Synthesis and Biochemical effects of magnetite nanoparticle by surfactant-free electrochemical method in an aqueous system:the current density effect
Obejective(s): In this research, magnetite nanoparticles with an average size of 23-36 nm were successfully synthesized via surfactant-free electrochemical method using iron as the anode and water as the electrolyte in a closed aqueous system in the presence of NaOH at room temperature. Methods: The...
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| Format: | Article |
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Iranian Society of Nanomedicine
2016-07-01
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| Series: | Nanomedicine Research Journal |
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| Online Access: | http://www.nanomedicine-rj.com/article_20582_7aa9f1dae4b44bad32fb35e360f3577c.pdf |
| _version_ | 1811283858632474624 |
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| author | Mousa Aliahmad Abbas Rahdar Fardin Sadeghfar Samira Bagheri Mohammad Reza Hajinezhad |
| author_facet | Mousa Aliahmad Abbas Rahdar Fardin Sadeghfar Samira Bagheri Mohammad Reza Hajinezhad |
| author_sort | Mousa Aliahmad |
| collection | DOAJ |
| description | Obejective(s): In this research, magnetite nanoparticles with an average size of 23-36 nm were successfully synthesized via surfactant-free electrochemical method using iron as the anode and water as the electrolyte in a closed aqueous system in the presence of NaOH at room temperature. Methods: The effect of the current density on product formation and particle size was investigated. Particle size was controlled by adjusting the current density. It was found that particle size decreases by decreasing the current density. In addition, the effect of current density on the structural and optical properties of nanostructures were studied by X-ray diffraction, Field emission scanning electron microscopy, Fourier transformed infrared, and vibrating sample magnetometer techniques. Results: The results obtained from the magnetization property study of samples at room temperature showed coactivity and saturation manetization of 0-100 Oe and 27.2- 40.5 emu. g-1, respectively. Finally, the results of biological activity study of nanoparticles on liver and kidney function in male wistar rats demonstrated that oral administration of NPs caused significant alterations to the levels of aspartate transaminase, alanine transaminase, and alkaline phosphatase in serum. Conclusions: No significant changes were detected in the groups treated with 10 and 100 ppm/ day nanostructure (P>0.05). There was a significant increase in the serum level of creatinine and blood urea nitrogen level (p |
| first_indexed | 2024-04-13T02:19:58Z |
| format | Article |
| id | doaj.art-27b384b252204776a986215b9c0f1430 |
| institution | Directory Open Access Journal |
| issn | 2476-3489 2476-7123 |
| language | English |
| last_indexed | 2024-04-13T02:19:58Z |
| publishDate | 2016-07-01 |
| publisher | Iranian Society of Nanomedicine |
| record_format | Article |
| series | Nanomedicine Research Journal |
| spelling | doaj.art-27b384b252204776a986215b9c0f14302022-12-22T03:07:02ZengIranian Society of NanomedicineNanomedicine Research Journal2476-34892476-71232016-07-0111394610.7508/nmrj.2016.01.00620582Synthesis and Biochemical effects of magnetite nanoparticle by surfactant-free electrochemical method in an aqueous system:the current density effectMousa Aliahmad0Abbas Rahdar1Fardin Sadeghfar2Samira Bagheri3Mohammad Reza Hajinezhad4Department of Physics, Faculty of Science, University of Sistan and Baluchestan, Zahedan, IranInstitute of Nano Science and Nano Technology, University of Kashan, Kashan, Iran|Departments of Physics, Faculty of Science, University of Zabol, Zabol, IranDepartments of Physics, Faculty of Science, University of Zabol, Zabol, IranNanotechnology & Catalysis Research Centre (NANOCAT), IPS Building, University of Malaya, 50603 Kuala ‎Lumpur,MalaysiaBasic Veteinary Science Department, Veterinary Faculty, University of Zabol, Zabol, IranObejective(s): In this research, magnetite nanoparticles with an average size of 23-36 nm were successfully synthesized via surfactant-free electrochemical method using iron as the anode and water as the electrolyte in a closed aqueous system in the presence of NaOH at room temperature. Methods: The effect of the current density on product formation and particle size was investigated. Particle size was controlled by adjusting the current density. It was found that particle size decreases by decreasing the current density. In addition, the effect of current density on the structural and optical properties of nanostructures were studied by X-ray diffraction, Field emission scanning electron microscopy, Fourier transformed infrared, and vibrating sample magnetometer techniques. Results: The results obtained from the magnetization property study of samples at room temperature showed coactivity and saturation manetization of 0-100 Oe and 27.2- 40.5 emu. g-1, respectively. Finally, the results of biological activity study of nanoparticles on liver and kidney function in male wistar rats demonstrated that oral administration of NPs caused significant alterations to the levels of aspartate transaminase, alanine transaminase, and alkaline phosphatase in serum. Conclusions: No significant changes were detected in the groups treated with 10 and 100 ppm/ day nanostructure (P>0.05). There was a significant increase in the serum level of creatinine and blood urea nitrogen level (phttp://www.nanomedicine-rj.com/article_20582_7aa9f1dae4b44bad32fb35e360f3577c.pdfVSMFESEMMagnetite nanoparticlesThe current density |
| spellingShingle | Mousa Aliahmad Abbas Rahdar Fardin Sadeghfar Samira Bagheri Mohammad Reza Hajinezhad Synthesis and Biochemical effects of magnetite nanoparticle by surfactant-free electrochemical method in an aqueous system:the current density effect Nanomedicine Research Journal VSM FESEM Magnetite nanoparticles The current density |
| title | Synthesis and Biochemical effects of magnetite nanoparticle by surfactant-free electrochemical method in an aqueous system:the current density effect |
| title_full | Synthesis and Biochemical effects of magnetite nanoparticle by surfactant-free electrochemical method in an aqueous system:the current density effect |
| title_fullStr | Synthesis and Biochemical effects of magnetite nanoparticle by surfactant-free electrochemical method in an aqueous system:the current density effect |
| title_full_unstemmed | Synthesis and Biochemical effects of magnetite nanoparticle by surfactant-free electrochemical method in an aqueous system:the current density effect |
| title_short | Synthesis and Biochemical effects of magnetite nanoparticle by surfactant-free electrochemical method in an aqueous system:the current density effect |
| title_sort | synthesis and biochemical effects of magnetite nanoparticle by surfactant free electrochemical method in an aqueous system the current density effect |
| topic | VSM FESEM Magnetite nanoparticles The current density |
| url | http://www.nanomedicine-rj.com/article_20582_7aa9f1dae4b44bad32fb35e360f3577c.pdf |
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