[(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate

The title compound, C11H18N2S4, was unexpectedly obtained during studies on the reactivity of the complex tris(acac-κ2O,O′)gallium(III) (acac is acetylacetonate) with C4H8NCS2H in dichloromethane. The title compound shows disordered two pyrrolidine rings with major and min...

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Main Authors: Yen-Hsiang Huang, Hsiao-Fen Wang, Wei-Lung Chou, Kuang-Hway Yih, Gene-Hsiang Lee
Format: Article
Language:English
Published: International Union of Crystallography 2010-12-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536810046027
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author Yen-Hsiang Huang
Hsiao-Fen Wang
Wei-Lung Chou
Kuang-Hway Yih
Gene-Hsiang Lee
author_facet Yen-Hsiang Huang
Hsiao-Fen Wang
Wei-Lung Chou
Kuang-Hway Yih
Gene-Hsiang Lee
author_sort Yen-Hsiang Huang
collection DOAJ
description The title compound, C11H18N2S4, was unexpectedly obtained during studies on the reactivity of the complex tris(acac-κ2O,O′)gallium(III) (acac is acetylacetonate) with C4H8NCS2H in dichloromethane. The title compound shows disordered two pyrrolidine rings with major and minor occupancies of 0.546 (4) and 0.454 (4). Two (pyrrolidin-1-yl)carbothioylsulfanyl units are linked together through a methylene C atom and weak C—H...S interactions are found.
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spelling doaj.art-20de76bcaa4940f88fe329a2edc496b62022-12-21T19:28:52ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-12-016612o3193o319310.1107/S1600536810046027[(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioateYen-Hsiang HuangHsiao-Fen WangWei-Lung ChouKuang-Hway YihGene-Hsiang LeeThe title compound, C11H18N2S4, was unexpectedly obtained during studies on the reactivity of the complex tris(acac-κ2O,O′)gallium(III) (acac is acetylacetonate) with C4H8NCS2H in dichloromethane. The title compound shows disordered two pyrrolidine rings with major and minor occupancies of 0.546 (4) and 0.454 (4). Two (pyrrolidin-1-yl)carbothioylsulfanyl units are linked together through a methylene C atom and weak C—H...S interactions are found.http://scripts.iucr.org/cgi-bin/paper?S1600536810046027
spellingShingle Yen-Hsiang Huang
Hsiao-Fen Wang
Wei-Lung Chou
Kuang-Hway Yih
Gene-Hsiang Lee
[(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate
Acta Crystallographica Section E
title [(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate
title_full [(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate
title_fullStr [(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate
title_full_unstemmed [(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate
title_short [(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate
title_sort pyrrolidin 1 yl carbothioylsulfanyl methyl pyrrolidine 1 carbodithioate
url http://scripts.iucr.org/cgi-bin/paper?S1600536810046027
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AT weilungchou pyrrolidin1ylcarbothioylsulfanylmethylpyrrolidine1carbodithioate
AT kuanghwayyih pyrrolidin1ylcarbothioylsulfanylmethylpyrrolidine1carbodithioate
AT genehsianglee pyrrolidin1ylcarbothioylsulfanylmethylpyrrolidine1carbodithioate