Utilization of Areca Nut Leaf Sheath Fibers for the Extraction of Cellulose Whiskers

In this study, cellulose whiskers were extracted from an agricultural plant waste, Areca Nut Leaf Sheath, by employing a sulfuric acid hydrolysis method. The effect of hydrolysis time and temperature on the morphology, crystallinity, and degree of polymerization of the resultant cellulose particles...

Full description

Bibliographic Details
Main Authors: Silviya Elanthikkal, Tania Francis, Sultan Akhtar
Format: Article
Language:English
Published: Taylor & Francis Group 2021-09-01
Series:Journal of Natural Fibers
Subjects:
Online Access:http://dx.doi.org/10.1080/15440478.2019.1689885
_version_ 1797680206083784704
author Silviya Elanthikkal
Tania Francis
Sultan Akhtar
author_facet Silviya Elanthikkal
Tania Francis
Sultan Akhtar
author_sort Silviya Elanthikkal
collection DOAJ
description In this study, cellulose whiskers were extracted from an agricultural plant waste, Areca Nut Leaf Sheath, by employing a sulfuric acid hydrolysis method. The effect of hydrolysis time and temperature on the morphology, crystallinity, and degree of polymerization of the resultant cellulose particles was studied. Highly crystalline cellulose whiskers with an aspect ratio around 20 were obtained under moderate conditions of hydrolysis by maintaining the temperature at 45°C and hydrolysis time of 180 min. However, on increasing the temperature and time of hydrolysis, surface flattening of fibers was observed and aspect ratio was decreased. Isolated cellulose whiskers were found to contain traces of biosilica.
first_indexed 2024-03-11T23:26:20Z
format Article
id doaj.art-1da8a1c5ca3c4dc6894b1d468007b52a
institution Directory Open Access Journal
issn 1544-0478
1544-046X
language English
last_indexed 2024-03-11T23:26:20Z
publishDate 2021-09-01
publisher Taylor & Francis Group
record_format Article
series Journal of Natural Fibers
spelling doaj.art-1da8a1c5ca3c4dc6894b1d468007b52a2023-09-20T12:50:17ZengTaylor & Francis GroupJournal of Natural Fibers1544-04781544-046X2021-09-011891261127310.1080/15440478.2019.16898851689885Utilization of Areca Nut Leaf Sheath Fibers for the Extraction of Cellulose WhiskersSilviya Elanthikkal0Tania Francis1Sultan Akhtar2Imam Abdulrahman Bin Faisal UniversitySt. Joseph’s College (Autonomous), DevagiriImam Abdulrahman Bin Faisal UniversityIn this study, cellulose whiskers were extracted from an agricultural plant waste, Areca Nut Leaf Sheath, by employing a sulfuric acid hydrolysis method. The effect of hydrolysis time and temperature on the morphology, crystallinity, and degree of polymerization of the resultant cellulose particles was studied. Highly crystalline cellulose whiskers with an aspect ratio around 20 were obtained under moderate conditions of hydrolysis by maintaining the temperature at 45°C and hydrolysis time of 180 min. However, on increasing the temperature and time of hydrolysis, surface flattening of fibers was observed and aspect ratio was decreased. Isolated cellulose whiskers were found to contain traces of biosilica.http://dx.doi.org/10.1080/15440478.2019.1689885areca nut leaf sheath fiberscellulose whiskersacid hydrolysiseffect of hydrolysis conditionsdegree of polymerizationbiosilica
spellingShingle Silviya Elanthikkal
Tania Francis
Sultan Akhtar
Utilization of Areca Nut Leaf Sheath Fibers for the Extraction of Cellulose Whiskers
Journal of Natural Fibers
areca nut leaf sheath fibers
cellulose whiskers
acid hydrolysis
effect of hydrolysis conditions
degree of polymerization
biosilica
title Utilization of Areca Nut Leaf Sheath Fibers for the Extraction of Cellulose Whiskers
title_full Utilization of Areca Nut Leaf Sheath Fibers for the Extraction of Cellulose Whiskers
title_fullStr Utilization of Areca Nut Leaf Sheath Fibers for the Extraction of Cellulose Whiskers
title_full_unstemmed Utilization of Areca Nut Leaf Sheath Fibers for the Extraction of Cellulose Whiskers
title_short Utilization of Areca Nut Leaf Sheath Fibers for the Extraction of Cellulose Whiskers
title_sort utilization of areca nut leaf sheath fibers for the extraction of cellulose whiskers
topic areca nut leaf sheath fibers
cellulose whiskers
acid hydrolysis
effect of hydrolysis conditions
degree of polymerization
biosilica
url http://dx.doi.org/10.1080/15440478.2019.1689885
work_keys_str_mv AT silviyaelanthikkal utilizationofarecanutleafsheathfibersfortheextractionofcellulosewhiskers
AT taniafrancis utilizationofarecanutleafsheathfibersfortheextractionofcellulosewhiskers
AT sultanakhtar utilizationofarecanutleafsheathfibersfortheextractionofcellulosewhiskers