Multi-material additive manufacturing of low sintering temperature Bi2Mo2O9 ceramics with Ag floating electrodes by selective laser burnout

Additive manufacturing (AM) of co-fired low temperature ceramics offers a unique route for fabrication of novel 3D radio frequency (RF) and microwave communication components, embedded electronics and sensors. This paper describes the first-ever direct 3D printing of low temperature co-fired ceramic...

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Main Authors: Reza Gheisari, Henry Chamberlain, George Chi-Tangyie, Shiyu Zhang, Athanasios Goulas, Chih-Kuo Lee, Tom Whittaker, Dawei Wang, Annapoorani Ketharam, Avishek Ghosh, Bala Vaidhyanathan, Will Whittow, Darren Cadman, Yiannis C. Vardaxoglou, Ian M. Reaney, Daniel S. Engstrøm
Format: Article
Language:English
Published: Taylor & Francis Group 2020-04-01
Series:Virtual and Physical Prototyping
Subjects:
Online Access:http://dx.doi.org/10.1080/17452759.2019.1708026
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author Reza Gheisari
Henry Chamberlain
George Chi-Tangyie
Shiyu Zhang
Athanasios Goulas
Chih-Kuo Lee
Tom Whittaker
Dawei Wang
Annapoorani Ketharam
Avishek Ghosh
Bala Vaidhyanathan
Will Whittow
Darren Cadman
Yiannis C. Vardaxoglou
Ian M. Reaney
Daniel S. Engstrøm
author_facet Reza Gheisari
Henry Chamberlain
George Chi-Tangyie
Shiyu Zhang
Athanasios Goulas
Chih-Kuo Lee
Tom Whittaker
Dawei Wang
Annapoorani Ketharam
Avishek Ghosh
Bala Vaidhyanathan
Will Whittow
Darren Cadman
Yiannis C. Vardaxoglou
Ian M. Reaney
Daniel S. Engstrøm
author_sort Reza Gheisari
collection DOAJ
description Additive manufacturing (AM) of co-fired low temperature ceramics offers a unique route for fabrication of novel 3D radio frequency (RF) and microwave communication components, embedded electronics and sensors. This paper describes the first-ever direct 3D printing of low temperature co-fired ceramics/floating electrode 3D structures. Slurry-based AM and selective laser burnout (SLB) were used to fabricate bulk dielectric, Bi2Mo2O9 (BMO, sintering temperature = 620–650°C, εr = 38) with silver (Ag) internal floating electrodes. A printable BMO slurry was developed and the SLB optimised to improve edge definition and burn out the binder without damaging the ceramic. The SLB increased the green strength needed for shape retention, produced crack-free parts and prevented Ag leaching into the ceramic during co-firing. The green parts were sintered after SLB in a conventional furnace at 645°C for 4 h and achieved 94.5% density, compressive strength of 4097 MPa, a relative permittivity (εr) of 33.8 and a loss tangent (tan δ) of 0.0004 (8 GHz) for BMO. The feasibility of using SLB followed by a post-printing sintering step to create BMO/Ag 3D structures was thus demonstrated.
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spelling doaj.art-20dbbd66c03140728f91e65344c04e8a2023-09-21T14:38:01ZengTaylor & Francis GroupVirtual and Physical Prototyping1745-27591745-27672020-04-0115213314710.1080/17452759.2019.17080261708026Multi-material additive manufacturing of low sintering temperature Bi2Mo2O9 ceramics with Ag floating electrodes by selective laser burnoutReza Gheisari0Henry Chamberlain1George Chi-Tangyie2Shiyu Zhang3Athanasios Goulas4Chih-Kuo Lee5Tom Whittaker6Dawei Wang7Annapoorani Ketharam8Avishek Ghosh9Bala Vaidhyanathan10Will Whittow11Darren Cadman12Yiannis C. Vardaxoglou13Ian M. Reaney14Daniel S. Engstrøm15Loughborough UniversityLoughborough UniversityLoughborough UniversityLoughborough UniversityLoughborough UniversityLoughborough UniversityLoughborough UniversityUniversity of SheffieldLoughborough UniversityLoughborough UniversityLoughborough UniversityLoughborough UniversityLoughborough UniversityLoughborough UniversityUniversity of SheffieldLoughborough UniversityAdditive manufacturing (AM) of co-fired low temperature ceramics offers a unique route for fabrication of novel 3D radio frequency (RF) and microwave communication components, embedded electronics and sensors. This paper describes the first-ever direct 3D printing of low temperature co-fired ceramics/floating electrode 3D structures. Slurry-based AM and selective laser burnout (SLB) were used to fabricate bulk dielectric, Bi2Mo2O9 (BMO, sintering temperature = 620–650°C, εr = 38) with silver (Ag) internal floating electrodes. A printable BMO slurry was developed and the SLB optimised to improve edge definition and burn out the binder without damaging the ceramic. The SLB increased the green strength needed for shape retention, produced crack-free parts and prevented Ag leaching into the ceramic during co-firing. The green parts were sintered after SLB in a conventional furnace at 645°C for 4 h and achieved 94.5% density, compressive strength of 4097 MPa, a relative permittivity (εr) of 33.8 and a loss tangent (tan δ) of 0.0004 (8 GHz) for BMO. The feasibility of using SLB followed by a post-printing sintering step to create BMO/Ag 3D structures was thus demonstrated.http://dx.doi.org/10.1080/17452759.2019.1708026additive manufacturingmetamaterialsmulti-material 3d printingselective laser burnoutco-fired ceramics
spellingShingle Reza Gheisari
Henry Chamberlain
George Chi-Tangyie
Shiyu Zhang
Athanasios Goulas
Chih-Kuo Lee
Tom Whittaker
Dawei Wang
Annapoorani Ketharam
Avishek Ghosh
Bala Vaidhyanathan
Will Whittow
Darren Cadman
Yiannis C. Vardaxoglou
Ian M. Reaney
Daniel S. Engstrøm
Multi-material additive manufacturing of low sintering temperature Bi2Mo2O9 ceramics with Ag floating electrodes by selective laser burnout
Virtual and Physical Prototyping
additive manufacturing
metamaterials
multi-material 3d printing
selective laser burnout
co-fired ceramics
title Multi-material additive manufacturing of low sintering temperature Bi2Mo2O9 ceramics with Ag floating electrodes by selective laser burnout
title_full Multi-material additive manufacturing of low sintering temperature Bi2Mo2O9 ceramics with Ag floating electrodes by selective laser burnout
title_fullStr Multi-material additive manufacturing of low sintering temperature Bi2Mo2O9 ceramics with Ag floating electrodes by selective laser burnout
title_full_unstemmed Multi-material additive manufacturing of low sintering temperature Bi2Mo2O9 ceramics with Ag floating electrodes by selective laser burnout
title_short Multi-material additive manufacturing of low sintering temperature Bi2Mo2O9 ceramics with Ag floating electrodes by selective laser burnout
title_sort multi material additive manufacturing of low sintering temperature bi2mo2o9 ceramics with ag floating electrodes by selective laser burnout
topic additive manufacturing
metamaterials
multi-material 3d printing
selective laser burnout
co-fired ceramics
url http://dx.doi.org/10.1080/17452759.2019.1708026
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