Crystal structure of (E)-3-{[2-(2,4-dichlorobenzylidene)hydrazin-1-yl]carbonyl}pyridinium chloride trihydrate
In the title hydrated salt, C13H10Cl2N3O+·Cl−·3H2O, the organic cation exhibits a dihedral angle of 8.26 (14)° between the mean planes of the pyridinium and benzene rings, and dihedral angles of 8.70 (15) and 15.93 (5)° between the mean planes of the hydrazide group and the benzene and pyridinium ri...
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International Union of Crystallography
2015-02-01
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Series: | Acta Crystallographica Section E: Crystallographic Communications |
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Online Access: | http://scripts.iucr.org/cgi-bin/paper?S2056989015000286 |
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author | J. Josephine Novina G. Vasuki M. Suresh M. Syed Ali Padusha |
author_facet | J. Josephine Novina G. Vasuki M. Suresh M. Syed Ali Padusha |
author_sort | J. Josephine Novina |
collection | DOAJ |
description | In the title hydrated salt, C13H10Cl2N3O+·Cl−·3H2O, the organic cation exhibits a dihedral angle of 8.26 (14)° between the mean planes of the pyridinium and benzene rings, and dihedral angles of 8.70 (15) and 15.93 (5)° between the mean planes of the hydrazide group and the benzene and pyridinium rings, respectively. In the crystal, N—H...O, N—H...Cl, C—H...O, C—H...Cl, O—H...O, O—H...N and O—H...Cl hydrogen bonds link the complex cations, chloride anions and solvent water molecules into a three-dimensional network. |
first_indexed | 2024-04-11T19:47:52Z |
format | Article |
id | doaj.art-21d0d8f2cf2744fdb1c2229c06163419 |
institution | Directory Open Access Journal |
issn | 2056-9890 |
language | English |
last_indexed | 2024-04-11T19:47:52Z |
publishDate | 2015-02-01 |
publisher | International Union of Crystallography |
record_format | Article |
series | Acta Crystallographica Section E: Crystallographic Communications |
spelling | doaj.art-21d0d8f2cf2744fdb1c2229c061634192022-12-22T04:06:24ZengInternational Union of CrystallographyActa Crystallographica Section E: Crystallographic Communications2056-98902015-02-01712o105o10610.1107/S2056989015000286bq2398Crystal structure of (E)-3-{[2-(2,4-dichlorobenzylidene)hydrazin-1-yl]carbonyl}pyridinium chloride trihydrateJ. Josephine Novina0G. Vasuki1M. Suresh2M. Syed Ali Padusha3Department of Physics, Idhaya College for Women, Kumbakonam 1, IndiaDepartment of Physics, Kunthavai Naachiar Govt. Arts College (W) (Autonomous), Thanjavur 7, IndiaPG & Research Department of Chemistry, Jamal Mohamed College, Tiruchirappalli 20, IndiaPG & Research Department of Chemistry, Jamal Mohamed College, Tiruchirappalli 20, IndiaIn the title hydrated salt, C13H10Cl2N3O+·Cl−·3H2O, the organic cation exhibits a dihedral angle of 8.26 (14)° between the mean planes of the pyridinium and benzene rings, and dihedral angles of 8.70 (15) and 15.93 (5)° between the mean planes of the hydrazide group and the benzene and pyridinium rings, respectively. In the crystal, N—H...O, N—H...Cl, C—H...O, C—H...Cl, O—H...O, O—H...N and O—H...Cl hydrogen bonds link the complex cations, chloride anions and solvent water molecules into a three-dimensional network.http://scripts.iucr.org/cgi-bin/paper?S2056989015000286crystals structurepyridiniumhydrazide grouphydrogen bonds |
spellingShingle | J. Josephine Novina G. Vasuki M. Suresh M. Syed Ali Padusha Crystal structure of (E)-3-{[2-(2,4-dichlorobenzylidene)hydrazin-1-yl]carbonyl}pyridinium chloride trihydrate Acta Crystallographica Section E: Crystallographic Communications crystals structure pyridinium hydrazide group hydrogen bonds |
title | Crystal structure of (E)-3-{[2-(2,4-dichlorobenzylidene)hydrazin-1-yl]carbonyl}pyridinium chloride trihydrate |
title_full | Crystal structure of (E)-3-{[2-(2,4-dichlorobenzylidene)hydrazin-1-yl]carbonyl}pyridinium chloride trihydrate |
title_fullStr | Crystal structure of (E)-3-{[2-(2,4-dichlorobenzylidene)hydrazin-1-yl]carbonyl}pyridinium chloride trihydrate |
title_full_unstemmed | Crystal structure of (E)-3-{[2-(2,4-dichlorobenzylidene)hydrazin-1-yl]carbonyl}pyridinium chloride trihydrate |
title_short | Crystal structure of (E)-3-{[2-(2,4-dichlorobenzylidene)hydrazin-1-yl]carbonyl}pyridinium chloride trihydrate |
title_sort | crystal structure of e 3 2 2 4 dichlorobenzylidene hydrazin 1 yl carbonyl pyridinium chloride trihydrate |
topic | crystals structure pyridinium hydrazide group hydrogen bonds |
url | http://scripts.iucr.org/cgi-bin/paper?S2056989015000286 |
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