Thin-layer chromatography of DNS amino acids derivatives in systems with silica gel and silanized silica gel plates
Investigations into separation selectivity of High-Performance Thin-layer chromatography (HPTLC) of dansyl (DNS) derivatives of amino acids in silica gel (Silica gel 60 F254s plates) and silanized silica gel (RP-18 W plates) systems are presented. The results have been obtained for mobile phases con...
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Materialtyp: | Artikel |
Språk: | English |
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Sciendo
2022-08-01
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Serie: | Current Issues in Pharmacy and Medical Sciences |
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Länkar: | https://doi.org/10.2478/cipms-2022-0011 |
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author | Chomicki Adam Dzido Tadeusz H. |
author_facet | Chomicki Adam Dzido Tadeusz H. |
author_sort | Chomicki Adam |
collection | DOAJ |
description | Investigations into separation selectivity of High-Performance Thin-layer chromatography (HPTLC) of dansyl (DNS) derivatives of amino acids in silica gel (Silica gel 60 F254s plates) and silanized silica gel (RP-18 W plates) systems are presented. The results have been obtained for mobile phases containing different concentrations of acetonitrile (ACN) in formic acid (FA) water solution (final concentration of FA in the mobile phase was equal to 265 mmol/dm3). The data obtained show differences in separation selectivity of the solutes between employment of HPTLC silica gel and RP-18 W systems. |
first_indexed | 2024-04-12T16:41:07Z |
format | Article |
id | doaj.art-22109b51e7a14266b51bfa05725fb740 |
institution | Directory Open Access Journal |
issn | 2300-6676 |
language | English |
last_indexed | 2024-04-12T16:41:07Z |
publishDate | 2022-08-01 |
publisher | Sciendo |
record_format | Article |
series | Current Issues in Pharmacy and Medical Sciences |
spelling | doaj.art-22109b51e7a14266b51bfa05725fb7402022-12-22T03:24:46ZengSciendoCurrent Issues in Pharmacy and Medical Sciences2300-66762022-08-01352586110.2478/cipms-2022-0011Thin-layer chromatography of DNS amino acids derivatives in systems with silica gel and silanized silica gel platesChomicki Adam0Dzido Tadeusz H.1Department of Physical Chemistry, Medical University of Lublin, PolandDepartment of Physical Chemistry, Medical University of Lublin, PolandInvestigations into separation selectivity of High-Performance Thin-layer chromatography (HPTLC) of dansyl (DNS) derivatives of amino acids in silica gel (Silica gel 60 F254s plates) and silanized silica gel (RP-18 W plates) systems are presented. The results have been obtained for mobile phases containing different concentrations of acetonitrile (ACN) in formic acid (FA) water solution (final concentration of FA in the mobile phase was equal to 265 mmol/dm3). The data obtained show differences in separation selectivity of the solutes between employment of HPTLC silica gel and RP-18 W systems.https://doi.org/10.2478/cipms-2022-0011thin layer chromatographyhptlcamino acidsdansyl derivatives |
spellingShingle | Chomicki Adam Dzido Tadeusz H. Thin-layer chromatography of DNS amino acids derivatives in systems with silica gel and silanized silica gel plates Current Issues in Pharmacy and Medical Sciences thin layer chromatography hptlc amino acids dansyl derivatives |
title | Thin-layer chromatography of DNS amino acids derivatives in systems with silica gel and silanized silica gel plates |
title_full | Thin-layer chromatography of DNS amino acids derivatives in systems with silica gel and silanized silica gel plates |
title_fullStr | Thin-layer chromatography of DNS amino acids derivatives in systems with silica gel and silanized silica gel plates |
title_full_unstemmed | Thin-layer chromatography of DNS amino acids derivatives in systems with silica gel and silanized silica gel plates |
title_short | Thin-layer chromatography of DNS amino acids derivatives in systems with silica gel and silanized silica gel plates |
title_sort | thin layer chromatography of dns amino acids derivatives in systems with silica gel and silanized silica gel plates |
topic | thin layer chromatography hptlc amino acids dansyl derivatives |
url | https://doi.org/10.2478/cipms-2022-0011 |
work_keys_str_mv | AT chomickiadam thinlayerchromatographyofdnsaminoacidsderivativesinsystemswithsilicagelandsilanizedsilicagelplates AT dzidotadeuszh thinlayerchromatographyofdnsaminoacidsderivativesinsystemswithsilicagelandsilanizedsilicagelplates |