Mechanical and antibacterial properties of FDM additively manufactured PLA parts

This study explores the compression and antibacterial properties of 10x10 × 10 mm polylactic acid (PLA) cubes manufactured through FDM additive printing for biomedical parts. A 3x3 full factorial DOE with 3 replicates examines the impact of printing parameters (infill %, print speed, and layer heigh...

Full description

Bibliographic Details
Main Authors: Anesu Nyabadza, Louis Michael Mc Donough, Arul Manikandan, Abhishek Basu Ray, Anouk Plouze, Corné Muilwijk, Brian Freeland, Mercedes Vazquez, Dermot Brabazon
Format: Article
Language:English
Published: Elsevier 2024-03-01
Series:Results in Engineering
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S259012302300871X
_version_ 1797247721109716992
author Anesu Nyabadza
Louis Michael Mc Donough
Arul Manikandan
Abhishek Basu Ray
Anouk Plouze
Corné Muilwijk
Brian Freeland
Mercedes Vazquez
Dermot Brabazon
author_facet Anesu Nyabadza
Louis Michael Mc Donough
Arul Manikandan
Abhishek Basu Ray
Anouk Plouze
Corné Muilwijk
Brian Freeland
Mercedes Vazquez
Dermot Brabazon
author_sort Anesu Nyabadza
collection DOAJ
description This study explores the compression and antibacterial properties of 10x10 × 10 mm polylactic acid (PLA) cubes manufactured through FDM additive printing for biomedical parts. A 3x3 full factorial DOE with 3 replicates examines the impact of printing parameters (infill %, print speed, and layer height). The highest compression strength and stiffness recorded were 91 MPa and 0.76 GPa, respectively. Despite minor mass variations (1.05 ± 0.09 g) under all the investigated parameters, the mean strength of all printed parts was 67.6 ± 10.6 MPa, highlighting the significant influence of processing parameters on mechanical properties. Heat treatment at 60 °C for 30 min improved stiffness. Investigation of various parameters, including layer height and orientation, revealed that larger layer heights resulted in reduced compression strength. Anisotropic compression properties persisted post-heat treatment due to thermal stresses and interlayer bonding. The flat direction (top view) exhibited higher compression properties due to a homogeneous microstructure, minimized interlayer bonding impact, and increased crystallinity. Antibacterial properties against E.coli were induced via coating with peanut-shaped copper nanoparticles (68–267 nm). Nanoparticles were fabricated via a combination of wet chemistry and laser ablation.
first_indexed 2024-03-08T17:06:36Z
format Article
id doaj.art-258195d4baad41009ed77b7a11c4ef79
institution Directory Open Access Journal
issn 2590-1230
language English
last_indexed 2024-04-24T20:03:11Z
publishDate 2024-03-01
publisher Elsevier
record_format Article
series Results in Engineering
spelling doaj.art-258195d4baad41009ed77b7a11c4ef792024-03-24T07:00:29ZengElsevierResults in Engineering2590-12302024-03-0121101744Mechanical and antibacterial properties of FDM additively manufactured PLA partsAnesu Nyabadza0Louis Michael Mc Donough1Arul Manikandan2Abhishek Basu Ray3Anouk Plouze4Corné Muilwijk5Brian Freeland6Mercedes Vazquez7Dermot Brabazon8I-Form Advanced Manufacturing Centre Research, Dublin City University, Glasnevin, Dublin, 9, Ireland; Advanced Processing Technology Research Centre, School of Mechanical and Manufacturing Engineering, Dublin City University, Glasnevin, Dublin, 9, Ireland; Corresponding author. I-Form Advanced Manufacturing Centre Research, Dublin City University, Glasnevin, Dublin, 9, Ireland.Advanced Processing Technology Research Centre, School of Mechanical and Manufacturing Engineering, Dublin City University, Glasnevin, Dublin, 9, IrelandSchool of Biotechnology, Dublin City University, Glasnevin, D09 K20V, Dublin, IrelandAdvanced Processing Technology Research Centre, School of Mechanical and Manufacturing Engineering, Dublin City University, Glasnevin, Dublin, 9, IrelandAdvanced Processing Technology Research Centre, School of Mechanical and Manufacturing Engineering, Dublin City University, Glasnevin, Dublin, 9, Ireland; Conservatoire national des arts et métiers (Cnam), 61 Rue du Landy, 93210, Saint-Denis, FranceI-Form Advanced Manufacturing Centre Research, Dublin City University, Glasnevin, Dublin, 9, Ireland; Advanced Processing Technology Research Centre, School of Mechanical and Manufacturing Engineering, Dublin City University, Glasnevin, Dublin, 9, IrelandI-Form Advanced