N,N′-Bis(4-bromophenyl)naphthalene-1,4-dicarboxamide N,N-dimethylacetamide disolvate
The title compound, C24H16Br2N2O2·2C4H9NO, crystallizes in an anti C=O orientation. The two amide groups are twisted away from the naphthalene ring system by 62.67 (8) and 75.93 (7)°. The crystal packing is stabilized by N—H...O and...
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2010-01-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536809051447 |
| _version_ | 1818488736210485248 |
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| author | Lin-Hai Jing |
| author_facet | Lin-Hai Jing |
| author_sort | Lin-Hai Jing |
| collection | DOAJ |
| description | The title compound, C24H16Br2N2O2·2C4H9NO, crystallizes in an anti C=O orientation. The two amide groups are twisted away from the naphthalene ring system by 62.67 (8) and 75.93 (7)°. The crystal packing is stabilized by N—H...O and C—H...O hydrogen bonds. Each of the dimethylacetamide solvent molecules is disordered over two positions, with occupancy ratios of 0.556 (7):0.444 (7) and 0.654 (7):0.346 (7). |
| first_indexed | 2024-12-10T16:55:02Z |
| format | Article |
| id | doaj.art-27f76c25e7414e18a8c879ceed179613 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-10T16:55:02Z |
| publishDate | 2010-01-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-27f76c25e7414e18a8c879ceed1796132022-12-22T01:40:46ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-01-01661o27o2710.1107/S1600536809051447N,N′-Bis(4-bromophenyl)naphthalene-1,4-dicarboxamide N,N-dimethylacetamide disolvateLin-Hai JingThe title compound, C24H16Br2N2O2·2C4H9NO, crystallizes in an anti C=O orientation. The two amide groups are twisted away from the naphthalene ring system by 62.67 (8) and 75.93 (7)°. The crystal packing is stabilized by N—H...O and C—H...O hydrogen bonds. Each of the dimethylacetamide solvent molecules is disordered over two positions, with occupancy ratios of 0.556 (7):0.444 (7) and 0.654 (7):0.346 (7).http://scripts.iucr.org/cgi-bin/paper?S1600536809051447 |
| spellingShingle | Lin-Hai Jing N,N′-Bis(4-bromophenyl)naphthalene-1,4-dicarboxamide N,N-dimethylacetamide disolvate Acta Crystallographica Section E |
| title | N,N′-Bis(4-bromophenyl)naphthalene-1,4-dicarboxamide N,N-dimethylacetamide disolvate |
| title_full | N,N′-Bis(4-bromophenyl)naphthalene-1,4-dicarboxamide N,N-dimethylacetamide disolvate |
| title_fullStr | N,N′-Bis(4-bromophenyl)naphthalene-1,4-dicarboxamide N,N-dimethylacetamide disolvate |
| title_full_unstemmed | N,N′-Bis(4-bromophenyl)naphthalene-1,4-dicarboxamide N,N-dimethylacetamide disolvate |
| title_short | N,N′-Bis(4-bromophenyl)naphthalene-1,4-dicarboxamide N,N-dimethylacetamide disolvate |
| title_sort | n n amp 8242 bis 4 bromophenyl naphthalene 1 4 dicarboxamide n n dimethylacetamide disolvate |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536809051447 |
| work_keys_str_mv | AT linhaijing nnamp8242bis4bromophenylnaphthalene14dicarboxamidenndimethylacetamidedisolvate |