Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode-free batteries
Summary: In this protocol, we describe the quantification of electrolytes using nuclear magnetic resonance. We detail the steps involved for battery cycling, sample preparation, instrument operation, and data analysis. The protocol can be used to quantify electrolyte decomposition reactions and the...
| Main Authors: | , , , , , , , |
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| Format: | Article |
| Language: | English |
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Elsevier
2022-12-01
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| Series: | STAR Protocols |
| Subjects: | |
| Online Access: | http://www.sciencedirect.com/science/article/pii/S266616672200747X |
| _version_ | 1811292651178164224 |
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| author | Ming-Yue Zhou Xiao-Qing Ding Li-Peng Hou Jin Xie Bo-Quan Li Jia-Qi Huang Xue-Qiang Zhang Qiang Zhang |
| author_facet | Ming-Yue Zhou Xiao-Qing Ding Li-Peng Hou Jin Xie Bo-Quan Li Jia-Qi Huang Xue-Qiang Zhang Qiang Zhang |
| author_sort | Ming-Yue Zhou |
| collection | DOAJ |
| description | Summary: In this protocol, we describe the quantification of electrolytes using nuclear magnetic resonance. We detail the steps involved for battery cycling, sample preparation, instrument operation, and data analysis. The protocol can be used to quantify electrolyte decomposition reactions and the apparent electron transfer numbers of different electrolyte components. The protocol is optimized for lithium-based anode-free batteries but can also be applied to other rechargeable batteries.For complete details on the use and execution of this protocol, please refer to Zhou et al. (2022).1 : Publisher’s note: Undertaking any experimental protocol requires adherence to local institutional guidelines for laboratory safety and ethics. |
| first_indexed | 2024-04-13T04:48:32Z |
| format | Article |
| id | doaj.art-23a0f744b6424b4ea97e4578b5c10746 |
| institution | Directory Open Access Journal |
| issn | 2666-1667 |
| language | English |
| last_indexed | 2024-04-13T04:48:32Z |
| publishDate | 2022-12-01 |
| publisher | Elsevier |
| record_format | Article |
| series | STAR Protocols |
| spelling | doaj.art-23a0f744b6424b4ea97e4578b5c107462022-12-22T03:01:45ZengElsevierSTAR Protocols2666-16672022-12-0134101867Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode-free batteriesMing-Yue Zhou0Xiao-Qing Ding1Li-Peng Hou2Jin Xie3Bo-Quan Li4Jia-Qi Huang5Xue-Qiang Zhang6Qiang Zhang7Beijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering, Tsinghua University, Beijing 100084, ChinaAdvanced Research Institute for Multidisciplinary Science, Beijing Institute of Technology, Beijing 100081, China; School of Materials Science and Engineering, Beijing Institute of Technology, Beijing 100081, ChinaBeijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering, Tsinghua University, Beijing 100084, ChinaBeijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering, Tsinghua University, Beijing 100084, ChinaAdvanced Research Institute for Multidisciplinary Science, Beijing Institute of Technology, Beijing 100081, China; School of Materials Science and Engineering, Beijing Institute of Technology, Beijing 100081, ChinaAdvanced Research Institute for Multidisciplinary Science, Beijing Institute of Technology, Beijing 100081, China; School of Materials Science and Engineering, Beijing Institute of Technology, Beijing 100081, ChinaAdvanced Research Institute for Multidisciplinary Science, Beijing Institute of Technology, Beijing 100081, China; School of Materials Science and Engineering, Beijing Institute of Technology, Beijing 100081, China; Corresponding authorBeijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering, Tsinghua University, Beijing 100084, China; Corresponding authorSummary: In this protocol, we describe the quantification of electrolytes using nuclear magnetic resonance. We detail the steps involved for battery cycling, sample preparation, instrument operation, and data analysis. The protocol can be used to quantify electrolyte decomposition reactions and the apparent electron transfer numbers of different electrolyte components. The protocol is optimized for lithium-based anode-free batteries but can also be applied to other rechargeable batteries.For complete details on the use and execution of this protocol, please refer to Zhou et al. (2022).1 : Publisher’s note: Undertaking any experimental protocol requires adherence to local institutional guidelines for laboratory safety and ethics.http://www.sciencedirect.com/science/article/pii/S266616672200747XNMREnergyChemistryMaterial sciences |
| spellingShingle | Ming-Yue Zhou Xiao-Qing Ding Li-Peng Hou Jin Xie Bo-Quan Li Jia-Qi Huang Xue-Qiang Zhang Qiang Zhang Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode-free batteries STAR Protocols NMR Energy Chemistry Material sciences |
| title | Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode-free batteries |
| title_full | Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode-free batteries |
| title_fullStr | Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode-free batteries |
| title_full_unstemmed | Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode-free batteries |
| title_short | Protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode-free batteries |
| title_sort | protocol for quantitative nuclear magnetic resonance for deciphering electrolyte decomposition reactions in anode free batteries |
| topic | NMR Energy Chemistry Material sciences |
| url | http://www.sciencedirect.com/science/article/pii/S266616672200747X |
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