Synthesis of Doped and non-Doped Nano MgO Ceramic Membranes
Doped and non-doped MgO coated thin films on alumina substrates were prepared using a chelating sol-gel method under controlled conditions to prepare nanomaterials with unprecedented properties. The effect of doping of ZnO on thermal, surface and structural properties was investigated using DTA-TG,...
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| Format: | Article |
| Language: | English |
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Sultan Qaboos University
2013-12-01
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| Series: | Sultan Qaboos University Journal for Science |
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| Online Access: | https://journals.squ.edu.om/index.php/squjs/article/view/413 |
| _version_ | 1819093721005686784 |
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| author | Shiraz Labib |
| author_facet | Shiraz Labib |
| author_sort | Shiraz Labib |
| collection | DOAJ |
| description | Doped and non-doped MgO coated thin films on alumina substrates were prepared using a chelating sol-gel method under controlled conditions to prepare nanomaterials with unprecedented properties. The effect of doping of ZnO on thermal, surface and structural properties was investigated using DTA-TG, BET and XRD respectively. Also microstructural studies and coating thickness measurements of MgO thin film were conducted using SEM. An increase in the thermal stability of MgO with increasing ZnO doping percent was observed. The increase of ZnO doping percent showed a marked decrease in the average particle size of MgO powder as a result of the replacement of some Mg2+ by Zn2+ which has similar ionic radius as Mg2+. This decrease in particle size of MgO was also related to the decrease of the degree of MgO crystalinity. The increase of ZnO doping also showed a marked decrease in coating thickness values of the prepared membranes. This decrease was related to the mechanism of ZnO doping into a MgO crystal lattice. |
| first_indexed | 2024-12-21T23:16:00Z |
| format | Article |
| id | doaj.art-2815b37de84b4879b2d03c2dc10a79b8 |
| institution | Directory Open Access Journal |
| issn | 1027-524X 2414-536X |
| language | English |
| last_indexed | 2024-12-21T23:16:00Z |
| publishDate | 2013-12-01 |
| publisher | Sultan Qaboos University |
| record_format | Article |
| series | Sultan Qaboos University Journal for Science |
| spelling | doaj.art-2815b37de84b4879b2d03c2dc10a79b82022-12-21T18:46:54ZengSultan Qaboos UniversitySultan Qaboos University Journal for Science1027-524X2414-536X2013-12-01180253210.24200/squjs.vol18iss0pp25-32408Synthesis of Doped and non-Doped Nano MgO Ceramic MembranesShiraz Labib0Nuclear Chemistry Department, Hot Laboratories Center, Atomic Energy Authority, Cairo, EgyptDoped and non-doped MgO coated thin films on alumina substrates were prepared using a chelating sol-gel method under controlled conditions to prepare nanomaterials with unprecedented properties. The effect of doping of ZnO on thermal, surface and structural properties was investigated using DTA-TG, BET and XRD respectively. Also microstructural studies and coating thickness measurements of MgO thin film were conducted using SEM. An increase in the thermal stability of MgO with increasing ZnO doping percent was observed. The increase of ZnO doping percent showed a marked decrease in the average particle size of MgO powder as a result of the replacement of some Mg2+ by Zn2+ which has similar ionic radius as Mg2+. This decrease in particle size of MgO was also related to the decrease of the degree of MgO crystalinity. The increase of ZnO doping also showed a marked decrease in coating thickness values of the prepared membranes. This decrease was related to the mechanism of ZnO doping into a MgO crystal lattice.https://journals.squ.edu.om/index.php/squjs/article/view/413MgOMgO-ZnOpolymeric sol-geldoping mechanismnano propertiesthin films. |
| spellingShingle | Shiraz Labib Synthesis of Doped and non-Doped Nano MgO Ceramic Membranes Sultan Qaboos University Journal for Science MgO MgO-ZnO polymeric sol-gel doping mechanism nano properties thin films. |
| title | Synthesis of Doped and non-Doped Nano MgO Ceramic Membranes |
| title_full | Synthesis of Doped and non-Doped Nano MgO Ceramic Membranes |
| title_fullStr | Synthesis of Doped and non-Doped Nano MgO Ceramic Membranes |
| title_full_unstemmed | Synthesis of Doped and non-Doped Nano MgO Ceramic Membranes |
| title_short | Synthesis of Doped and non-Doped Nano MgO Ceramic Membranes |
| title_sort | synthesis of doped and non doped nano mgo ceramic membranes |
| topic | MgO MgO-ZnO polymeric sol-gel doping mechanism nano properties thin films. |
| url | https://journals.squ.edu.om/index.php/squjs/article/view/413 |
| work_keys_str_mv | AT shirazlabib synthesisofdopedandnondopednanomgoceramicmembranes |