4-[(1-Hydroxy-2-naphthyl)methyleneamino]-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one
The title antipyrine derivative, C22H19N3O2, was synthesized by the reaction of 4-amino-1,5-dimethyl-2-phenyl-1,2-dihydropyrazol-3-one and 1-hydroxynaphthalene-2-carbaldehyde in methanol solution. As expected, the compound adopts a trans configuration about the central C=N bond. The N atom is involv...
| Main Authors: | , |
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| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2010-08-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536810026450 |
| _version_ | 1828884698827325440 |
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| author | Qiang Liang Qian Wang |
| author_facet | Qiang Liang Qian Wang |
| author_sort | Qiang Liang |
| collection | DOAJ |
| description | The title antipyrine derivative, C22H19N3O2, was synthesized by the reaction of 4-amino-1,5-dimethyl-2-phenyl-1,2-dihydropyrazol-3-one and 1-hydroxynaphthalene-2-carbaldehyde in methanol solution. As expected, the compound adopts a trans configuration about the central C=N bond. The N atom is involved in an intramolecular O—H...N bond which stabilizes the molecular configuration. In the crystal structure, adjacent molecules stack with no short contacts. |
| first_indexed | 2024-12-13T11:12:59Z |
| format | Article |
| id | doaj.art-1f68fc5918514a76adb3bd969018a610 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-13T11:12:59Z |
| publishDate | 2010-08-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-1f68fc5918514a76adb3bd969018a6102022-12-21T23:48:42ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-08-01668o1968o196910.1107/S16005368100264504-[(1-Hydroxy-2-naphthyl)methyleneamino]-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-oneQiang LiangQian WangThe title antipyrine derivative, C22H19N3O2, was synthesized by the reaction of 4-amino-1,5-dimethyl-2-phenyl-1,2-dihydropyrazol-3-one and 1-hydroxynaphthalene-2-carbaldehyde in methanol solution. As expected, the compound adopts a trans configuration about the central C=N bond. The N atom is involved in an intramolecular O—H...N bond which stabilizes the molecular configuration. In the crystal structure, adjacent molecules stack with no short contacts.http://scripts.iucr.org/cgi-bin/paper?S1600536810026450 |
| spellingShingle | Qiang Liang Qian Wang 4-[(1-Hydroxy-2-naphthyl)methyleneamino]-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one Acta Crystallographica Section E |
| title | 4-[(1-Hydroxy-2-naphthyl)methyleneamino]-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one |
| title_full | 4-[(1-Hydroxy-2-naphthyl)methyleneamino]-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one |
| title_fullStr | 4-[(1-Hydroxy-2-naphthyl)methyleneamino]-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one |
| title_full_unstemmed | 4-[(1-Hydroxy-2-naphthyl)methyleneamino]-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one |
| title_short | 4-[(1-Hydroxy-2-naphthyl)methyleneamino]-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one |
| title_sort | 4 1 hydroxy 2 naphthyl methyleneamino 1 5 dimethyl 2 phenyl 1h pyrazol 3 2h one |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536810026450 |
| work_keys_str_mv | AT qiangliang 41hydroxy2naphthylmethyleneamino15dimethyl2phenyl1hpyrazol32hone AT qianwang 41hydroxy2naphthylmethyleneamino15dimethyl2phenyl1hpyrazol32hone |