Additive manufacturing of carbon steels by materials extrusion of oxide precursors and hydrogen reduction

A hydrogen reduction-based method for additive manufacturing of carbon steels from low cost and stable oxide powders is presented. This method uses materials extrusion processes to extrude inks composed of oxide powders, plastic binders, and solvents. Oxide powders are synthesized into viscous inks...

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Main Authors: Collin Stiers, Katie Koube, Ethan Sinclair, Hyoungjun Sim, Elias Winterscheidt, Josh Kacher
Format: Article
Language:English
Published: Elsevier 2023-12-01
Series:Additive Manufacturing Letters
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2772369023000464
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author Collin Stiers
Katie Koube
Ethan Sinclair
Hyoungjun Sim
Elias Winterscheidt
Josh Kacher
author_facet Collin Stiers
Katie Koube
Ethan Sinclair
Hyoungjun Sim
Elias Winterscheidt
Josh Kacher
author_sort Collin Stiers
collection DOAJ
description A hydrogen reduction-based method for additive manufacturing of carbon steels from low cost and stable oxide powders is presented. This method uses materials extrusion processes to extrude inks composed of oxide powders, plastic binders, and solvents. Oxide powders are synthesized into viscous inks and extruded under ambient conditions into three-dimensional architectures. The three-dimensional printed green bodies are reduced at elevated temperatures in hydrogen-rich environments to burn off the polymer binder and reduce the oxide powders, yielding metal alloys with controlled compositions. While this approach has been demonstrated in previous publications for various alloys, the addition of carbon, an important element in most industrial steels, has been a persistent challenge. This paper demonstrates an approach to introduce carbon during the reduction process, resulting in through-thickness carburization of the final parts.
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spelling doaj.art-1b02ef2723a44aa9923c75f2c5bc410d2023-11-09T04:12:08ZengElsevierAdditive Manufacturing Letters2772-36902023-12-017100166Additive manufacturing of carbon steels by materials extrusion of oxide precursors and hydrogen reductionCollin Stiers0Katie Koube1Ethan Sinclair2Hyoungjun Sim3Elias Winterscheidt4Josh Kacher5Georgia Institute of Technology, Atlanta, GA, United StatesGeorgia Institute of Technology, Atlanta, GA, United StatesGeorgia Institute of Technology, Atlanta, GA, United StatesGeorgia Institute of Technology, Atlanta, GA, United StatesGeorgia Institute of Technology, Atlanta, GA, United StatesCorresponding author.; Georgia Institute of Technology, Atlanta, GA, United StatesA hydrogen reduction-based method for additive manufacturing of carbon steels from low cost and stable oxide powders is presented. This method uses materials extrusion processes to extrude inks composed of oxide powders, plastic binders, and solvents. Oxide powders are synthesized into viscous inks and extruded under ambient conditions into three-dimensional architectures. The three-dimensional printed green bodies are reduced at elevated temperatures in hydrogen-rich environments to burn off the polymer binder and reduce the oxide powders, yielding metal alloys with controlled compositions. While this approach has been demonstrated in previous publications for various alloys, the addition of carbon, an important element in most industrial steels, has been a persistent challenge. This paper demonstrates an approach to introduce carbon during the reduction process, resulting in through-thickness carburization of the final parts.http://www.sciencedirect.com/science/article/pii/S2772369023000464Material extrusionCarbon steelHydrogen reductionHeat treatmentMetal additive manufacturing
spellingShingle Collin Stiers
Katie Koube
Ethan Sinclair
Hyoungjun Sim
Elias Winterscheidt
Josh Kacher
Additive manufacturing of carbon steels by materials extrusion of oxide precursors and hydrogen reduction
Additive Manufacturing Letters
Material extrusion
Carbon steel
Hydrogen reduction
Heat treatment
Metal additive manufacturing
title Additive manufacturing of carbon steels by materials extrusion of oxide precursors and hydrogen reduction
title_full Additive manufacturing of carbon steels by materials extrusion of oxide precursors and hydrogen reduction
title_fullStr Additive manufacturing of carbon steels by materials extrusion of oxide precursors and hydrogen reduction
title_full_unstemmed Additive manufacturing of carbon steels by materials extrusion of oxide precursors and hydrogen reduction
title_short Additive manufacturing of carbon steels by materials extrusion of oxide precursors and hydrogen reduction
title_sort additive manufacturing of carbon steels by materials extrusion of oxide precursors and hydrogen reduction
topic Material extrusion
Carbon steel
Hydrogen reduction
Heat treatment
Metal additive manufacturing
url http://www.sciencedirect.com/science/article/pii/S2772369023000464
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AT eliaswinterscheidt additivemanufacturingofcarbonsteelsbymaterialsextrusionofoxideprecursorsandhydrogenreduction
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