Flotation and Humic Acid Extraction Test of Zhaotong Lignite

This is an essay in the field of mineral processing engineering. Humic acid is an important part of Zhaotong lignite. In order to extract humic acid efficiently, the optimum flotation conditions of Zhaotong lignite were explored by using the process of direct flotation and reverse flotation. Orthogo...

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Main Authors: Peng Chen, Xinwei Bai, Yuan Li, Chenhu Zhang, Shiwei Wang, Yaoyao Chen
Format: Article
Language:zho
Published: Institute of Multipurpose Utilization of Mineral Resources, Chinese Academy of Geological Sciences 2023-12-01
Series:Kuangchan zonghe liyong
Subjects:
Online Access:http://www.kczhly.com/en/article/doi/10.3969/j.issn.1000-6532.2023.06.026
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author Peng Chen
Xinwei Bai
Yuan Li
Chenhu Zhang
Shiwei Wang
Yaoyao Chen
author_facet Peng Chen
Xinwei Bai
Yuan Li
Chenhu Zhang
Shiwei Wang
Yaoyao Chen
author_sort Peng Chen
collection DOAJ
description This is an essay in the field of mineral processing engineering. Humic acid is an important part of Zhaotong lignite. In order to extract humic acid efficiently, the optimum flotation conditions of Zhaotong lignite were explored by using the process of direct flotation and reverse flotation. Orthogonal experiments were designed by using the method of oxygen decomposition and alkali solution-acid separation to extract humic acid from flotation cleaned coal, and the optimal conditions of humic acid extraction were explored. The results show that the positive flotation collector consumption is large, and under the condition of surface modification of Span 80, the flotation cleaned coal yield is the highest of 26.64% and ash content is the lowest of 20.08%; the optimum conditions of reverse flotation are laurylamine 5 kg/t, dextrin 3 kg/t and foaming agent 260 g/t, and the optimum flotation indexes are as follows: flotation cleaned coal yield 84.35% and ash 20.52%, flotation tailcoal yield 15.65% and ash 36.75%, and flotation perfection index 12.08; the optimum extraction conditions of oxygen decomposition are as follows: H2O2 concentration 0.7 mol/L, H2O2 activation time 35 min, NaOH concentration 0.3 mol/L, NaOH soaking time 30 min, and the extraction rate of humic acid 37.14%; the optimal extraction conditions of alkali-soluble acid chromatography are as follows: concentration of hydrochloric acid 10%, activation time of hydrochloric acid 30 min, NaOH concentration 0.7 moL/L, NaOH soaking time 30 min, and the extraction yield 43.80%. Reverse flotation can obtain higher yield of high ash flotation clean coal than normal flotation, and the extraction rate is higher when the humic acid of Zhaotong lignite is extracted by alkali solution-acid separation method.
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spelling doaj.art-221640c11c974997ac80bbf625f8520a2023-12-21T08:27:18ZzhoInstitute of Multipurpose Utilization of Mineral Resources, Chinese Academy of Geological SciencesKuangchan zonghe liyong1000-65322023-12-0144616917510.3969/j.issn.1000-6532.2023.06.0262023-06chenpengFlotation and Humic Acid Extraction Test of Zhaotong LignitePeng Chen0Xinwei Bai1Yuan Li2Chenhu Zhang3Shiwei Wang4Yaoyao Chen5School of Chemistry and Materials Engineering, Liupanshui Normal University, Liupanshui , Guizhou, ChinaSchool of Chemistry and Materials Engineering, Liupanshui Normal University, Liupanshui , Guizhou, ChinaGuizhou Coal Product Quality Supervision and Inspection Institute, Liupanshui, Guizhou, ChinaSchool of Chemistry and Materials Engineering, Liupanshui Normal University, Liupanshui , Guizhou, ChinaSchool of Chemistry and Materials Engineering, Liupanshui Normal University, Liupanshui , Guizhou, ChinaSchool of Chemistry and Materials Engineering, Liupanshui Normal University, Liupanshui , Guizhou, ChinaThis is an essay in the field of mineral processing engineering. Humic acid is an important part of Zhaotong lignite. In order to extract humic acid efficiently, the optimum flotation conditions of Zhaotong lignite were explored by using the process of direct flotation and reverse flotation. Orthogonal experiments were designed by using the method of oxygen decomposition and alkali solution-acid separation to extract humic acid from flotation cleaned coal, and the optimal conditions of humic acid extraction were explored. The results show that the positive flotation collector consumption is large, and under the condition of surface modification of Span 80, the flotation cleaned coal yield is the highest of 26.64% and ash content is the lowest of 20.08%; the optimum conditions of reverse flotation are laurylamine 5 kg/t, dextrin 3 kg/t and foaming agent 260 g/t, and the optimum flotation indexes are as follows: flotation cleaned coal yield 84.35% and ash 20.52%, flotation tailcoal yield 15.65% and ash 36.75%, and flotation perfection index 12.08; the optimum extraction conditions of oxygen decomposition are as follows: H2O2 concentration 0.7 mol/L, H2O2 activation time 35 min, NaOH concentration 0.3 mol/L, NaOH soaking time 30 min, and the extraction rate of humic acid 37.14%; the optimal extraction conditions of alkali-soluble acid chromatography are as follows: concentration of hydrochloric acid 10%, activation time of hydrochloric acid 30 min, NaOH concentration 0.7 moL/L, NaOH soaking time 30 min, and the extraction yield 43.80%. Reverse flotation can obtain higher yield of high ash flotation clean coal than normal flotation, and the extraction rate is higher when the humic acid of Zhaotong lignite is extracted by alkali solution-acid separation method.http://www.kczhly.com/en/article/doi/10.3969/j.issn.1000-6532.2023.06.026mineral processing engineeringzhaotong lignitedirect flotationreverse floatationhumic acidextraction process
spellingShingle Peng Chen
Xinwei Bai
Yuan Li
Chenhu Zhang
Shiwei Wang
Yaoyao Chen
Flotation and Humic Acid Extraction Test of Zhaotong Lignite
Kuangchan zonghe liyong
mineral processing engineering
zhaotong lignite
direct flotation
reverse floatation
humic acid
extraction process
title Flotation and Humic Acid Extraction Test of Zhaotong Lignite
title_full Flotation and Humic Acid Extraction Test of Zhaotong Lignite
title_fullStr Flotation and Humic Acid Extraction Test of Zhaotong Lignite
title_full_unstemmed Flotation and Humic Acid Extraction Test of Zhaotong Lignite
title_short Flotation and Humic Acid Extraction Test of Zhaotong Lignite
title_sort flotation and humic acid extraction test of zhaotong lignite
topic mineral processing engineering
zhaotong lignite
direct flotation
reverse floatation
humic acid
extraction process
url http://www.kczhly.com/en/article/doi/10.3969/j.issn.1000-6532.2023.06.026
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