Synthesis and characterization of new 1,4-dihydropyran derivatives by novel Ta-MOF nanostructures as reusable nanocatalyst with antimicrobial activity
Novel Ta- MOF was synthesized under mild conditions by ultrasound irradiations. The sample was characterized by SEM, FTIR, XRD, XPS, TG and BET technique. The final structures showed high physicho-chemical properties including narrow particle size distribution, homogenous morphology, high thermal st...
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| Format: | Article |
| Language: | English |
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Frontiers Media S.A.
2022-09-01
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| Series: | Frontiers in Chemistry |
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| Online Access: | https://www.frontiersin.org/articles/10.3389/fchem.2022.967111/full |
| _version_ | 1811203820261212160 |
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| author | Irfan Ahmad Saade Abdalkareem Jasim Ghulam Yasin Basim Al-Qargholi Ali Thaeer Hammid |
| author_facet | Irfan Ahmad Saade Abdalkareem Jasim Ghulam Yasin Basim Al-Qargholi Ali Thaeer Hammid |
| author_sort | Irfan Ahmad |
| collection | DOAJ |
| description | Novel Ta- MOF was synthesized under mild conditions by ultrasound irradiations. The sample was characterized by SEM, FTIR, XRD, XPS, TG and BET technique. The final structures showed high physicho-chemical properties including narrow particle size distribution, homogenous morphology, high thermal stability and remarkable surface area. Ta- MOF synthesized in this study was used as a catalyst in the synthesis of 1,4-dihydropyran derivatives. The results proved that it has a high catalyst capability. Its advantages include high recyclability, less reaction time with higher efficiency and synthesis of new1,4-dihydropyran derivatives. In the following, antimicrobial activity including antifungal and antibacterial activity of Ta- MOF nanoparticles based on Minimum Inhibitory Concentration, Minimum Fungicidal Concentration and Minimum Bactericidal Concentration were evaluated. The synthesized Ta- MOF, in addition to high catalytic properties, showed high antimicrobial activity with MIC value between 16 and −256 μg/ml, and can be introduced as an agent against bacteria and fungi. |
| first_indexed | 2024-04-12T03:01:25Z |
| format | Article |
| id | doaj.art-1d8d8c19511142bcb50f72905d729e16 |
| institution | Directory Open Access Journal |
| issn | 2296-2646 |
| language | English |
| last_indexed | 2024-04-12T03:01:25Z |
| publishDate | 2022-09-01 |
| publisher | Frontiers Media S.A. |
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| series | Frontiers in Chemistry |
| spelling | doaj.art-1d8d8c19511142bcb50f72905d729e162022-12-22T03:50:38ZengFrontiers Media S.A.Frontiers in Chemistry2296-26462022-09-011010.3389/fchem.2022.967111967111Synthesis and characterization of new 1,4-dihydropyran derivatives by novel Ta-MOF nanostructures as reusable nanocatalyst with antimicrobial activityIrfan Ahmad0Saade Abdalkareem Jasim1Ghulam Yasin2Basim Al-Qargholi3Ali Thaeer Hammid4Department of Clinical Laboratory Sciences, College of Applied Medical Sciences, King Khalid University, Abha, Saudi ArabiaMedical Laboratory Techniques Department, Al-maarif University College, Al-anbar-Ramadi, IraqDepartment of Botany, Bahauddin Zakariya University, Multan, PakistanDepartment of Biomedical Engineering, Al-Mustaqbal University College, Babylon, IraqComputer Engineering Techniques Department, Faculty of Information Technology, Imam Ja’afar Al-Sadiq University, Baghdad, IraqNovel Ta- MOF was synthesized under mild conditions by ultrasound irradiations. The sample was characterized by SEM, FTIR, XRD, XPS, TG and BET technique. The final structures showed high physicho-chemical properties including narrow particle size distribution, homogenous morphology, high thermal stability and remarkable surface area. Ta- MOF synthesized in this study was used as a catalyst in the synthesis of 1,4-dihydropyran derivatives. The results proved that it has a high catalyst capability. Its advantages include high recyclability, less reaction time with higher efficiency and synthesis of new1,4-dihydropyran derivatives. In the following, antimicrobial activity including antifungal and antibacterial activity of Ta- MOF nanoparticles based on Minimum Inhibitory Concentration, Minimum Fungicidal Concentration and Minimum Bactericidal Concentration were evaluated. The synthesized Ta- MOF, in addition to high catalytic properties, showed high antimicrobial activity with MIC value between 16 and −256 μg/ml, and can be introduced as an agent against bacteria and fungi.https://www.frontiersin.org/articles/10.3389/fchem.2022.967111/fullmulticomponent reaction14-dihydropyranTa-MOF nanostructuresreusable nanocatalystantimicrobial activity |
| spellingShingle | Irfan Ahmad Saade Abdalkareem Jasim Ghulam Yasin Basim Al-Qargholi Ali Thaeer Hammid Synthesis and characterization of new 1,4-dihydropyran derivatives by novel Ta-MOF nanostructures as reusable nanocatalyst with antimicrobial activity Frontiers in Chemistry multicomponent reaction 1 4-dihydropyran Ta-MOF nanostructures reusable nanocatalyst antimicrobial activity |
| title | Synthesis and characterization of new 1,4-dihydropyran derivatives by novel Ta-MOF nanostructures as reusable nanocatalyst with antimicrobial activity |
| title_full | Synthesis and characterization of new 1,4-dihydropyran derivatives by novel Ta-MOF nanostructures as reusable nanocatalyst with antimicrobial activity |
| title_fullStr | Synthesis and characterization of new 1,4-dihydropyran derivatives by novel Ta-MOF nanostructures as reusable nanocatalyst with antimicrobial activity |
| title_full_unstemmed | Synthesis and characterization of new 1,4-dihydropyran derivatives by novel Ta-MOF nanostructures as reusable nanocatalyst with antimicrobial activity |
| title_short | Synthesis and characterization of new 1,4-dihydropyran derivatives by novel Ta-MOF nanostructures as reusable nanocatalyst with antimicrobial activity |
| title_sort | synthesis and characterization of new 1 4 dihydropyran derivatives by novel ta mof nanostructures as reusable nanocatalyst with antimicrobial activity |
| topic | multicomponent reaction 1 4-dihydropyran Ta-MOF nanostructures reusable nanocatalyst antimicrobial activity |
| url | https://www.frontiersin.org/articles/10.3389/fchem.2022.967111/full |
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