Effect of Grain Orientation on Hydrogen Embrittlement Behavior of Interstitial-Free Steel

In interstitial-free (IF) steel with a certain microtexture, the micro-orientation of grains is essential to understand the occurrence of hydrogen-induced cracking in body-centered cubic (BCC) structural steels. In this study, the hydrogen embrittlement (HE) susceptibility of IF steels was determine...

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Main Authors: Wei Wang, Hao Fu, Hailong Zhang, Yu Yan, Jinxu Li
Format: Article
Language:English
Published: MDPI AG 2022-06-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/12/6/981
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author Wei Wang
Hao Fu
Hailong Zhang
Yu Yan
Jinxu Li
author_facet Wei Wang
Hao Fu
Hailong Zhang
Yu Yan
Jinxu Li
author_sort Wei Wang
collection DOAJ
description In interstitial-free (IF) steel with a certain microtexture, the micro-orientation of grains is essential to understand the occurrence of hydrogen-induced cracking in body-centered cubic (BCC) structural steels. In this study, the hydrogen embrittlement (HE) susceptibility of IF steels was determined by slow strain rate tensile (SSRT) tests and hydrogen microprinting (HMT) experiments from the perspective of crystal orientation. The strength of the specimen with hydrogen was slightly higher than that without hydrogen, while the ductility and toughness were drastically reduced by hydrogen charging during the SSRT test. The HE susceptibility was characterized by the loss of elongation (I<sub>δ</sub>) and toughness (I<sub>ψ</sub>), with losses of 46.3% and 70%, respectively. The microstructural observations indicate that cracks initiated along grains oriented in the {100} || normal direction (ND), and grain boundaries (GBs) around {100}||ND were prone to be enriched in hydrogen atoms; that is, {100} || ND showed poor resistance to intergranular cracking and susceptible to hydrogen segregation. HMT was used to confirm the above viewpoints. Meanwhile, the statistical results showed those high-angle misorientations of 50–60° deviation are the locations most vulnerable to fracture.
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spelling doaj.art-26e4d08145f64033ae9e5aca2ef90ab02023-11-23T17:58:16ZengMDPI AGMetals2075-47012022-06-0112698110.3390/met12060981Effect of Grain Orientation on Hydrogen Embrittlement Behavior of Interstitial-Free SteelWei Wang0Hao Fu1Hailong Zhang2Yu Yan3Jinxu Li4Corrosion and Protection Center, Institute for Advanced Materials and Technology, University of Science and Technology Beijing, Beijing 100083, ChinaCorrosion and Protection Center, Institute for Advanced Materials and Technology, University of Science and Technology Beijing, Beijing 100083, ChinaNCS Testing Technology Co., Ltd., Beijing 100083, ChinaCorrosion and Protection Center, Institute for Advanced Materials and Technology, University of Science and Technology Beijing, Beijing 100083, ChinaCorrosion and Protection Center, Institute for Advanced Materials and Technology, University of Science and Technology Beijing, Beijing 100083, ChinaIn interstitial-free (IF) steel with a certain microtexture, the micro-orientation of grains is essential to understand the occurrence of hydrogen-induced cracking in body-centered cubic (BCC) structural steels. In this study, the hydrogen embrittlement (HE) susceptibility of IF steels was determined by slow strain rate tensile (SSRT) tests and hydrogen microprinting (HMT) experiments from the perspective of crystal orientation. The strength of the specimen with hydrogen was slightly higher than that without hydrogen, while the ductility and toughness were drastically reduced by hydrogen charging during the SSRT test. The HE susceptibility was characterized by the loss of elongation (I<sub>δ</sub>) and toughness (I<sub>ψ</sub>), with losses of 46.3% and 70%, respectively. The microstructural observations indicate that cracks initiated along grains oriented in the {100} || normal direction (ND), and grain boundaries (GBs) around {100}||ND were prone to be enriched in hydrogen atoms; that is, {100} || ND showed poor resistance to intergranular cracking and susceptible to hydrogen segregation. HMT was used to confirm the above viewpoints. Meanwhile, the statistical results showed those high-angle misorientations of 50–60° deviation are the locations most vulnerable to fracture.https://www.mdpi.com/2075-4701/12/6/981IF steelhydrogen embrittlementgrain orientationslow strain rate tensilehydrogen microprintcrack initiation
spellingShingle Wei Wang
Hao Fu
Hailong Zhang
Yu Yan
Jinxu Li
Effect of Grain Orientation on Hydrogen Embrittlement Behavior of Interstitial-Free Steel
Metals
IF steel
hydrogen embrittlement
grain orientation
slow strain rate tensile
hydrogen microprint
crack initiation
title Effect of Grain Orientation on Hydrogen Embrittlement Behavior of Interstitial-Free Steel
title_full Effect of Grain Orientation on Hydrogen Embrittlement Behavior of Interstitial-Free Steel
title_fullStr Effect of Grain Orientation on Hydrogen Embrittlement Behavior of Interstitial-Free Steel
title_full_unstemmed Effect of Grain Orientation on Hydrogen Embrittlement Behavior of Interstitial-Free Steel
title_short Effect of Grain Orientation on Hydrogen Embrittlement Behavior of Interstitial-Free Steel
title_sort effect of grain orientation on hydrogen embrittlement behavior of interstitial free steel
topic IF steel
hydrogen embrittlement
grain orientation
slow strain rate tensile
hydrogen microprint
crack initiation
url https://www.mdpi.com/2075-4701/12/6/981
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