EFFECT OF SPINEL ADDITION ON THE SINTERING BEHAVIOR AND MICROSTRUCTURE OF ALUMINA-SPINEL CERAMICS

Sintering behaviors of alumina-spinel powder mixtures were investigated up to 1600oC using a vertical dilatometer. Final density and microstructure of pure alumina, magnesium aluminate spinel (MgAl2O4) ceramics and ceramic composites with different alumina-spinel ratio were examined. As a result, th...

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Main Author: Emre Yalamac
Format: Article
Language:English
Published: University of Chemistry and Technology, Prague 2014-12-01
Series:Ceramics-Silikáty
Subjects:
Online Access: http://www.ceramics-silikaty.cz/2014/pdf/2014_04_314.pdf
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author Emre Yalamac
author_facet Emre Yalamac
author_sort Emre Yalamac
collection DOAJ
description Sintering behaviors of alumina-spinel powder mixtures were investigated up to 1600oC using a vertical dilatometer. Final density and microstructure of pure alumina, magnesium aluminate spinel (MgAl2O4) ceramics and ceramic composites with different alumina-spinel ratio were examined. As a result, the densification and final density of alumina-spinel composites were affected by addition of 10 wt. % and 20 wt. % spinel into alumina. Non-stoichiometric alumina-rich spinel phase was detected in the matrix of the composites by EDS. The presence of spinel phase inhibited alumina grain growth, therefore the pure alumina sample had nearly twice the grain size as the multiphase alumina-spinel samples. Vickers hardness of the samples was tested and compared. The hardness of the composite with 10 wt. % spinel was slightly higher than the pure alumina ceramic, due to grain size and density of the samples.
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spelling doaj.art-1f7ed39aeaa04d1ba745073ef1a7369e2022-12-21T19:56:54ZengUniversity of Chemistry and Technology, PragueCeramics-Silikáty0862-54681804-58472014-12-01584314319.20160312095943EFFECT OF SPINEL ADDITION ON THE SINTERING BEHAVIOR AND MICROSTRUCTURE OF ALUMINA-SPINEL CERAMICSEmre Yalamac0 Celal Bayar University, Department of Materials Engineering, 45140 Manisa, Turkey Sintering behaviors of alumina-spinel powder mixtures were investigated up to 1600oC using a vertical dilatometer. Final density and microstructure of pure alumina, magnesium aluminate spinel (MgAl2O4) ceramics and ceramic composites with different alumina-spinel ratio were examined. As a result, the densification and final density of alumina-spinel composites were affected by addition of 10 wt. % and 20 wt. % spinel into alumina. Non-stoichiometric alumina-rich spinel phase was detected in the matrix of the composites by EDS. The presence of spinel phase inhibited alumina grain growth, therefore the pure alumina sample had nearly twice the grain size as the multiphase alumina-spinel samples. Vickers hardness of the samples was tested and compared. The hardness of the composite with 10 wt. % spinel was slightly higher than the pure alumina ceramic, due to grain size and density of the samples. http://www.ceramics-silikaty.cz/2014/pdf/2014_04_314.pdf Alumina Magnesium Aluminate Spinel Ceramic Composite Densification Hardness
spellingShingle Emre Yalamac
EFFECT OF SPINEL ADDITION ON THE SINTERING BEHAVIOR AND MICROSTRUCTURE OF ALUMINA-SPINEL CERAMICS
Ceramics-Silikáty
Alumina
Magnesium Aluminate Spinel
Ceramic Composite
Densification
Hardness
title EFFECT OF SPINEL ADDITION ON THE SINTERING BEHAVIOR AND MICROSTRUCTURE OF ALUMINA-SPINEL CERAMICS
title_full EFFECT OF SPINEL ADDITION ON THE SINTERING BEHAVIOR AND MICROSTRUCTURE OF ALUMINA-SPINEL CERAMICS
title_fullStr EFFECT OF SPINEL ADDITION ON THE SINTERING BEHAVIOR AND MICROSTRUCTURE OF ALUMINA-SPINEL CERAMICS
title_full_unstemmed EFFECT OF SPINEL ADDITION ON THE SINTERING BEHAVIOR AND MICROSTRUCTURE OF ALUMINA-SPINEL CERAMICS
title_short EFFECT OF SPINEL ADDITION ON THE SINTERING BEHAVIOR AND MICROSTRUCTURE OF ALUMINA-SPINEL CERAMICS
title_sort effect of spinel addition on the sintering behavior and microstructure of alumina spinel ceramics
topic Alumina
Magnesium Aluminate Spinel
Ceramic Composite
Densification
Hardness
url http://www.ceramics-silikaty.cz/2014/pdf/2014_04_314.pdf
work_keys_str_mv AT emreyalamac effectofspineladditiononthesinteringbehaviorandmicrostructureofaluminaspinelceramics