Garcinia Mangostana Peel Extract as Sustainable Fuel Source on Ceria Synthesis under Hydrothermal Condition

Cerium (IV) oxide or ceria (CeO2) was fabricated by heating an aqueous extract of Garcinia mangostana and cerium (III) nitrate in hydrothermal autoclave reactor at 200 °C for 3 hours, followed by calcination at 600 °C for 5 hours. The powder X-ray diffraction (XRD) pattern of the precipitate from ce...

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Main Authors: SALPRIMA YUDHA S, Morina Adfa, Aswin Falahudin, Deni Agus Triawan, Liana Wahyuni, Meka Saima Perdani
Format: Article
Language:English
Published: University of Brawijaya 2019-12-01
Series:Journal of Pure and Applied Chemistry Research
Subjects:
Online Access:https://jpacr.ub.ac.id/index.php/jpacr/article/view/496/pdf
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author SALPRIMA YUDHA S
Morina Adfa
Aswin Falahudin
Deni Agus Triawan
Liana Wahyuni
Meka Saima Perdani
author_facet SALPRIMA YUDHA S
Morina Adfa
Aswin Falahudin
Deni Agus Triawan
Liana Wahyuni
Meka Saima Perdani
author_sort SALPRIMA YUDHA S
collection DOAJ
description Cerium (IV) oxide or ceria (CeO2) was fabricated by heating an aqueous extract of Garcinia mangostana and cerium (III) nitrate in hydrothermal autoclave reactor at 200 °C for 3 hours, followed by calcination at 600 °C for 5 hours. The powder X-ray diffraction (XRD) pattern of the precipitate from cerium(III) nitrate under hydrothermal reaction conditions shows no clear XRD peaks, indicating its amorphous nature. In contrast, the products from the calcinated samples exhibit XRD peaks, which correspond to cubic fluorite structure with an average crystal size of 7.55 nm. The elemental mapping using the energy-dispersive X-ray (EDX) analysis reveals the main elements present were cerium and oxygen, with minor impurities in low amounts. The presence of Garcinia mangostana extract is predicted to be the key component and fuel source to obtain CeO2 particles with narrow crystal size.
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spelling doaj.art-2389c702d8a64eee90d424ea8fbcc7b22022-12-21T22:55:14ZengUniversity of BrawijayaJournal of Pure and Applied Chemistry Research2302-46902302-46902019-12-0183255261Garcinia Mangostana Peel Extract as Sustainable Fuel Source on Ceria Synthesis under Hydrothermal ConditionSALPRIMA YUDHA S0Morina Adfa1Aswin Falahudin2Deni Agus Triawan3Liana Wahyuni4Meka Saima Perdani5Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Bengkulu, Jalan W.R. Supratman Kandang Limun, Kota Bengkulu, Indonesia 38371A.Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Bengkulu, Jalan W.R. Supratman Kandang Limun, Kota Bengkulu, Indonesia 38371A.Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Bengkulu, Jalan W.R. Supratman Kandang Limun, Kota Bengkulu, Indonesia 38371A.Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Bengkulu, Jalan W.R. Supratman Kandang Limun, Kota Bengkulu, Indonesia 38371A.Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Bengkulu, Jalan W.R. Supratman Kandang Limun, Kota Bengkulu, Indonesia 38371A.Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Bengkulu, Jalan W.R. Supratman Kandang Limun, Kota Bengkulu, Indonesia 38371A.Cerium (IV) oxide or ceria (CeO2) was fabricated by heating an aqueous extract of Garcinia mangostana and cerium (III) nitrate in hydrothermal autoclave reactor at 200 °C for 3 hours, followed by calcination at 600 °C for 5 hours. The powder X-ray diffraction (XRD) pattern of the precipitate from cerium(III) nitrate under hydrothermal reaction conditions shows no clear XRD peaks, indicating its amorphous nature. In contrast, the products from the calcinated samples exhibit XRD peaks, which correspond to cubic fluorite structure with an average crystal size of 7.55 nm. The elemental mapping using the energy-dispersive X-ray (EDX) analysis reveals the main elements present were cerium and oxygen, with minor impurities in low amounts. The presence of Garcinia mangostana extract is predicted to be the key component and fuel source to obtain CeO2 particles with narrow crystal size.https://jpacr.ub.ac.id/index.php/jpacr/article/view/496/pdfceriaceo2fuel sourcegarcinia mangostanahydrothermal
spellingShingle SALPRIMA YUDHA S
Morina Adfa
Aswin Falahudin
Deni Agus Triawan
Liana Wahyuni
Meka Saima Perdani
Garcinia Mangostana Peel Extract as Sustainable Fuel Source on Ceria Synthesis under Hydrothermal Condition
Journal of Pure and Applied Chemistry Research
ceria
ceo2
fuel source
garcinia mangostana
hydrothermal
title Garcinia Mangostana Peel Extract as Sustainable Fuel Source on Ceria Synthesis under Hydrothermal Condition
title_full Garcinia Mangostana Peel Extract as Sustainable Fuel Source on Ceria Synthesis under Hydrothermal Condition
title_fullStr Garcinia Mangostana Peel Extract as Sustainable Fuel Source on Ceria Synthesis under Hydrothermal Condition
title_full_unstemmed Garcinia Mangostana Peel Extract as Sustainable Fuel Source on Ceria Synthesis under Hydrothermal Condition
title_short Garcinia Mangostana Peel Extract as Sustainable Fuel Source on Ceria Synthesis under Hydrothermal Condition
title_sort garcinia mangostana peel extract as sustainable fuel source on ceria synthesis under hydrothermal condition
topic ceria
ceo2
fuel source
garcinia mangostana
hydrothermal
url https://jpacr.ub.ac.id/index.php/jpacr/article/view/496/pdf
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