Nanocomposites Based on PCL and Halloysite Nanotubes Filled with Lysozyme: Effect of Draw Ratio on the Physical Properties and Release Analysis
Halloysite nanotubes (HNTs) were loaded with lsozyme, as antimicrobial molecule, at a HNTs/lysozyme ratio of 1:1. Such a nano-hybrid was incorporated into a poly (ε-caprolactone) (PCL) matrix at 10 wt % and films were obtained. The nano-composites were submitted to a cold drawn process at three diff...
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MDPI AG
2017-08-01
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Online Access: | https://www.mdpi.com/2079-4991/7/8/213 |
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author | Valeria Bugatti Gianluca Viscusi Carlo Naddeo Giuliana Gorrasi |
author_facet | Valeria Bugatti Gianluca Viscusi Carlo Naddeo Giuliana Gorrasi |
author_sort | Valeria Bugatti |
collection | DOAJ |
description | Halloysite nanotubes (HNTs) were loaded with lsozyme, as antimicrobial molecule, at a HNTs/lysozyme ratio of 1:1. Such a nano-hybrid was incorporated into a poly (ε-caprolactone) (PCL) matrix at 10 wt % and films were obtained. The nano-composites were submitted to a cold drawn process at three different draw ratios, λ = 3, 4, and 5, where λ is l(final length)/l0(initial length). Morphology, physical, and barrier properties of the starting nanocomposite and drawn samples were studied, and correlated to the release of the lysozyme molecule. It was demonstrated that with a simple mechanical treatment it is possible to obtain controlled release systems for specific active packaging requirements. |
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id | doaj.art-1bd46d43270742b0a2f5e5b14d377d58 |
institution | Directory Open Access Journal |
issn | 2079-4991 |
language | English |
last_indexed | 2024-04-12T21:34:12Z |
publishDate | 2017-08-01 |
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series | Nanomaterials |
spelling | doaj.art-1bd46d43270742b0a2f5e5b14d377d582022-12-22T03:15:57ZengMDPI AGNanomaterials2079-49912017-08-017821310.3390/nano7080213nano7080213Nanocomposites Based on PCL and Halloysite Nanotubes Filled with Lysozyme: Effect of Draw Ratio on the Physical Properties and Release AnalysisValeria Bugatti0Gianluca Viscusi1Carlo Naddeo2Giuliana Gorrasi3Department of Industrial Engineering, University of Salerno, Via Giovanni Paolo II, 132, 84084 Fisciano (Salerno), ItalyDepartment of Industrial Engineering, University of Salerno, Via Giovanni Paolo II, 132, 84084 Fisciano (Salerno), ItalyDepartment of Industrial Engineering, University of Salerno, Via Giovanni Paolo II, 132, 84084 Fisciano (Salerno), ItalyDepartment of Industrial Engineering, University of Salerno, Via Giovanni Paolo II, 132, 84084 Fisciano (Salerno), ItalyHalloysite nanotubes (HNTs) were loaded with lsozyme, as antimicrobial molecule, at a HNTs/lysozyme ratio of 1:1. Such a nano-hybrid was incorporated into a poly (ε-caprolactone) (PCL) matrix at 10 wt % and films were obtained. The nano-composites were submitted to a cold drawn process at three different draw ratios, λ = 3, 4, and 5, where λ is l(final length)/l0(initial length). Morphology, physical, and barrier properties of the starting nanocomposite and drawn samples were studied, and correlated to the release of the lysozyme molecule. It was demonstrated that with a simple mechanical treatment it is possible to obtain controlled release systems for specific active packaging requirements.https://www.mdpi.com/2079-4991/7/8/213halloysite nanotubesPCLlysozymecontrolled releaseactive packaging |
spellingShingle | Valeria Bugatti Gianluca Viscusi Carlo Naddeo Giuliana Gorrasi Nanocomposites Based on PCL and Halloysite Nanotubes Filled with Lysozyme: Effect of Draw Ratio on the Physical Properties and Release Analysis Nanomaterials halloysite nanotubes PCL lysozyme controlled release active packaging |
title | Nanocomposites Based on PCL and Halloysite Nanotubes Filled with Lysozyme: Effect of Draw Ratio on the Physical Properties and Release Analysis |
title_full | Nanocomposites Based on PCL and Halloysite Nanotubes Filled with Lysozyme: Effect of Draw Ratio on the Physical Properties and Release Analysis |
title_fullStr | Nanocomposites Based on PCL and Halloysite Nanotubes Filled with Lysozyme: Effect of Draw Ratio on the Physical Properties and Release Analysis |
title_full_unstemmed | Nanocomposites Based on PCL and Halloysite Nanotubes Filled with Lysozyme: Effect of Draw Ratio on the Physical Properties and Release Analysis |
title_short | Nanocomposites Based on PCL and Halloysite Nanotubes Filled with Lysozyme: Effect of Draw Ratio on the Physical Properties and Release Analysis |
title_sort | nanocomposites based on pcl and halloysite nanotubes filled with lysozyme effect of draw ratio on the physical properties and release analysis |
topic | halloysite nanotubes PCL lysozyme controlled release active packaging |
url | https://www.mdpi.com/2079-4991/7/8/213 |
work_keys_str_mv | AT valeriabugatti nanocompositesbasedonpclandhalloysitenanotubesfilledwithlysozymeeffectofdrawratioonthephysicalpropertiesandreleaseanalysis AT gianlucaviscusi nanocompositesbasedonpclandhalloysitenanotubesfilledwithlysozymeeffectofdrawratioonthephysicalpropertiesandreleaseanalysis AT carlonaddeo nanocompositesbasedonpclandhalloysitenanotubesfilledwithlysozymeeffectofdrawratioonthephysicalpropertiesandreleaseanalysis AT giulianagorrasi nanocompositesbasedonpclandhalloysitenanotubesfilledwithlysozymeeffectofdrawratioonthephysicalpropertiesandreleaseanalysis |