Study of gypsum composites with fine solid aggregates at elevated temperatures

The structure and behaviour of two gypsum composites after exposition to elevated temperatures were investigated. The silica sand and fine basalt aggregate were used as solid fillers. The changes in structure and composition at temperatures from 50 to 1,000°C were investigated by scanning electron m...

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Main Authors: Doleželová Magdaléna, Scheinherrová Lenka, Vimmrová Alena
Format: Article
Language:English
Published: De Gruyter 2021-05-01
Series:Science and Engineering of Composite Materials
Subjects:
Online Access:https://doi.org/10.1515/secm-2021-0025
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author Doleželová Magdaléna
Scheinherrová Lenka
Vimmrová Alena
author_facet Doleželová Magdaléna
Scheinherrová Lenka
Vimmrová Alena
author_sort Doleželová Magdaléna
collection DOAJ
description The structure and behaviour of two gypsum composites after exposition to elevated temperatures were investigated. The silica sand and fine basalt aggregate were used as solid fillers. The changes in structure and composition at temperatures from 50 to 1,000°C were investigated by scanning electron microscopy and X-ray diffraction together with the size and strength of the samples and their pore size distribution. The structure of gypsum matrix changed significantly at 1,000°C in both composites, while the aggregate particles were not changed. It was found that even if the silica sand is considered as less suitable filler at high temperatures because of its volume changes, the gypsum with sand performed better than gypsum with basalt at the highest temperatures, because the shrinkage of the gypsum matrix was compensated by the increase in the volume of aggregate. The final volume change at 1,000°C was 3.5% in composite with silica sand and 6.8% in composite with basalt. The residual compressive strength of both composites was about 9.4%. No cracks appeared in the samples and no spalling was observed.
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spelling doaj.art-1ea1ce92bef04cd7a5556a455afcd9eb2022-12-21T19:24:29ZengDe GruyterScience and Engineering of Composite Materials2191-03592021-05-0128123724810.1515/secm-2021-0025Study of gypsum composites with fine solid aggregates at elevated temperaturesDoleželová Magdaléna0Scheinherrová Lenka1Vimmrová Alena2Department of Material Engineering and Chemistry, Faculty of Civil Engineering, Czech Technical University in Prague, Thakurova 7, 166 29 Prague 6, Czech RepublicDepartment of Material Engineering and Chemistry, Faculty of Civil Engineering, Czech Technical University in Prague, Thakurova 7, 166 29 Prague 6, Czech RepublicDepartment of Material Engineering and Chemistry, Faculty of Civil Engineering, Czech Technical University in Prague, Thakurova 7, 166 29 Prague 6, Czech RepublicThe structure and behaviour of two gypsum composites after exposition to elevated temperatures were investigated. The silica sand and fine basalt aggregate were used as solid fillers. The changes in structure and composition at temperatures from 50 to 1,000°C were investigated by scanning electron microscopy and X-ray diffraction together with the size and strength of the samples and their pore size distribution. The structure of gypsum matrix changed significantly at 1,000°C in both composites, while the aggregate particles were not changed. It was found that even if the silica sand is considered as less suitable filler at high temperatures because of its volume changes, the gypsum with sand performed better than gypsum with basalt at the highest temperatures, because the shrinkage of the gypsum matrix was compensated by the increase in the volume of aggregate. The final volume change at 1,000°C was 3.5% in composite with silica sand and 6.8% in composite with basalt. The residual compressive strength of both composites was about 9.4%. No cracks appeared in the samples and no spalling was observed.https://doi.org/10.1515/secm-2021-0025gypsum compositeelevated temperaturesmicrostructureporosityproperties
spellingShingle Doleželová Magdaléna
Scheinherrová Lenka
Vimmrová Alena
Study of gypsum composites with fine solid aggregates at elevated temperatures
Science and Engineering of Composite Materials
gypsum composite
elevated temperatures
microstructure
porosity
properties
title Study of gypsum composites with fine solid aggregates at elevated temperatures
title_full Study of gypsum composites with fine solid aggregates at elevated temperatures
title_fullStr Study of gypsum composites with fine solid aggregates at elevated temperatures
title_full_unstemmed Study of gypsum composites with fine solid aggregates at elevated temperatures
title_short Study of gypsum composites with fine solid aggregates at elevated temperatures
title_sort study of gypsum composites with fine solid aggregates at elevated temperatures
topic gypsum composite
elevated temperatures
microstructure
porosity
properties
url https://doi.org/10.1515/secm-2021-0025
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