Magnetic characterization of cobalt nanowires and square nanorings fabricated by focused electron beam induced deposition

The magnetic properties of nanowires (NWs) and square nanorings, which were deposited by focused electron beam induced deposition (FEBID) of a Co carbonyl precursor, are studied using off-axis electron holography (EH), Lorentz transmission electron microscopy (L-TEM) and magnetic force microscopy (M...

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Main Authors: Federico Venturi, Gian Carlo Gazzadi, Amir H. Tavabi, Alberto Rota, Rafal E. Dunin-Borkowski, Stefano Frabboni
Format: Article
Language:English
Published: Beilstein-Institut 2018-04-01
Series:Beilstein Journal of Nanotechnology
Subjects:
Online Access:https://doi.org/10.3762/bjnano.9.97
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author Federico Venturi
Gian Carlo Gazzadi
Amir H. Tavabi
Alberto Rota
Rafal E. Dunin-Borkowski
Stefano Frabboni
author_facet Federico Venturi
Gian Carlo Gazzadi
Amir H. Tavabi
Alberto Rota
Rafal E. Dunin-Borkowski
Stefano Frabboni
author_sort Federico Venturi
collection DOAJ
description The magnetic properties of nanowires (NWs) and square nanorings, which were deposited by focused electron beam induced deposition (FEBID) of a Co carbonyl precursor, are studied using off-axis electron holography (EH), Lorentz transmission electron microscopy (L-TEM) and magnetic force microscopy (MFM). EH shows that NWs deposited using beam energies of 5 and 15 keV have the characteristics of magnetic dipoles, with larger magnetic moments observed for NWs deposited at lower energy. L-TEM is used to image magnetic domain walls in NWs and nanorings and their motion as a function of applied magnetic field. The NWs are found to have almost square hysteresis loops, with coercivities of ca. 10 mT. The nanorings show two different magnetization states: for low values of the applied in-plane field (0.02 T) a horseshoe state is observed using L-TEM, while for higher values of the applied in-plane field (0.3 T) an onion state is observed at remanence using L-TEM and MFM. Our results confirm the suitability of FEBID for nanofabrication of magnetic structures and demonstrate the versatility of TEM techniques for the study and manipulation of magnetic domain walls in nanostructures.
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spelling doaj.art-17c650365456481c84054efce21335732022-12-22T00:08:37ZengBeilstein-InstitutBeilstein Journal of Nanotechnology2190-42862018-04-01911040104910.3762/bjnano.9.972190-4286-9-97Magnetic characterization of cobalt nanowires and square nanorings fabricated by focused electron beam induced depositionFederico Venturi0Gian Carlo Gazzadi1Amir H. Tavabi2Alberto Rota3Rafal E. Dunin-Borkowski4Stefano Frabboni5FIM Department, University of Modena and Reggio Emilia, Via G. Campi 213/a, Modena I-41125, ItalyCNR – Nanoscience Institute, S3 Center, Via G. Campi 213/a, Modena I-41125, ItalyErnst Ruska-Centre for Microscopy and Spectroscopy with Electrons and Peter Grünberg Institute, Forschungszentrum Jülich, 52425 Jülich, GermanyIntermech-Mo.Re. Center, University of Modena and Reggio Emilia, Via Vignolese 905/b, Modena I-41125, ItalyErnst Ruska-Centre for Microscopy and Spectroscopy with Electrons and Peter Grünberg Institute, Forschungszentrum Jülich, 52425 Jülich, GermanyFIM Department, University of Modena and Reggio Emilia, Via G. Campi 213/a, Modena I-41125, ItalyThe magnetic properties of nanowires (NWs) and square nanorings, which were deposited by focused electron beam induced deposition (FEBID) of a Co carbonyl precursor, are studied using off-axis electron holography (EH), Lorentz transmission electron microscopy (L-TEM) and magnetic force microscopy (MFM). EH shows that NWs deposited using beam energies of 5 and 15 keV have the characteristics of magnetic dipoles, with larger magnetic moments observed for NWs deposited at lower energy. L-TEM is used to image magnetic domain walls in NWs and nanorings and their motion as a function of applied magnetic field. The NWs are found to have almost square hysteresis loops, with coercivities of ca. 10 mT. The nanorings show two different magnetization states: for low values of the applied in-plane field (0.02 T) a horseshoe state is observed using L-TEM, while for higher values of the applied in-plane field (0.3 T) an onion state is observed at remanence using L-TEM and MFM. Our results confirm the suitability of FEBID for nanofabrication of magnetic structures and demonstrate the versatility of TEM techniques for the study and manipulation of magnetic domain walls in nanostructures.https://doi.org/10.3762/bjnano.9.97focused electron beam induced depositionmagnetic force microscopymagnetic nanostructuresoff-axis electron holographytransmission electron microscopy
spellingShingle Federico Venturi
Gian Carlo Gazzadi
Amir H. Tavabi
Alberto Rota
Rafal E. Dunin-Borkowski
Stefano Frabboni
Magnetic characterization of cobalt nanowires and square nanorings fabricated by focused electron beam induced deposition
Beilstein Journal of Nanotechnology
focused electron beam induced deposition
magnetic force microscopy
magnetic nanostructures
off-axis electron holography
transmission electron microscopy
title Magnetic characterization of cobalt nanowires and square nanorings fabricated by focused electron beam induced deposition
title_full Magnetic characterization of cobalt nanowires and square nanorings fabricated by focused electron beam induced deposition
title_fullStr Magnetic characterization of cobalt nanowires and square nanorings fabricated by focused electron beam induced deposition
title_full_unstemmed Magnetic characterization of cobalt nanowires and square nanorings fabricated by focused electron beam induced deposition
title_short Magnetic characterization of cobalt nanowires and square nanorings fabricated by focused electron beam induced deposition
title_sort magnetic characterization of cobalt nanowires and square nanorings fabricated by focused electron beam induced deposition
topic focused electron beam induced deposition
magnetic force microscopy
magnetic nanostructures
off-axis electron holography
transmission electron microscopy
url https://doi.org/10.3762/bjnano.9.97
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