Mechanical alloying of Mg-Zn-Ca-Er alloy

Magnesium-based materials constitute promising alternatives for medical applications, due to their characteristics, such as good mechanical and biological properties. This opens many possibilities for biodegradable materials to be used as less-invasive options for treatment. Degradation is prompted...

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Main Authors: Bartłomiej Hrapkowicz, Sabina Lesz, Marek Kremzer, Małgorzata Karolus, Wojciech Pakieła
Format: Article
Language:English
Published: Polish Academy of Sciences 2021-06-01
Series:Bulletin of the Polish Academy of Sciences: Technical Sciences
Subjects:
Online Access:https://journals.pan.pl/Content/119855/PDF/08_02180_Bpast.No.69(5)_drukM_OK.pdf
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author Bartłomiej Hrapkowicz
Sabina Lesz
Marek Kremzer
Małgorzata Karolus
Wojciech Pakieła
author_facet Bartłomiej Hrapkowicz
Sabina Lesz
Marek Kremzer
Małgorzata Karolus
Wojciech Pakieła
author_sort Bartłomiej Hrapkowicz
collection DOAJ
description Magnesium-based materials constitute promising alternatives for medical applications, due to their characteristics, such as good mechanical and biological properties. This opens many possibilities for biodegradable materials to be used as less-invasive options for treatment. Degradation is prompted by their chemical composition and microstructure. Both those aspects can be finely adjusted by means of proper manufacturing processes, such as mechanical alloying (MA). Furthermore, MA allows for alloying elements that would normally be really hard to mix due to their very different properties. Magnesium usually needs various alloying elements, which can further increase its characteristics. Alloying magnesium with rare earth elements is considered to greatly improve the aforementioned properties. Due to that fact, erbium was used as one of the alloying elements, alongside zinc and calcium, to obtain an Mg₆₄Zn₃₀Ca₄Er₁ alloy via mechanical alloying. The alloy was milled in the SPEX 8000 Dual Mixer/Mill high energy mill under an argon atmosphere for 8, 13, and 20 hours. It was assessed using X-ray diffraction, energy dispersive spectroscopy and granulometric analysis as well as by studying its hardness. The hardness values reached 232, 250, and 302 HV, respectively, which is closely related to their particle size. Average particle sizes were 15, 16, and 17 μm, respectively
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spelling doaj.art-259c55c5fbed40f4bd949e4400bd56752022-12-22T02:49:15ZengPolish Academy of SciencesBulletin of the Polish Academy of Sciences: Technical Sciences2300-19172021-06-01695https://doi.org/10.24425/bpasts.2021.137587Mechanical alloying of Mg-Zn-Ca-Er alloyBartłomiej Hrapkowicz0https://orcid.org/0000-0002-3772-9685Sabina Lesz1https://orcid.org/0000-0002-2703-2059Marek Kremzer2https://orcid.org/0000-0002-6869-5115Małgorzata Karolus3https://orcid.org/0000-0002-2388-8036Wojciech Pakieła4https://orcid.org/0000-0002-6553-3217Department of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18A, 44-100 Gliwice, PolandDepartment of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18A, 44-100 Gliwice, PolandDepartment of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18A, 44-100 Gliwice, PolandInstitute of Materials Engineering, University of Silesia, ul. 75 Pułku Piechoty 1a, 41-500 Chorzów, PolandDepartment of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18A, 44-100 Gliwice, PolandMagnesium-based materials constitute promising alternatives for medical applications, due to their characteristics, such as good mechanical and biological properties. This opens many possibilities for biodegradable materials to be used as less-invasive options for treatment. Degradation is prompted by their chemical composition and microstructure. Both those aspects can be finely adjusted by means of proper manufacturing processes, such as mechanical alloying (MA). Furthermore, MA allows for alloying elements that would normally be really hard to mix due to their very different properties. Magnesium usually needs various alloying elements, which can further increase its characteristics. Alloying magnesium with rare earth elements is considered to greatly improve the aforementioned properties. Due to that fact, erbium was used as one of the alloying elements, alongside zinc and calcium, to obtain an Mg₆₄Zn₃₀Ca₄Er₁ alloy via mechanical alloying. The alloy was milled in the SPEX 8000 Dual Mixer/Mill high energy mill under an argon atmosphere for 8, 13, and 20 hours. It was assessed using X-ray diffraction, energy dispersive spectroscopy and granulometric analysis as well as by studying its hardness. The hardness values reached 232, 250, and 302 HV, respectively, which is closely related to their particle size. Average particle sizes were 15, 16, and 17 μm, respectivelyhttps://journals.pan.pl/Content/119855/PDF/08_02180_Bpast.No.69(5)_drukM_OK.pdfmagnesiummechanical alloyingerbiumrare earth elements
spellingShingle Bartłomiej Hrapkowicz
Sabina Lesz
Marek Kremzer
Małgorzata Karolus
Wojciech Pakieła
Mechanical alloying of Mg-Zn-Ca-Er alloy
Bulletin of the Polish Academy of Sciences: Technical Sciences
magnesium
mechanical alloying
erbium
rare earth elements
title Mechanical alloying of Mg-Zn-Ca-Er alloy
title_full Mechanical alloying of Mg-Zn-Ca-Er alloy
title_fullStr Mechanical alloying of Mg-Zn-Ca-Er alloy
title_full_unstemmed Mechanical alloying of Mg-Zn-Ca-Er alloy
title_short Mechanical alloying of Mg-Zn-Ca-Er alloy
title_sort mechanical alloying of mg zn ca er alloy
topic magnesium
mechanical alloying
erbium
rare earth elements
url https://journals.pan.pl/Content/119855/PDF/08_02180_Bpast.No.69(5)_drukM_OK.pdf
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AT marekkremzer mechanicalalloyingofmgzncaeralloy
AT małgorzatakarolus mechanicalalloyingofmgzncaeralloy
AT wojciechpakieła mechanicalalloyingofmgzncaeralloy