Marginal Micro-Seal and Tensile Bond Strength of a Biopolymer Hybrid Layer Coupled with Dental Prosthesis Using a Primerless-Wet System
The aim of this study is to compare the marginal seal and tensile bond strength (TBS) of prostheses fixed to enamel-dentin using different adhesive systems. Resin-composite inlays directly fabricated from Class V cavities of extracted human molars/premolars and mini-dumbbell-shaped specimens of bond...
Main Authors: | , , |
---|---|
Format: | Article |
Language: | English |
Published: |
MDPI AG
2023-01-01
|
Series: | Polymers |
Subjects: | |
Online Access: | https://www.mdpi.com/2073-4360/15/2/283 |
_version_ | 1797437550215823360 |
---|---|
author | Morakot Piemjai Onusa Waleepitackdej Franklin Garcia-Godoy |
author_facet | Morakot Piemjai Onusa Waleepitackdej Franklin Garcia-Godoy |
author_sort | Morakot Piemjai |
collection | DOAJ |
description | The aim of this study is to compare the marginal seal and tensile bond strength (TBS) of prostheses fixed to enamel-dentin using different adhesive systems. Resin-composite inlays directly fabricated from Class V cavities of extracted human molars/premolars and mini-dumbbell-shaped specimens of bonded enamel-dentin were prepared for microleakage and tensile tests, respectively. Four adhesive systems were used: primerless-wet (1-1 etching for 10-, 30-, or 60-s, and 4-META/MMA-TBB), primer-moist (All-Bond2 + Duolink or Single-Bond2 + RelyX ARC), self-etch (AQ-Bond + Metafil FLO), and dry (Super-Bond C&B) bonding. Dye penetration distance and TBS data were recorded. Failure modes and characteristics of the tooth-resin interface were examined on the fractured specimens. All specimens in 10-, 30-, and 60-s etching primerless-wet, Super-Bond, and AQ-Bond had a microleakage-free tooth-resin interface. Primer-moist groups showed microleakage at the cementum/dentin-resin margin/interface. Significantly higher TBSs (<i>p</i> < 0.05) were recorded in primer-less-wet and Super-Bond groups with the consistent hybridized biopolymer layer after the chemical challenge and mixed failure in tooth structure, luting-resin, and at the PMMA-rod interface. There was no correlation between microleakage and TBS data (<i>p</i> = −0.148). A 1–3 µm hybrid layer created in the 10–60 s primerless-wet technique, producing complete micro-seal and higher tensile strength than enamel and cured 4-META/MMA-TBB, may enhance clinical performances like Super-Bond C&B, the sustainable luting resin. |
first_indexed | 2024-03-09T11:24:06Z |
format | Article |
id | doaj.art-218b9a43b124433fac7bb7867d16a09d |
institution | Directory Open Access Journal |
issn | 2073-4360 |
language | English |
last_indexed | 2024-03-09T11:24:06Z |
publishDate | 2023-01-01 |
publisher | MDPI AG |
record_format | Article |
series | Polymers |
spelling | doaj.art-218b9a43b124433fac7bb7867d16a09d2023-12-01T00:07:19ZengMDPI AGPolymers2073-43602023-01-0115228310.3390/polym15020283Marginal Micro-Seal and Tensile Bond Strength of a Biopolymer Hybrid Layer Coupled with Dental Prosthesis Using a Primerless-Wet SystemMorakot Piemjai0Onusa Waleepitackdej1Franklin Garcia-Godoy2Department of Prosthodontics, Faculty of Dentistry, Chulalongkorn University, Bangkok 10330, ThailandDepartment of Prosthodontics, Faculty of Dentistry, Chulalongkorn University, Bangkok 10330, ThailandDepartment of Bioscience Research, College of Dentistry, University of Tennessee Health Science Center, Memphis, TN 38163, USAThe aim of this study is to compare the marginal seal and tensile bond strength (TBS) of prostheses fixed to enamel-dentin using different adhesive systems. Resin-composite inlays directly fabricated from Class V cavities of extracted human molars/premolars and mini-dumbbell-shaped specimens of bonded enamel-dentin were prepared for microleakage and tensile tests, respectively. Four adhesive systems were used: primerless-wet (1-1 etching for 10-, 30-, or 60-s, and 4-META/MMA-TBB), primer-moist (All-Bond2 + Duolink or Single-Bond2 + RelyX ARC), self-etch (AQ-Bond + Metafil FLO), and dry (Super-Bond C&B) bonding. Dye penetration distance and TBS data were recorded. Failure modes and characteristics of the tooth-resin interface were examined on the fractured specimens. All specimens in 10-, 30-, and 60-s etching primerless-wet, Super-Bond, and AQ-Bond had a microleakage-free tooth-resin interface. Primer-moist groups showed microleakage at the cementum/dentin-resin margin/interface. Significantly higher TBSs (<i>p</i> < 0.05) were recorded in primer-less-wet and Super-Bond groups with the consistent hybridized biopolymer layer after the chemical challenge and mixed failure in tooth structure, luting-resin, and at the PMMA-rod interface. There was no correlation between microleakage and TBS data (<i>p</i> = −0.148). A 1–3 µm hybrid layer created in the 10–60 s primerless-wet technique, producing complete micro-seal and higher tensile strength than enamel and cured 4-META/MMA-TBB, may enhance clinical performances like Super-Bond C&B, the sustainable luting resin.https://www.mdpi.com/2073-4360/15/2/283primerless-wet bondingresin adhesive systemhybrid layertensile bond strengthmicro-sealluting resin |
spellingShingle | Morakot Piemjai Onusa Waleepitackdej Franklin Garcia-Godoy Marginal Micro-Seal and Tensile Bond Strength of a Biopolymer Hybrid Layer Coupled with Dental Prosthesis Using a Primerless-Wet System Polymers primerless-wet bonding resin adhesive system hybrid layer tensile bond strength micro-seal luting resin |
title | Marginal Micro-Seal and Tensile Bond Strength of a Biopolymer Hybrid Layer Coupled with Dental Prosthesis Using a Primerless-Wet System |
title_full | Marginal Micro-Seal and Tensile Bond Strength of a Biopolymer Hybrid Layer Coupled with Dental Prosthesis Using a Primerless-Wet System |
title_fullStr | Marginal Micro-Seal and Tensile Bond Strength of a Biopolymer Hybrid Layer Coupled with Dental Prosthesis Using a Primerless-Wet System |
title_full_unstemmed | Marginal Micro-Seal and Tensile Bond Strength of a Biopolymer Hybrid Layer Coupled with Dental Prosthesis Using a Primerless-Wet System |
title_short | Marginal Micro-Seal and Tensile Bond Strength of a Biopolymer Hybrid Layer Coupled with Dental Prosthesis Using a Primerless-Wet System |
title_sort | marginal micro seal and tensile bond strength of a biopolymer hybrid layer coupled with dental prosthesis using a primerless wet system |
topic | primerless-wet bonding resin adhesive system hybrid layer tensile bond strength micro-seal luting resin |
url | https://www.mdpi.com/2073-4360/15/2/283 |
work_keys_str_mv | AT morakotpiemjai marginalmicrosealandtensilebondstrengthofabiopolymerhybridlayercoupledwithdentalprosthesisusingaprimerlesswetsystem AT onusawaleepitackdej marginalmicrosealandtensilebondstrengthofabiopolymerhybridlayercoupledwithdentalprosthesisusingaprimerlesswetsystem AT franklingarciagodoy marginalmicrosealandtensilebondstrengthofabiopolymerhybridlayercoupledwithdentalprosthesisusingaprimerlesswetsystem |