SYNTHESIS AND CHARACTERIZATION OF NOVEL 1,3-OXAZEPANE DERIVATIVES VIA REACTION OF PHENYI SUCCINIC ANHYDRIDE WITH SCHHIF'S BASES
Novel 1,3-oxazepane-4,7-dione derivatives were synthesized by the reaction of phenyl succinic anhydride with Schiff‘s bases in anhydrous benzen with high yields. Schiff's bases were synthesized by the reaction of heteroaromatic aldehydes or ketones with primary heterocyclic amines. The resultin...
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University of Anbar
2014-08-01
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Series: | مجلة جامعة الانبار للعلوم الصرفة |
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Online Access: | https://juaps.uoanbar.edu.iq/article_123911_d41d8cd98f00b204e9800998ecf8427e.pdf |
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author | Amaadh F. Nassar Obaid H.Abid |
author_facet | Amaadh F. Nassar Obaid H.Abid |
author_sort | Amaadh F. Nassar |
collection | DOAJ |
description | Novel 1,3-oxazepane-4,7-dione derivatives were synthesized by the reaction of phenyl succinic anhydride with Schiff‘s bases in anhydrous benzen with high yields. Schiff's bases were synthesized by the reaction of heteroaromatic aldehydes or ketones with primary heterocyclic amines. The resulting products were identified by their melting point and their molecular structures were confirmed by FT-IR , UV-Vis. and 1HNMR spectroscopy. |
first_indexed | 2024-03-08T18:47:44Z |
format | Article |
id | doaj.art-27a265246948463cb6b3b451df323079 |
institution | Directory Open Access Journal |
issn | 1991-8941 2706-6703 |
language | English |
last_indexed | 2024-03-08T18:47:44Z |
publishDate | 2014-08-01 |
publisher | University of Anbar |
record_format | Article |
series | مجلة جامعة الانبار للعلوم الصرفة |
spelling | doaj.art-27a265246948463cb6b3b451df3230792023-12-28T21:57:27ZengUniversity of Anbarمجلة جامعة الانبار للعلوم الصرفة1991-89412706-67032014-08-0182142210.37652/juaps.2014.123911123911SYNTHESIS AND CHARACTERIZATION OF NOVEL 1,3-OXAZEPANE DERIVATIVES VIA REACTION OF PHENYI SUCCINIC ANHYDRIDE WITH SCHHIF'S BASESAmaadh F. Nassar0Obaid H.Abid1University of Anbar- College of Education for Pure ScienceUniversity of Anbar- College of Education for Pure ScienceNovel 1,3-oxazepane-4,7-dione derivatives were synthesized by the reaction of phenyl succinic anhydride with Schiff‘s bases in anhydrous benzen with high yields. Schiff's bases were synthesized by the reaction of heteroaromatic aldehydes or ketones with primary heterocyclic amines. The resulting products were identified by their melting point and their molecular structures were confirmed by FT-IR , UV-Vis. and 1HNMR spectroscopy.https://juaps.uoanbar.edu.iq/article_123911_d41d8cd98f00b204e9800998ecf8427e.pdfoxazepanephenyl succinic anhydrideschiff basessynthesis |
spellingShingle | Amaadh F. Nassar Obaid H.Abid SYNTHESIS AND CHARACTERIZATION OF NOVEL 1,3-OXAZEPANE DERIVATIVES VIA REACTION OF PHENYI SUCCINIC ANHYDRIDE WITH SCHHIF'S BASES مجلة جامعة الانبار للعلوم الصرفة oxazepane phenyl succinic anhydride schiff bases synthesis |
title | SYNTHESIS AND CHARACTERIZATION OF NOVEL 1,3-OXAZEPANE DERIVATIVES VIA REACTION OF PHENYI SUCCINIC ANHYDRIDE WITH SCHHIF'S BASES |
title_full | SYNTHESIS AND CHARACTERIZATION OF NOVEL 1,3-OXAZEPANE DERIVATIVES VIA REACTION OF PHENYI SUCCINIC ANHYDRIDE WITH SCHHIF'S BASES |
title_fullStr | SYNTHESIS AND CHARACTERIZATION OF NOVEL 1,3-OXAZEPANE DERIVATIVES VIA REACTION OF PHENYI SUCCINIC ANHYDRIDE WITH SCHHIF'S BASES |
title_full_unstemmed | SYNTHESIS AND CHARACTERIZATION OF NOVEL 1,3-OXAZEPANE DERIVATIVES VIA REACTION OF PHENYI SUCCINIC ANHYDRIDE WITH SCHHIF'S BASES |
title_short | SYNTHESIS AND CHARACTERIZATION OF NOVEL 1,3-OXAZEPANE DERIVATIVES VIA REACTION OF PHENYI SUCCINIC ANHYDRIDE WITH SCHHIF'S BASES |
title_sort | synthesis and characterization of novel 1 3 oxazepane derivatives via reaction of phenyi succinic anhydride with schhif s bases |
topic | oxazepane phenyl succinic anhydride schiff bases synthesis |
url | https://juaps.uoanbar.edu.iq/article_123911_d41d8cd98f00b204e9800998ecf8427e.pdf |
work_keys_str_mv | AT amaadhfnassar synthesisandcharacterizationofnovel13oxazepanederivativesviareactionofphenyisuccinicanhydridewithschhifsbases AT obaidhabid synthesisandcharacterizationofnovel13oxazepanederivativesviareactionofphenyisuccinicanhydridewithschhifsbases |