Microstructure and Mechanical Properties of 4Al Alumina-Forming Austenitic Steel after Cold-Rolling Deformation and Annealing

Microstructural evolutions of the 4Al alumina-forming austenitic steel after cold rolling with different reductions from 5% to 30% and then annealing were investigated using electron backscattering diffraction (EBSD), X-ray diffraction (XRD) and transmission electron microscopy (TEM). Tensile proper...

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Main Authors: Chenchen Jiang, Qiuzhi Gao, Hailian Zhang, Ziyun Liu, Huijun Li
Format: Article
Language:English
Published: MDPI AG 2020-06-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/13/12/2767
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author Chenchen Jiang
Qiuzhi Gao
Hailian Zhang
Ziyun Liu
Huijun Li
author_facet Chenchen Jiang
Qiuzhi Gao
Hailian Zhang
Ziyun Liu
Huijun Li
author_sort Chenchen Jiang
collection DOAJ
description Microstructural evolutions of the 4Al alumina-forming austenitic steel after cold rolling with different reductions from 5% to 30% and then annealing were investigated using electron backscattering diffraction (EBSD), X-ray diffraction (XRD) and transmission electron microscopy (TEM). Tensile properties and hardness were also measured. The results show that the average grain size gradually decreases with an increase in the cold-rolling reduction. The low angle grain boundaries (LAGBs) are dominant in the cold-rolled samples, but high angle grain boundaries (HAGBs) form in the annealed samples, indicating that the grains are refined under the action of dislocations. During cold rolling, high-density dislocations are initially introduced in the samples, which contributes to a large number of dislocations remaining after annealing. With the sustaining increase in cold-rolled deformation, the samples exhibit more excellent tensile strength and hardness due to the decrease in grain size and increase in dislocation density, especially for the samples subjected to 30% cold-rolling reduction. The contribution of dislocations on yield strength is more than 60%.
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spelling doaj.art-16c6ffbff1e64eea9b55cffcbd5c2cdc2023-11-20T04:15:19ZengMDPI AGMaterials1996-19442020-06-011312276710.3390/ma13122767Microstructure and Mechanical Properties of 4Al Alumina-Forming Austenitic Steel after Cold-Rolling Deformation and AnnealingChenchen Jiang0Qiuzhi Gao1Hailian Zhang2Ziyun Liu3Huijun Li4School of Resources and Materials, Northeastern University at Qinhuangdao, Qinhuangdao 066004, ChinaSchool of Resources and Materials, Northeastern University at Qinhuangdao, Qinhuangdao 066004, ChinaDaotian High Technology Co., Ltd., Qinhuangdao 066004, ChinaSchool of Resources and Materials, Northeastern University at Qinhuangdao, Qinhuangdao 066004, ChinaSchool of Materials Science & Engineering, Tianjin University, Tianjin 300354, ChinaMicrostructural evolutions of the 4Al alumina-forming austenitic steel after cold rolling with different reductions from 5% to 30% and then annealing were investigated using electron backscattering diffraction (EBSD), X-ray diffraction (XRD) and transmission electron microscopy (TEM). Tensile properties and hardness were also measured. The results show that the average grain size gradually decreases with an increase in the cold-rolling reduction. The low angle grain boundaries (LAGBs) are dominant in the cold-rolled samples, but high angle grain boundaries (HAGBs) form in the annealed samples, indicating that the grains are refined under the action of dislocations. During cold rolling, high-density dislocations are initially introduced in the samples, which contributes to a large number of dislocations remaining after annealing. With the sustaining increase in cold-rolled deformation, the samples exhibit more excellent tensile strength and hardness due to the decrease in grain size and increase in dislocation density, especially for the samples subjected to 30% cold-rolling reduction. The contribution of dislocations on yield strength is more than 60%.https://www.mdpi.com/1996-1944/13/12/2767alumina-forming austenitic steelcold rollingdislocation densitymechanical properties
spellingShingle Chenchen Jiang
Qiuzhi Gao
Hailian Zhang
Ziyun Liu
Huijun Li
Microstructure and Mechanical Properties of 4Al Alumina-Forming Austenitic Steel after Cold-Rolling Deformation and Annealing
Materials
alumina-forming austenitic steel
cold rolling
dislocation density
mechanical properties
title Microstructure and Mechanical Properties of 4Al Alumina-Forming Austenitic Steel after Cold-Rolling Deformation and Annealing
title_full Microstructure and Mechanical Properties of 4Al Alumina-Forming Austenitic Steel after Cold-Rolling Deformation and Annealing
title_fullStr Microstructure and Mechanical Properties of 4Al Alumina-Forming Austenitic Steel after Cold-Rolling Deformation and Annealing
title_full_unstemmed Microstructure and Mechanical Properties of 4Al Alumina-Forming Austenitic Steel after Cold-Rolling Deformation and Annealing
title_short Microstructure and Mechanical Properties of 4Al Alumina-Forming Austenitic Steel after Cold-Rolling Deformation and Annealing
title_sort microstructure and mechanical properties of 4al alumina forming austenitic steel after cold rolling deformation and annealing
topic alumina-forming austenitic steel
cold rolling
dislocation density
mechanical properties
url https://www.mdpi.com/1996-1944/13/12/2767
work_keys_str_mv AT chenchenjiang microstructureandmechanicalpropertiesof4alaluminaformingausteniticsteelaftercoldrollingdeformationandannealing
AT qiuzhigao microstructureandmechanicalpropertiesof4alaluminaformingausteniticsteelaftercoldrollingdeformationandannealing
AT hailianzhang microstructureandmechanicalpropertiesof4alaluminaformingausteniticsteelaftercoldrollingdeformationandannealing
AT ziyunliu microstructureandmechanicalpropertiesof4alaluminaformingausteniticsteelaftercoldrollingdeformationandannealing
AT huijunli microstructureandmechanicalpropertiesof4alaluminaformingausteniticsteelaftercoldrollingdeformationandannealing