| Summary: | For the first time ever, samples were collected from volcanic lake waters in Costa Rica using an unmanned aerial vehicle (drone), which represents a major achievement in human–machine interaction and innovation in the technology sector. A Matrice 600 Pro drone was used for remote sampling in the hyperacid crater lake of the Poás volcano, the mildly acidic Lake Botos, and the nearly neutral Lake Hule. A bailer bottle of 250 mL and a HOBO temperature probe, mounted on the drone, were deployed using a specially designed delivery retrieval system. A comparison was carried out relating to the geochemistry of lake water collected by drone as opposed to the hand-collected samples. The SO4−2/Cl ratios of the two samples at Poás hyperacid crater lake were similar, (1.1 ± 0.2) on average, an indication of a lake with homogenous water composition. The Lake Hule showed a similar composition to that registered 20 years ago. The waters from Lake Botos showed some differences, which may be explained by the influence of springs at the bottom of the lake, but the Wilcoxon's signed-rank test showed a good exhibit of a satisfactory level of similarity. Autonomous navigation proves to be very useful for faster, more efficient, reliable, and less hazardous sampling of volcanic lakes.
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