N′-(4-Methoxybenzylidene)-4-nitrobenzohydrazide methanol solvate
The title compound, C15H13N3O4·CH4O, was synthesized from the reaction of 4-methoxybenzaldehyde with 4-nitrobenzohydrazide in methanol. The benzene rings of the Schiff base molecule are nearly coplanar, making a dihedral angle of 7.0 (3)°. The methanol solvent molecules a...
| Main Authors: | , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2008-04-01
|
| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536808005813 |
| _version_ | 1819002731178754048 |
|---|---|
| author | Qian Cai Yun-Peng Diao Ming-Dong Wang Yuan-Zhi Wang |
| author_facet | Qian Cai Yun-Peng Diao Ming-Dong Wang Yuan-Zhi Wang |
| author_sort | Qian Cai |
| collection | DOAJ |
| description | The title compound, C15H13N3O4·CH4O, was synthesized from the reaction of 4-methoxybenzaldehyde with 4-nitrobenzohydrazide in methanol. The benzene rings of the Schiff base molecule are nearly coplanar, making a dihedral angle of 7.0 (3)°. The methanol solvent molecules are linked to the Schiff base molecules by N—H...O, O—H...N and O—H...O hydrogen bonds, forming chains running parallel to the b axis. |
| first_indexed | 2024-12-20T23:09:46Z |
| format | Article |
| id | doaj.art-234eaab8b4624088a68be2054cc2da61 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-20T23:09:46Z |
| publishDate | 2008-04-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-234eaab8b4624088a68be2054cc2da612022-12-21T19:23:45ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682008-04-01644o668o66810.1107/S1600536808005813N′-(4-Methoxybenzylidene)-4-nitrobenzohydrazide methanol solvateQian CaiYun-Peng DiaoMing-Dong WangYuan-Zhi WangThe title compound, C15H13N3O4·CH4O, was synthesized from the reaction of 4-methoxybenzaldehyde with 4-nitrobenzohydrazide in methanol. The benzene rings of the Schiff base molecule are nearly coplanar, making a dihedral angle of 7.0 (3)°. The methanol solvent molecules are linked to the Schiff base molecules by N—H...O, O—H...N and O—H...O hydrogen bonds, forming chains running parallel to the b axis.http://scripts.iucr.org/cgi-bin/paper?S1600536808005813 |
| spellingShingle | Qian Cai Yun-Peng Diao Ming-Dong Wang Yuan-Zhi Wang N′-(4-Methoxybenzylidene)-4-nitrobenzohydrazide methanol solvate Acta Crystallographica Section E |
| title | N′-(4-Methoxybenzylidene)-4-nitrobenzohydrazide methanol solvate |
| title_full | N′-(4-Methoxybenzylidene)-4-nitrobenzohydrazide methanol solvate |
| title_fullStr | N′-(4-Methoxybenzylidene)-4-nitrobenzohydrazide methanol solvate |
| title_full_unstemmed | N′-(4-Methoxybenzylidene)-4-nitrobenzohydrazide methanol solvate |
| title_short | N′-(4-Methoxybenzylidene)-4-nitrobenzohydrazide methanol solvate |
| title_sort | n 8242 4 methoxybenzylidene 4 nitrobenzohydrazide methanol solvate |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536808005813 |
| work_keys_str_mv | AT qiancai n82424methoxybenzylidene4nitrobenzohydrazidemethanolsolvate AT yunpengdiao n82424methoxybenzylidene4nitrobenzohydrazidemethanolsolvate AT mingdongwang n82424methoxybenzylidene4nitrobenzohydrazidemethanolsolvate AT yuanzhiwang n82424methoxybenzylidene4nitrobenzohydrazidemethanolsolvate |