[(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate
The title compound, C11H18N2S4, was unexpectedly obtained during studies on the reactivity of the complex tris(acac-κ2O,O′)gallium(III) (acac is acetylacetonate) with C4H8NCS2H in dichloromethane. The title compound shows disordered two pyrrolidine rings with major and min...
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Format: | Article |
Language: | English |
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International Union of Crystallography
2010-12-01
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Series: | Acta Crystallographica Section E |
Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536810046027 |
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author | Yen-Hsiang Huang Hsiao-Fen Wang Wei-Lung Chou Kuang-Hway Yih Gene-Hsiang Lee |
author_facet | Yen-Hsiang Huang Hsiao-Fen Wang Wei-Lung Chou Kuang-Hway Yih Gene-Hsiang Lee |
author_sort | Yen-Hsiang Huang |
collection | DOAJ |
description | The title compound, C11H18N2S4, was unexpectedly obtained during studies on the reactivity of the complex tris(acac-κ2O,O′)gallium(III) (acac is acetylacetonate) with C4H8NCS2H in dichloromethane. The title compound shows disordered two pyrrolidine rings with major and minor occupancies of 0.546 (4) and 0.454 (4). Two (pyrrolidin-1-yl)carbothioylsulfanyl units are linked together through a methylene C atom and weak C—H...S interactions are found. |
first_indexed | 2024-12-20T19:25:55Z |
format | Article |
id | doaj.art-20de76bcaa4940f88fe329a2edc496b6 |
institution | Directory Open Access Journal |
issn | 1600-5368 |
language | English |
last_indexed | 2024-12-20T19:25:55Z |
publishDate | 2010-12-01 |
publisher | International Union of Crystallography |
record_format | Article |
series | Acta Crystallographica Section E |
spelling | doaj.art-20de76bcaa4940f88fe329a2edc496b62022-12-21T19:28:52ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-12-016612o3193o319310.1107/S1600536810046027[(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioateYen-Hsiang HuangHsiao-Fen WangWei-Lung ChouKuang-Hway YihGene-Hsiang LeeThe title compound, C11H18N2S4, was unexpectedly obtained during studies on the reactivity of the complex tris(acac-κ2O,O′)gallium(III) (acac is acetylacetonate) with C4H8NCS2H in dichloromethane. The title compound shows disordered two pyrrolidine rings with major and minor occupancies of 0.546 (4) and 0.454 (4). Two (pyrrolidin-1-yl)carbothioylsulfanyl units are linked together through a methylene C atom and weak C—H...S interactions are found.http://scripts.iucr.org/cgi-bin/paper?S1600536810046027 |
spellingShingle | Yen-Hsiang Huang Hsiao-Fen Wang Wei-Lung Chou Kuang-Hway Yih Gene-Hsiang Lee [(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate Acta Crystallographica Section E |
title | [(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate |
title_full | [(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate |
title_fullStr | [(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate |
title_full_unstemmed | [(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate |
title_short | [(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate |
title_sort | pyrrolidin 1 yl carbothioylsulfanyl methyl pyrrolidine 1 carbodithioate |
url | http://scripts.iucr.org/cgi-bin/paper?S1600536810046027 |
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