Consolidation and Characterisation of Hard Metal Powders Milled under Dichloromethane
This work presents the development of a safer processing route for hard metals. Traditional processing of fine particles under organic solvents presents significant explosion risks. The milling under dichloromethane (DCM) reduces the risks associated with fire hazards. After milling and drying, the...
| Main Authors: | , , , , , |
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| Format: | Article |
| Language: | English |
| Published: |
Polish Academy of Sciences
2022-06-01
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| Series: | Archives of Metallurgy and Materials |
| Subjects: | |
| Online Access: | https://journals.pan.pl/Content/123277/PDF/AMM-2022-2-20-Chicinas.pdf |
| _version_ | 1818489631979601920 |
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| author | H.-F. Chicinaș O.-D. Jucan R.V. Gădălean G. Conțiu A. Cotai C.O. Popa |
| author_facet | H.-F. Chicinaș O.-D. Jucan R.V. Gădălean G. Conțiu A. Cotai C.O. Popa |
| author_sort | H.-F. Chicinaș |
| collection | DOAJ |
| description | This work presents the development of a safer processing route for hard metals. Traditional processing of fine particles under organic solvents presents significant explosion risks. The milling under dichloromethane (DCM) reduces the risks associated with fire hazards. After milling and drying, the samples have been sintered in an industrial sintering furnace under a vacuum at 1380°C. The materials’ characterisation has been done by X-ray diffraction, scanning electron microscopy, particle size analysis, optical microscopy, and by magnetic measurements. The present work results reveal the powders’ appropriate properties after milling and drying and the desired biphasic (Co-WC) phases obtained after sintering, thus proving the feasibility of such a route, therefore the diminishing of specific fire hazards. |
| first_indexed | 2024-12-10T17:06:22Z |
| format | Article |
| id | doaj.art-173eb1ad5fbf434fb5bb0c140a54cc5e |
| institution | Directory Open Access Journal |
| issn | 2300-1909 |
| language | English |
| last_indexed | 2024-12-10T17:06:22Z |
| publishDate | 2022-06-01 |
| publisher | Polish Academy of Sciences |
| record_format | Article |
| series | Archives of Metallurgy and Materials |
| spelling | doaj.art-173eb1ad5fbf434fb5bb0c140a54cc5e2022-12-22T01:40:26ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092022-06-01vol. 67No 2541545https://doi.org/10.24425/amm.2022.137788Consolidation and Characterisation of Hard Metal Powders Milled under DichloromethaneH.-F. Chicinaș0https://orcid.org/0000-0001-7150-8029O.-D. Jucan1https://orcid.org/0000-0002-5574-5873R.V. Gădălean2https://orcid.org/0000-0002-6186-9207G. Conțiu3https://orcid.org/0000-0002-1209-4839A. Cotai4https://orcid.org/0000-0002-0250-1293C.O. Popa5https://orcid.org/0000-0003-4188-1169Technical University of Cluj-Napoca, Materials Science and Engineering Department, 103-105 Muncii Avenue, 400641 Cluj-Napoca, RomaniaTechnical University of Cluj-Napoca, Materials Science and Engineering Department, 103-105 Muncii Avenue, 400641 Cluj-Napoca, RomaniaTechnical University of Cluj-Napoca, Materials Science and Engineering Department, 103-105 Muncii Avenue, 400641 Cluj-Napoca, RomaniaTechnical University of Cluj-Napoca, Materials Science and Engineering Department, 103-105 Muncii Avenue, 400641 Cluj-Napoca, RomaniaTechnical University of Cluj-Napoca, Materials Science and Engineering Department, 103-105 Muncii Avenue, 400641 Cluj-Napoca, RomaniaTechnical University of Cluj-Napoca, Materials Science and Engineering Department, 103-105 Muncii Avenue, 400641 Cluj-Napoca, RomaniaThis work presents the development of a safer processing route for hard metals. Traditional processing of fine particles under organic solvents presents significant explosion risks. The milling under dichloromethane (DCM) reduces the risks associated with fire hazards. After milling and drying, the samples have been sintered in an industrial sintering furnace under a vacuum at 1380°C. The materials’ characterisation has been done by X-ray diffraction, scanning electron microscopy, particle size analysis, optical microscopy, and by magnetic measurements. The present work results reveal the powders’ appropriate properties after milling and drying and the desired biphasic (Co-WC) phases obtained after sintering, thus proving the feasibility of such a route, therefore the diminishing of specific fire hazards.https://journals.pan.pl/Content/123277/PDF/AMM-2022-2-20-Chicinas.pdfhard metalsinteringmillingparticledichloromethane |
| spellingShingle | H.-F. Chicinaș O.-D. Jucan R.V. Gădălean G. Conțiu A. Cotai C.O. Popa Consolidation and Characterisation of Hard Metal Powders Milled under Dichloromethane Archives of Metallurgy and Materials hard metal sintering milling particle dichloromethane |
| title | Consolidation and Characterisation of Hard Metal Powders Milled under Dichloromethane |
| title_full | Consolidation and Characterisation of Hard Metal Powders Milled under Dichloromethane |
| title_fullStr | Consolidation and Characterisation of Hard Metal Powders Milled under Dichloromethane |
| title_full_unstemmed | Consolidation and Characterisation of Hard Metal Powders Milled under Dichloromethane |
| title_short | Consolidation and Characterisation of Hard Metal Powders Milled under Dichloromethane |
| title_sort | consolidation and characterisation of hard metal powders milled under dichloromethane |
| topic | hard metal sintering milling particle dichloromethane |
| url | https://journals.pan.pl/Content/123277/PDF/AMM-2022-2-20-Chicinas.pdf |
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