Preparation and characterisation of graphitic biochar materials derived from rose oil industry waste via different pyrolysis durations and ball milling for advanced composites
The valorisation of waste from rose-based industrial products produces value-added substances and paves the way for advanced composites. The rose waste generated from the essential oil industry of the Taif rose ( Rosa damascena trigintipetala Dieck) is significant, and its management or disposal is...
| Main Authors: | , , , , , , |
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| Format: | Article |
| Language: | English |
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IOP Publishing
2024-01-01
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| Series: | Materials Research Express |
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| Online Access: | https://doi.org/10.1088/2053-1591/ad3523 |
| _version_ | 1797236839861452800 |
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| author | Saleh M Alluqmani Hissah Saedoon Albaqawi Musaed A Hakami Nadiyah M Alabdallah Hana M Almarri Asla A AL-Zahrani Ahmed Alshahrie |
| author_facet | Saleh M Alluqmani Hissah Saedoon Albaqawi Musaed A Hakami Nadiyah M Alabdallah Hana M Almarri Asla A AL-Zahrani Ahmed Alshahrie |
| author_sort | Saleh M Alluqmani |
| collection | DOAJ |
| description | The valorisation of waste from rose-based industrial products produces value-added substances and paves the way for advanced composites. The rose waste generated from the essential oil industry of the Taif rose ( Rosa damascena trigintipetala Dieck) is significant, and its management or disposal is a source of concern. In this study, it was valorised to produce a value-added nanomaterial. The synthesis of biochar nanoparticles via high-energy ball milling has gained tremendous research interest in recent times because of its low cost and eco-friendliness. Ball milling is a solvent-free technology with strong potential for waste volatilisation and eco-sustainability through the production of engineered biochar nanoparticles. Different biochar samples were produced and characterised to harness the synergistic combination of biochar production and ball milling. They were prepared at a constant pyrolysis temperature of 300 °C by varying the pyrolysis times for 2 h, 5 h, and 10 h. The characterisation results showed that pyrolysis confirms a high content of carbon, minerals, graphitic structure, novel morphology and chemical characteristics attached to the biochar surface controlled by different pyrolysis durations. These properties were further enhanced by ball milling for 10 h. The results showed that ball milling enhanced the porosity, surface area, surface functional groups, visible light absorption, crystallinity, and carbon content, and these were accompanied by a reduction in the particle size and mineral impurities. The engineered biochar can be an important tool, with promising potential in novel composites for water purification and energy harvesting. |
| first_indexed | 2024-04-24T17:10:14Z |
| format | Article |
| id | doaj.art-1eeae72cfdc347af878b3c2f00ee9fcb |
| institution | Directory Open Access Journal |
| issn | 2053-1591 |
| language | English |
| last_indexed | 2024-04-24T17:10:14Z |
| publishDate | 2024-01-01 |
| publisher | IOP Publishing |
| record_format | Article |
| series | Materials Research Express |
| spelling | doaj.art-1eeae72cfdc347af878b3c2f00ee9fcb2024-03-28T11:52:32ZengIOP PublishingMaterials Research Express2053-15912024-01-0111303500510.1088/2053-1591/ad3523Preparation and characterisation of graphitic biochar materials derived from rose oil industry waste via different pyrolysis durations and ball milling for advanced compositesSaleh M Alluqmani0https://orcid.org/0000-0001-6364-0185Hissah Saedoon Albaqawi1https://orcid.org/0000-0001-6408-0343Musaed A Hakami2Nadiyah M Alabdallah3https://orcid.org/0000-0002-1970-8792Hana M Almarri4https://orcid.org/0000-0003-3837-8255Asla A AL-Zahrani5https://orcid.org/0000-0003-4311-633XAhmed Alshahrie6Department of Physic, College of Science, Umm Al-Qura University , PO Box 715, Makkah 24382, Saudi ArabiaDepartment of Physics, College of Science, University Ha’il , PO Box 2440, Ha’il 8145, Saudi ArabiaDepartment of Physic, College of Science, Umm Al-Qura University , PO Box 715, Makkah 24382, Saudi ArabiaDepartment of Biology, College of Science, Imam Abdulrahman Bin Faisal University , PO Box 1982, Dammam 31441, Saudi Arabia; Basic and Applied