Ethyl 5-methyl-4-oxo-3-phenyl-2-propylamino-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxylate
The title compound, C19H21N3O3S, was synthesized via the aza-Wittig reaction of functionalized iminophosphorane with phenyl isocyanate under mild conditions. In the molecule, the fused thienopyrimidine ring system is essentially planar, with a maximum deviation of 0.072 (2)&#81...
| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2009-09-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536809033595 |
| _version_ | 1819278018844033024 |
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| author | Ai-Hua Zheng Yan-Mei Ren Jing Xu |
| author_facet | Ai-Hua Zheng Yan-Mei Ren Jing Xu |
| author_sort | Ai-Hua Zheng |
| collection | DOAJ |
| description | The title compound, C19H21N3O3S, was synthesized via the aza-Wittig reaction of functionalized iminophosphorane with phenyl isocyanate under mild conditions. In the molecule, the fused thienopyrimidine ring system is essentially planar, with a maximum deviation of 0.072 (2) Å, and makes a dihedral angle of 60.11 (9)° with the phenyl ring. An intramolecular C—H...O hydrogen bond is present. The crystal packing is stabilized by intermolecular N—H...O and C—H...O hydrogen bonds. |
| first_indexed | 2024-12-24T00:05:20Z |
| format | Article |
| id | doaj.art-218b026e07724e05b0a64fe097fefba4 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-24T00:05:20Z |
| publishDate | 2009-09-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-218b026e07724e05b0a64fe097fefba42022-12-21T17:25:01ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-09-01659o2266o226610.1107/S1600536809033595Ethyl 5-methyl-4-oxo-3-phenyl-2-propylamino-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxylateAi-Hua ZhengYan-Mei RenJing XuThe title compound, C19H21N3O3S, was synthesized via the aza-Wittig reaction of functionalized iminophosphorane with phenyl isocyanate under mild conditions. In the molecule, the fused thienopyrimidine ring system is essentially planar, with a maximum deviation of 0.072 (2) Å, and makes a dihedral angle of 60.11 (9)° with the phenyl ring. An intramolecular C—H...O hydrogen bond is present. The crystal packing is stabilized by intermolecular N—H...O and C—H...O hydrogen bonds.http://scripts.iucr.org/cgi-bin/paper?S1600536809033595 |
| spellingShingle | Ai-Hua Zheng Yan-Mei Ren Jing Xu Ethyl 5-methyl-4-oxo-3-phenyl-2-propylamino-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxylate Acta Crystallographica Section E |
| title | Ethyl 5-methyl-4-oxo-3-phenyl-2-propylamino-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxylate |
| title_full | Ethyl 5-methyl-4-oxo-3-phenyl-2-propylamino-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxylate |
| title_fullStr | Ethyl 5-methyl-4-oxo-3-phenyl-2-propylamino-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxylate |
| title_full_unstemmed | Ethyl 5-methyl-4-oxo-3-phenyl-2-propylamino-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxylate |
| title_short | Ethyl 5-methyl-4-oxo-3-phenyl-2-propylamino-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxylate |
| title_sort | ethyl 5 methyl 4 oxo 3 phenyl 2 propylamino 3 4 dihydrothieno 2 3 d pyrimidine 6 carboxylate |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536809033595 |
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