Effect of Prior Boriding on Microstructure and Mechanical Properties of Nanobainitic X37CrMoV5-1 Hot-Work Tool Steel

The influence of prior pack boriding on the microstructure and properties of nanobainitised X37CrMoV5-1 hot-work tool steel was investigated in the present work. Pack boriding was conducted at 950 °C for 4 h. Nanobainitising consisted of two-step isothermal quenching at 320 °C for 1 h, followed by a...

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Main Authors: Grzegorz Łukaszewicz, Michał Tacikowski, Michał Kulka, Krzysztof Chmielarz, Monika Węsierska-Hinca, Wiesław A. Świątnicki
Format: Article
Language:English
Published: MDPI AG 2023-06-01
Series:Materials
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Online Access:https://www.mdpi.com/1996-1944/16/12/4237
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author Grzegorz Łukaszewicz
Michał Tacikowski
Michał Kulka
Krzysztof Chmielarz
Monika Węsierska-Hinca
Wiesław A. Świątnicki
author_facet Grzegorz Łukaszewicz
Michał Tacikowski
Michał Kulka
Krzysztof Chmielarz
Monika Węsierska-Hinca
Wiesław A. Świątnicki
author_sort Grzegorz Łukaszewicz
collection DOAJ
description The influence of prior pack boriding on the microstructure and properties of nanobainitised X37CrMoV5-1 hot-work tool steel was investigated in the present work. Pack boriding was conducted at 950 °C for 4 h. Nanobainitising consisted of two-step isothermal quenching at 320 °C for 1 h, followed by annealing at 260 °C for 18 h. A combination of boriding with nanobainitising constituted a new hybrid treatment. The obtained material exhibited a hard borided layer (up to 1822 ± 226 HV0.05) and a strong (rupture strength 1233 ± 41 MPa) nanobainitic core. However, the presence of a borided layer decreased mechanical properties under tensile and impact load conditions (total elongation decreased by 95% and impact toughness by 92%). Compared with borided and conventionally quenched and tempered steel, the hybrid–treated material retained higher plasticity (total elongation higher by 80%) and higher impact toughness (higher by 21%). It was found that the boriding led to the redistribution of carbon and silicon atoms between the borided layer and substrate, which could influence bainitic transformation in the transition zone. Furthermore, the thermal cycle in the boriding process also influenced the phase transformations during subsequent nanobainitising.
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spelling doaj.art-279e3153dd074826ae7e0ea9fc156c4f2023-11-18T11:23:26ZengMDPI AGMaterials1996-19442023-06-011612423710.3390/ma16124237Effect of Prior Boriding on Microstructure and Mechanical Properties of Nanobainitic X37CrMoV5-1 Hot-Work Tool SteelGrzegorz Łukaszewicz0Michał Tacikowski1Michał Kulka2Krzysztof Chmielarz3Monika Węsierska-Hinca4Wiesław A. Świątnicki5Faculty of Materials Science and Engineering, Warsaw University of Technology, ul. Wołoska 141, 02-507 Warsaw, PolandFaculty of Materials Science and Engineering, Warsaw University of Technology, ul. Wołoska 141, 02-507 Warsaw, PolandFaculty of Materials Engineering and Technical Physics, Poznan University of Technology, Pl. M. Skłodowskiej-Curie 5, 60-965 Poznan, PolandFaculty of Materials Science and Engineering, Warsaw University of Technology, ul. Wołoska 141, 02-507 Warsaw, PolandFaculty of Materials Science and Engineering, Warsaw University of Technology, ul. Wołoska 141, 02-507 Warsaw, PolandFaculty of Materials Science and Engineering, Warsaw University of Technology, ul. Wołoska 141, 02-507 Warsaw, PolandThe influence of prior pack boriding on the microstructure and properties of nanobainitised X37CrMoV5-1 hot-work tool steel was investigated in the present work. Pack boriding was conducted at 950 °C for 4 h. Nanobainitising consisted of two-step isothermal quenching at 320 °C for 1 h, followed by annealing at 260 °C for 18 h. A combination of boriding with nanobainitising constituted a new hybrid treatment. The obtained material exhibited a hard borided layer (up to 1822 ± 226 HV0.05) and a strong (rupture strength 1233 ± 41 MPa) nanobainitic core. However, the presence of a borided layer decreased mechanical properties under tensile and impact load conditions (total elongation decreased by 95% and impact toughness by 92%). Compared with borided and conventionally quenched and tempered steel, the hybrid–treated material retained higher plasticity (total elongation higher by 80%) and higher impact toughness (higher by 21%). It was found that the boriding led to the redistribution of carbon and silicon atoms between the borided layer and substrate, which could influence bainitic transformation in the transition zone. Furthermore, the thermal cycle in the boriding process also influenced the phase transformations during subsequent nanobainitising.https://www.mdpi.com/1996-1944/16/12/4237hybrid treatmentpack boridingnanobainitemicrostructuremechanical propertiesdilatometry
spellingShingle Grzegorz Łukaszewicz
Michał Tacikowski
Michał Kulka
Krzysztof Chmielarz
Monika Węsierska-Hinca
Wiesław A. Świątnicki
Effect of Prior Boriding on Microstructure and Mechanical Properties of Nanobainitic X37CrMoV5-1 Hot-Work Tool Steel
Materials
hybrid treatment
pack boriding
nanobainite
microstructure
mechanical properties
dilatometry
title Effect of Prior Boriding on Microstructure and Mechanical Properties of Nanobainitic X37CrMoV5-1 Hot-Work Tool Steel
title_full Effect of Prior Boriding on Microstructure and Mechanical Properties of Nanobainitic X37CrMoV5-1 Hot-Work Tool Steel
title_fullStr Effect of Prior Boriding on Microstructure and Mechanical Properties of Nanobainitic X37CrMoV5-1 Hot-Work Tool Steel
title_full_unstemmed Effect of Prior Boriding on Microstructure and Mechanical Properties of Nanobainitic X37CrMoV5-1 Hot-Work Tool Steel
title_short Effect of Prior Boriding on Microstructure and Mechanical Properties of Nanobainitic X37CrMoV5-1 Hot-Work Tool Steel
title_sort effect of prior boriding on microstructure and mechanical properties of nanobainitic x37crmov5 1 hot work tool steel
topic hybrid treatment
pack boriding
nanobainite
microstructure
mechanical properties
dilatometry
url https://www.mdpi.com/1996-1944/16/12/4237
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