(E)-2,4-Dihydroxy-N′-(2-hydroxy-3-methoxy-5-nitrobenzylidene)benzohydrazide dihydrate
The asymmetric unit of the title compound, C15H13N3O7·2H2O, consists of a hydrazone molecule and two solvent water molecules. The molecule adopts an E configuration with respect to the C=N bond. It is relatively planar, with a dihedral angle between the two benzene rings of 2.6&...
| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2010-05-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536810013000 |
| _version_ | 1818775483036205056 |
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| author | You-Yue Han Yong-Hong Li Qiu-Rong Zhao |
| author_facet | You-Yue Han Yong-Hong Li Qiu-Rong Zhao |
| author_sort | You-Yue Han |
| collection | DOAJ |
| description | The asymmetric unit of the title compound, C15H13N3O7·2H2O, consists of a hydrazone molecule and two solvent water molecules. The molecule adopts an E configuration with respect to the C=N bond. It is relatively planar, with a dihedral angle between the two benzene rings of 2.6 (1)°. There are intramolecular O—H...N and O—H...O hydrogen bonds in the hydrazone molecule. In the crystal structure, symmetry-related molecules are linked through intermolecular N—H...O and O—H...O hydrogen bonds to form a three-dimensional network. |
| first_indexed | 2024-12-18T10:57:45Z |
| format | Article |
| id | doaj.art-1715b59ed9ba4dbca089f8e0059f664b |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-18T10:57:45Z |
| publishDate | 2010-05-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-1715b59ed9ba4dbca089f8e0059f664b2022-12-21T21:10:17ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-05-01665o1085o108610.1107/S1600536810013000(E)-2,4-Dihydroxy-N′-(2-hydroxy-3-methoxy-5-nitrobenzylidene)benzohydrazide dihydrateYou-Yue HanYong-Hong LiQiu-Rong ZhaoThe asymmetric unit of the title compound, C15H13N3O7·2H2O, consists of a hydrazone molecule and two solvent water molecules. The molecule adopts an E configuration with respect to the C=N bond. It is relatively planar, with a dihedral angle between the two benzene rings of 2.6 (1)°. There are intramolecular O—H...N and O—H...O hydrogen bonds in the hydrazone molecule. In the crystal structure, symmetry-related molecules are linked through intermolecular N—H...O and O—H...O hydrogen bonds to form a three-dimensional network.http://scripts.iucr.org/cgi-bin/paper?S1600536810013000 |
| spellingShingle | You-Yue Han Yong-Hong Li Qiu-Rong Zhao (E)-2,4-Dihydroxy-N′-(2-hydroxy-3-methoxy-5-nitrobenzylidene)benzohydrazide dihydrate Acta Crystallographica Section E |
| title | (E)-2,4-Dihydroxy-N′-(2-hydroxy-3-methoxy-5-nitrobenzylidene)benzohydrazide dihydrate |
| title_full | (E)-2,4-Dihydroxy-N′-(2-hydroxy-3-methoxy-5-nitrobenzylidene)benzohydrazide dihydrate |
| title_fullStr | (E)-2,4-Dihydroxy-N′-(2-hydroxy-3-methoxy-5-nitrobenzylidene)benzohydrazide dihydrate |
| title_full_unstemmed | (E)-2,4-Dihydroxy-N′-(2-hydroxy-3-methoxy-5-nitrobenzylidene)benzohydrazide dihydrate |
| title_short | (E)-2,4-Dihydroxy-N′-(2-hydroxy-3-methoxy-5-nitrobenzylidene)benzohydrazide dihydrate |
| title_sort | e 2 4 dihydroxy n amp 8242 2 hydroxy 3 methoxy 5 nitrobenzylidene benzohydrazide dihydrate |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536810013000 |
| work_keys_str_mv | AT youyuehan e24dihydroxynamp82422hydroxy3methoxy5nitrobenzylidenebenzohydrazidedihydrate AT yonghongli e24dihydroxynamp82422hydroxy3methoxy5nitrobenzylidenebenzohydrazidedihydrate AT qiurongzhao e24dihydroxynamp82422hydroxy3methoxy5nitrobenzylidenebenzohydrazidedihydrate |