Scientific Research Center- College of Science, Imam Abdulrahman Bin Faisal University , PO Box 1982, Dammam, 31441, Saudi ArabiaBasic and Applied Scientific Research Center- College of Science, Imam Abdulrahman Bin Faisal University , PO Box 1982, Dammam, 31441, Saudi Arabia; Department of Physics, College of Science, Imam Abdulrahman Bin Faisal University , PO Box 1982, Dammam 31441, Saudi ArabiaBasic and Applied Scientific Research Center- College of Science, Imam Abdulrahman Bin Faisal University , PO Box 1982, Dammam, 31441, Saudi Arabia; Department of Chemistry, College of Science, Imam Abdulrahman Bin Faisal University , PO Box 1982, Dammam 31441, Saudi ArabiaCenter of Nanotechnology, King Abdulaziz University , Jeddah 21589, Saudi Arabia; Department of Physics, Faculty of Sciences, King Abdulaziz University , Jeddah 21589, Saudi ArabiaThe valorisation of waste from rose-based industrial products produces value-added substances and paves the way for advanced composites. The rose waste generated from the essential oil industry of the Taif rose ( Rosa damascena trigintipetala Dieck) is significant, and its management or disposal is a source of concern. In this study, it was valorised to produce a value-added nanomaterial. The synthesis of biochar nanoparticles via high-energy ball milling has gained tremendous research interest in recent times because of its low cost and eco-friendliness. Ball milling is a solvent-free technology with strong potential for waste volatilisation and eco-sustainability through the production of engineered biochar nanoparticles. Different biochar samples were produced and characterised to harness the synergistic combination of biochar production and ball milling. They were prepared at a constant pyrolysis temperature of 300 °C by varying the pyrolysis times for 2 h, 5 h, and 10 h. The characterisation results showed that pyrolysis confirms a high content of carbon, minerals, graphitic structure, novel morphology and chemical characteristics attached to the biochar surface controlled by different pyrolysis durations. These properties were further enhanced by ball milling for 10 h. The results showed that ball milling enhanced the porosity, surface area, surface functional groups, visible light absorption, crystallinity, and carbon content, and these were accompanied by a reduction in the particle size and mineral impurities. The engineered biochar can be an important tool, with promising potential in novel composites for water purification and energy harvesting.https://doi.org/10.1088/2053-1591/ad3523Biocharrose oil industry wastegraphitic carbonpyrolysiscarbon nanostructurehigh-energy ball-milling |
| spellingShingle | Saleh M Alluqmani Hissah Saedoon Albaqawi Musaed A Hakami Nadiyah M Alabdallah Hana M Almarri Asla A AL-Zahrani Ahmed Alshahrie Preparation and characterisation of graphitic biochar materials derived from rose oil industry waste via different pyrolysis durations and ball milling for advanced composites Materials Research Express Biochar rose oil industry waste graphitic carbon pyrolysis carbon nanostructure high-energy ball-milling |
| title | Preparation and characterisation of graphitic biochar materials derived from rose oil industry waste via different pyrolysis durations and ball milling for advanced composites |
| title_full | Preparation and characterisation of graphitic biochar materials derived from rose oil industry waste via different pyrolysis durations and ball milling for advanced composites |
| title_fullStr | Preparation and characterisation of graphitic biochar materials derived from rose oil industry waste via different pyrolysis durations and ball milling for advanced composites |
| title_full_unstemmed | Preparation and characterisation of graphitic biochar materials derived from rose oil industry waste via different pyrolysis durations and ball milling for advanced composites |
| title_short | Preparation and characterisation of graphitic biochar materials derived from rose oil industry waste via different pyrolysis durations and ball milling for advanced composites |
| title_sort | preparation and characterisation of graphitic biochar materials derived from rose oil industry waste via different pyrolysis durations and ball milling for advanced composites |
| topic | Biochar rose oil industry waste graphitic carbon pyrolysis carbon nanostructure high-energy ball-milling |
| url | https://doi.org/10.1088/2053-1591/ad3523 |
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