Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate
In the title compound, C21H17N5O3S3·C3H7NO, the toluenesulfonamide ring and the combined ring system involving the pyridone and benzothiazole rings subtend an interplanar angle of 39.86 (4)°. The pyridone and benzothiazyl rings are linked by the intramolecular hydrogen bond N—Hamine...Nthiazole. The...
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2017-12-01
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| Series: | Acta Crystallographica Section E: Crystallographic Communications |
| Subjects: | |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S2056989017015778 |
| _version_ | 1818998630554533888 |
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| author | Rasha A. Azzam Galal H. Elgemeie Rasha E. Elsayed Peter G. Jones |
| author_facet | Rasha A. Azzam Galal H. Elgemeie Rasha E. Elsayed Peter G. Jones |
| author_sort | Rasha A. Azzam |
| collection | DOAJ |
| description | In the title compound, C21H17N5O3S3·C3H7NO, the toluenesulfonamide ring and the combined ring system involving the pyridone and benzothiazole rings subtend an interplanar angle of 39.86 (4)°. The pyridone and benzothiazyl rings are linked by the intramolecular hydrogen bond N—Hamine...Nthiazole. The DMF O atom accepts two classical hydrogen bonds. The molecules are linked by hydrogen bonds and an S...O contact to form layers parallel to the bc plane. |
| first_indexed | 2024-12-20T22:04:35Z |
| format | Article |
| id | doaj.art-271289625b0c4ae0bde2ce3a9611fd1d |
| institution | Directory Open Access Journal |
| issn | 2056-9890 |
| language | English |
| last_indexed | 2024-12-20T22:04:35Z |
| publishDate | 2017-12-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E: Crystallographic Communications |
| spelling | doaj.art-271289625b0c4ae0bde2ce3a9611fd1d2022-12-21T19:25:18ZengInternational Union of CrystallographyActa Crystallographica Section E: Crystallographic Communications2056-98902017-12-0173121820182210.1107/S2056989017015778hg5500Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvateRasha A. Azzam0Galal H. Elgemeie1Rasha E. Elsayed2Peter G. Jones3Chemistry Department, Faculty of Science, Helwan University, Cairo, EgyptChemistry Department, Faculty of Science, Helwan University, Cairo, EgyptChemistry Department, Faculty of Science, Helwan University, Cairo, EgyptInstitut für Anorganische und Analytische Chemie, Technische Universität Braunschweig, Hagenring 30, D-38106 Braunschweig, GermanyIn the title compound, C21H17N5O3S3·C3H7NO, the toluenesulfonamide ring and the combined ring system involving the pyridone and benzothiazole rings subtend an interplanar angle of 39.86 (4)°. The pyridone and benzothiazyl rings are linked by the intramolecular hydrogen bond N—Hamine...Nthiazole. The DMF O atom accepts two classical hydrogen bonds. The molecules are linked by hydrogen bonds and an S...O contact to form layers parallel to the bc plane.http://scripts.iucr.org/cgi-bin/paper?S2056989017015778crystal structure2-pyridonebenzothiazoledimethylformamide |
| spellingShingle | Rasha A. Azzam Galal H. Elgemeie Rasha E. Elsayed Peter G. Jones Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate Acta Crystallographica Section E: Crystallographic Communications crystal structure 2-pyridone benzothiazole dimethylformamide |
| title | Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate |
| title_full | Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate |
| title_fullStr | Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate |
| title_full_unstemmed | Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate |
| title_short | Crystal structure of N-[6-amino-5-(benzo[d]thiazol-2-yl)-3-cyano-4-methylsulfanyl-2-oxo-1,2-dihydropyridin-1-yl]-4-methylbenzenesulfonamide dimethylformamide monosolvate |
| title_sort | crystal structure of n 6 amino 5 benzo d thiazol 2 yl 3 cyano 4 methylsulfanyl 2 oxo 1 2 dihydropyridin 1 yl 4 methylbenzenesulfonamide dimethylformamide monosolvate |
| topic | crystal structure 2-pyridone benzothiazole dimethylformamide |
| url | http://scripts.iucr.org/cgi-bin/paper?S2056989017015778 |
| work_keys_str_mv | AT rashaaazzam crystalstructureofn6amino5benzodthiazol2yl3cyano4methylsulfanyl2oxo12dihydropyridin1yl4methylbenzenesulfonamidedimethylformamidemonosolvate AT galalhelgemeie crystalstructureofn6amino5benzodthiazol2yl3cyano4methylsulfanyl2oxo12dihydropyridin1yl4methylbenzenesulfonamidedimethylformamidemonosolvate AT rashaeelsayed crystalstructureofn6amino5benzodthiazol2yl3cyano4methylsulfanyl2oxo12dihydropyridin1yl4methylbenzenesulfonamidedimethylformamidemonosolvate AT petergjones crystalstructureofn6amino5benzodthiazol2yl3cyano4methylsulfanyl2oxo12dihydropyridin1yl4methylbenzenesulfonamidedimethylformamidemonosolvate |