Nanocomposites graphene/CoFe2O4 and graphene/NiFe2O4 – preparation and characterization

A series of nanocomposite graphene/CoFe2O4 and graphene/NiFe2O4 hybrid materials was synthesized via facile, one-pot solvothermal route. The materials were obtained using two pressure methods: synthesis in the autoclave and synthesis in the microwave solvothermal reactor. The use of a microwave reac...

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Main Authors: A. Jędrzejewska, D. Sibera, R. Pełech, R. Jędrzejewski, U. Narkiewicz
Format: Article
Language:English
Published: Polish Academy of Sciences 2019-03-01
Series:Archives of Metallurgy and Materials
Subjects:
Online Access:https://journals.pan.pl/Content/110137/PDF/AMM-2019-1-15-Jedrzejewska.pdf
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author A. Jędrzejewska
D. Sibera
R. Pełech
R. Jędrzejewski
U. Narkiewicz
author_facet A. Jędrzejewska
D. Sibera
R. Pełech
R. Jędrzejewski
U. Narkiewicz
author_sort A. Jędrzejewska
collection DOAJ
description A series of nanocomposite graphene/CoFe2O4 and graphene/NiFe2O4 hybrid materials was synthesized via facile, one-pot solvothermal route. The materials were obtained using two pressure methods: synthesis in the autoclave and synthesis in the microwave solvothermal reactor. The use of a microwave reactor enabled to significantly shorten the synthesis time up to 15 min. All the syntheses were carried out in a solution of ethanol. The effect of processing conditions and composite composition on the physicochemical properties and electric conductivity was studied. The specific surface area, density, morphology, phase composition, thermal properties and electric conductivity of the obtained composites were investigated. The results of studies of composites obtained in an autoclave and in a microwave reactor were compared.
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spelling doaj.art-1b2edd56611c4ab58969af4faa1369432022-12-22T01:40:07ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092019-03-01vol. 64No 1103112https://doi.org/10.24425/amm.2019.126224Nanocomposites graphene/CoFe2O4 and graphene/NiFe2O4 – preparation and characterizationA. JędrzejewskaD. SiberaR. PełechR. JędrzejewskiU. NarkiewiczA series of nanocomposite graphene/CoFe2O4 and graphene/NiFe2O4 hybrid materials was synthesized via facile, one-pot solvothermal route. The materials were obtained using two pressure methods: synthesis in the autoclave and synthesis in the microwave solvothermal reactor. The use of a microwave reactor enabled to significantly shorten the synthesis time up to 15 min. All the syntheses were carried out in a solution of ethanol. The effect of processing conditions and composite composition on the physicochemical properties and electric conductivity was studied. The specific surface area, density, morphology, phase composition, thermal properties and electric conductivity of the obtained composites were investigated. The results of studies of composites obtained in an autoclave and in a microwave reactor were compared.https://journals.pan.pl/Content/110137/PDF/AMM-2019-1-15-Jedrzejewska.pdfgraphenenanocompositescofe2o4nife2o4
spellingShingle A. Jędrzejewska
D. Sibera
R. Pełech
R. Jędrzejewski
U. Narkiewicz
Nanocomposites graphene/CoFe2O4 and graphene/NiFe2O4 – preparation and characterization
Archives of Metallurgy and Materials
graphene
nanocomposites
cofe2o4
nife2o4
title Nanocomposites graphene/CoFe2O4 and graphene/NiFe2O4 – preparation and characterization
title_full Nanocomposites graphene/CoFe2O4 and graphene/NiFe2O4 – preparation and characterization
title_fullStr Nanocomposites graphene/CoFe2O4 and graphene/NiFe2O4 – preparation and characterization
title_full_unstemmed Nanocomposites graphene/CoFe2O4 and graphene/NiFe2O4 – preparation and characterization
title_short Nanocomposites graphene/CoFe2O4 and graphene/NiFe2O4 – preparation and characterization
title_sort nanocomposites graphene cofe2o4 and graphene nife2o4 preparation and characterization
topic graphene
nanocomposites
cofe2o4
nife2o4
url https://journals.pan.pl/Content/110137/PDF/AMM-2019-1-15-Jedrzejewska.pdf
work_keys_str_mv AT ajedrzejewska nanocompositesgraphenecofe2o4andgraphenenife2o4preparationandcharacterization
AT dsibera nanocompositesgraphenecofe2o4andgraphenenife2o4preparationandcharacterization
AT rpełech nanocompositesgraphenecofe2o4andgraphenenife2o4preparationandcharacterization
AT rjedrzejewski nanocompositesgraphenecofe2o4andgraphenenife2o4preparationandcharacterization
AT unarkiewicz nanocompositesgraphenecofe2o4andgraphenenife2o4preparationandcharacterization