Manufacturing Centre Research, Dublin City University, Glasnevin, Dublin, 9, Ireland; Advanced Processing Technology Research Centre, School of Mechanical and Manufacturing Engineering, Dublin City University, Glasnevin, Dublin, 9, Ireland; School of Biotechnology, Dublin City University, Glasnevin, D09 K20V, Dublin, IrelandI-Form Advanced Manufacturing Centre Research, Dublin City University, Glasnevin, Dublin, 9, Ireland; Advanced Processing Technology Research Centre, School of Mechanical and Manufacturing Engineering, Dublin City University, Glasnevin, Dublin, 9, Ireland; School of Analytical Chemistry, Dublin City University, Glasnevin, D09 K20V, Dublin, IrelandI-Form Advanced Manufacturing Centre Research, Dublin City University, Glasnevin, Dublin, 9, Ireland; Advanced Processing Technology Research Centre, School of Mechanical and Manufacturing Engineering, Dublin City University, Glasnevin, Dublin, 9, IrelandThis study explores the compression and antibacterial properties of 10x10 × 10 mm polylactic acid (PLA) cubes manufactured through FDM additive printing for biomedical parts. A 3x3 full factorial DOE with 3 replicates examines the impact of printing parameters (infill %, print speed, and layer height). The highest compression strength and stiffness recorded were 91 MPa and 0.76 GPa, respectively. Despite minor mass variations (1.05 ± 0.09 g) under all the investigated parameters, the mean strength of all printed parts was 67.6 ± 10.6 MPa, highlighting the significant influence of processing parameters on mechanical properties. Heat treatment at 60 °C for 30 min improved stiffness. Investigation of various parameters, including layer height and orientation, revealed that larger layer heights resulted in reduced compression strength. Anisotropic compression properties persisted post-heat treatment due to thermal stresses and interlayer bonding. The flat direction (top view) exhibited higher compression properties due to a homogeneous microstructure, minimized interlayer bonding impact, and increased crystallinity. Antibacterial properties against E.coli were induced via coating with peanut-shaped copper nanoparticles (68–267 nm). Nanoparticles were fabricated via a combination of wet chemistry and laser ablation.http://www.sciencedirect.com/science/article/pii/S259012302300871XAntibacterial copper nanoparticlesPolylactic acidFused deposition modellingLaser ablation in liquidAdditive manufacturingE.coli
spellingShingle Anesu Nyabadza
Louis Michael Mc Donough
Arul Manikandan
Abhishek Basu Ray
Anouk Plouze
Corné Muilwijk
Brian Freeland
Mercedes Vazquez
Dermot Brabazon
Mechanical and antibacterial properties of FDM additively manufactured PLA parts
Results in Engineering
Antibacterial copper nanoparticles
Polylactic acid
Fused deposition modelling
Laser ablation in liquid
Additive manufacturing
E.coli
title Mechanical and antibacterial properties of FDM additively manufactured PLA parts
title_full Mechanical and antibacterial properties of FDM additively manufactured PLA parts
title_fullStr Mechanical and antibacterial properties of FDM additively manufactured PLA parts
title_full_unstemmed Mechanical and antibacterial properties of FDM additively manufactured PLA parts
title_short Mechanical and antibacterial properties of FDM additively manufactured PLA parts
title_sort mechanical and antibacterial properties of fdm additively manufactured pla parts
topic Antibacterial copper nanoparticles
Polylactic acid
Fused deposition modelling
Laser ablation in liquid
Additive manufacturing
E.coli
url http://www.sciencedirect.com/science/article/pii/S259012302300871X
work_keys_str_mv AT anesunyabadza mechanicalandantibacterialpropertiesoffdmadditivelymanufacturedplaparts
AT louismichaelmcdonough mechanicalandantibacterialpropertiesoffdmadditivelymanufacturedplaparts
AT arulmanikandan mechanicalandantibacterialpropertiesoffdmadditivelymanufacturedplaparts
AT abhishekbasuray mechanicalandantibacterialpropertiesoffdmadditivelymanufacturedplaparts
AT anoukplouze mechanicalandantibacterialpropertiesoffdmadditivelymanufacturedplaparts
AT cornemuilwijk mechanicalandantibacterialpropertiesoffdmadditivelymanufacturedplaparts
AT brianfreeland mechanicalandantibacterialpropertiesoffdmadditivelymanufacturedplaparts
AT mercedesvazquez mechanicalandantibacterialpropertiesoffdmadditivelymanufacturedplaparts
AT dermotbrabazon mechanicalandantibacterialpropertiesoffdmadditivelymanufacturedplaparts