySyn flames
title_full Thermal and chemical structure of ethanol and 2-ethylhexanoic acid/ethanol SpraySyn flames
title_fullStr Thermal and chemical structure of ethanol and 2-ethylhexanoic acid/ethanol SpraySyn flames
title_full_unstemmed Thermal and chemical structure of ethanol and 2-ethylhexanoic acid/ethanol SpraySyn flames
title_short Thermal and chemical structure of ethanol and 2-ethylhexanoic acid/ethanol SpraySyn flames
title_sort thermal and chemical structure of ethanol and 2 ethylhexanoic acid ethanol spraysyn flames
topic Nanoparticle synthesis
Flame spray pyrolysis
SpraySyn burner
Flame structure
Species distribution
Temperature distribution
url http://www.sciencedirect.com/science/article/pii/S2666352X23000638
work_keys_str_mv AT munkogonchikzhapov thermalandchemicalstructureofethanoland2ethylhexanoicacidethanolspraysynflames
AT tinakasper thermalandchemicalstructureofethanoland2ethylhexanoicacidethanolspraysynflames